Consequences of Dispersity on the Self-Assembly of ABA-Type Amphiphilic Block Co-Oligomers
Identifieur interne : 000A30 ( Main/Exploration ); précédent : 000A29; suivant : 000A31Consequences of Dispersity on the Self-Assembly of ABA-Type Amphiphilic Block Co-Oligomers
Auteurs : Anindita Das ; Katja Petkau-Milroy ; Gilian Klerks ; Bas Van Genabeek ; René P. X0a M. Lafleur ; Anja R. A. Palmans ; E. W. MeijerSource :
- ACS Macro Letters [ 2161-1653 ] ; 2018.
Abstract
Intriguingly, little
is known about the impact of dispersity on
the crystallization driven self-assembly (CDSA) of amphiphilic block
copolymers in aqueous media. Here, we investigate the influence of
dispersity on the CDSA of ABA-type amphiphilic block co-oligomers
(ABCOs). Two pairs of ABCOs are synthesized comprising discrete (
Url:
DOI: 10.1021/acsmacrolett.8b00168
PubMed: 29862138
PubMed Central: 5973780
Affiliations:
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Consequences of Dispersity on the Self-Assembly of
ABA-Type Amphiphilic Block Co-Oligomers</title><author><name sortKey="Das, Anindita" sort="Das, Anindita" uniqKey="Das A" first="Anindita" last="Das">Anindita Das</name></author><author><name sortKey="Petkau Milroy, Katja" sort="Petkau Milroy, Katja" uniqKey="Petkau Milroy K" first="Katja" last="Petkau-Milroy">Katja Petkau-Milroy</name></author><author><name sortKey="Klerks, Gilian" sort="Klerks, Gilian" uniqKey="Klerks G" first="Gilian" last="Klerks">Gilian Klerks</name></author><author><name sortKey="Van Genabeek, Bas" sort="Van Genabeek, Bas" uniqKey="Van Genabeek B" first="Bas" last="Van Genabeek">Bas Van Genabeek</name></author><author><name sortKey="Lafleur, Rene P X0a M" sort="Lafleur, Rene P X0a M" uniqKey="Lafleur R" first="René P. X0a M." last="Lafleur">René P. X0a M. Lafleur</name></author><author><name sortKey="Palmans, Anja R A" sort="Palmans, Anja R A" uniqKey="Palmans A" first="Anja R. A." last="Palmans">Anja R. A. Palmans</name></author><author><name sortKey="Meijer, E W" sort="Meijer, E W" uniqKey="Meijer E" first="E. W." last="Meijer">E. W. Meijer</name></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">29862138</idno><idno type="pmc">5973780</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC5973780</idno><idno type="RBID">PMC:5973780</idno><idno type="doi">10.1021/acsmacrolett.8b00168</idno><date when="2018">2018</date><idno type="wicri:Area/Pmc/Corpus">000121</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000121</idno><idno type="wicri:Area/Pmc/Curation">000121</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Curation">000121</idno><idno type="wicri:Area/Pmc/Checkpoint">000615</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Checkpoint">000615</idno><idno type="wicri:source">PubMed</idno><idno type="RBID">pubmed:29862138</idno><idno type="wicri:Area/PubMed/Corpus">000880</idno><idno type="wicri:explorRef" wicri:stream="PubMed" wicri:step="Corpus" wicri:corpus="PubMed">000880</idno><idno type="wicri:Area/PubMed/Curation">000880</idno><idno type="wicri:explorRef" wicri:stream="PubMed" wicri:step="Curation">000880</idno><idno type="wicri:Area/PubMed/Checkpoint">000976</idno><idno type="wicri:explorRef" wicri:stream="Checkpoint" wicri:step="PubMed">000976</idno><idno type="wicri:Area/Ncbi/Merge">001E53</idno><idno type="wicri:Area/Ncbi/Curation">001E53</idno><idno type="wicri:Area/Ncbi/Checkpoint">001E53</idno><idno type="wicri:Area/Main/Merge">000A33</idno><idno type="wicri:Area/Main/Curation">000A30</idno><idno type="wicri:Area/Main/Exploration">000A30</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Consequences of Dispersity on the Self-Assembly of
ABA-Type Amphiphilic Block Co-Oligomers</title><author><name sortKey="Das, Anindita" sort="Das, Anindita" uniqKey="Das A" first="Anindita" last="Das">Anindita Das</name></author><author><name sortKey="Petkau Milroy, Katja" sort="Petkau Milroy, Katja" uniqKey="Petkau Milroy K" first="Katja" last="Petkau-Milroy">Katja Petkau-Milroy</name></author><author><name sortKey="Klerks, Gilian" sort="Klerks, Gilian" uniqKey="Klerks G" first="Gilian" last="Klerks">Gilian Klerks</name></author><author><name sortKey="Van Genabeek, Bas" sort="Van Genabeek, Bas" uniqKey="Van Genabeek B" first="Bas" last="Van Genabeek">Bas Van Genabeek</name></author><author><name sortKey="Lafleur, Rene P X0a M" sort="Lafleur, Rene P X0a M" uniqKey="Lafleur R" first="René P. X0a M." last="Lafleur">René P. X0a M. Lafleur</name></author><author><name sortKey="Palmans, Anja R A" sort="Palmans, Anja R A" uniqKey="Palmans A" first="Anja R. A." last="Palmans">Anja R. A. Palmans</name></author><author><name sortKey="Meijer, E W" sort="Meijer, E W" uniqKey="Meijer E" first="E. W." last="Meijer">E. W. Meijer</name></author></analytic><series><title level="j">ACS Macro Letters</title><idno type="eISSN">2161-1653</idno><imprint><date when="2018">2018</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p content-type="toc-graphic"><graphic xlink:href="mz-2018-00168t_0006" id="ab-tgr1"></graphic></p><p>Intriguingly, little
is known about the impact of dispersity on
the crystallization driven self-assembly (CDSA) of amphiphilic block
copolymers in aqueous media. Here, we investigate the influence of
dispersity on the CDSA of ABA-type amphiphilic block co-oligomers
(ABCOs). Two pairs of ABCOs are synthesized comprising discrete (<italic>Đ</italic> = 1.00) or disperse (<italic>Đ</italic> =
1.20) isotactic <sc>l</sc>-lactic acid 16-mers as the semicrystalline
hydrophobic block and either oligo(ethylene glycol) methyl ether (MeOoEG)
or oligo(tetraethylene glycol succinate) (oTEGSuc) as the discrete
hydrophilic block. Self-assembly studies in water with 10% THF reveal
uniform nanofibers/2D sheets for the discrete oligomers, but such
structural regularity is largely compromised in the disperse oligomers.
The results are corroborated by sharp melting transitions in both
solution and bulk for the discrete ABCOs, unlike their disperse analogues
that show a lack of crystallization. Interestingly, the discrete MeOoEG-LLA
oligomer reveals crystallization driven gelation, illustrating the
contrasting differences between the discrete oligomers and their disperse
counterparts.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Whitesides, G M" uniqKey="Whitesides G">G. M. Whitesides</name></author><author><name sortKey="Boncheva, M" uniqKey="Boncheva M">M. Boncheva</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Mai, Y" uniqKey="Mai Y">Y. Mai</name></author><author><name sortKey="Eisenberg, A" uniqKey="Eisenberg A">A. Eisenberg</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Lutz, J F" uniqKey="Lutz J">J.-F. Lutz</name></author><author><name sortKey="Lehn, J M" uniqKey="Lehn J">J.-M. Lehn</name></author><author><name sortKey="Meijer, E W" uniqKey="Meijer E">E. W. Meijer</name></author><author><name sortKey="Matyjaszewski, K" uniqKey="Matyjaszewski K">K. Matyjaszewski</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Hawker, C J" uniqKey="Hawker C">C. J. 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