Electron ionization‐induced fragmentation of R2N2Fe2(CO)6 complexes with distinct geometries of the tetrahedral core: investigation of µ‐1,2‐(1,2‐diaza‐3‐methylcyclopentane)diylbis(tricarbonyliron) and bis(µ2‐acetophenoniminato)bis(tricarbonyliron)
Identifieur interne : 000D89 ( Istex/Corpus ); précédent : 000D88; suivant : 000D90Electron ionization‐induced fragmentation of R2N2Fe2(CO)6 complexes with distinct geometries of the tetrahedral core: investigation of µ‐1,2‐(1,2‐diaza‐3‐methylcyclopentane)diylbis(tricarbonyliron) and bis(µ2‐acetophenoniminato)bis(tricarbonyliron)
Auteurs : Andrzej ZimniakSource :
- Journal of Mass Spectrometry [ 1076-5174 ] ; 2002-11.
English descriptors
- Teeft :
- Acceleration voltage, Acta crystallogr, Admixture, Andrzej zimniak, Carbon monoxide molecules, Chem, Copyright, Fragmentation, Fragmentation ions, Fragmentation paths, Fragmentation pathways, Fragmentation pattern, Fragmentation patterns, Fragmentation route, Fragmentation routes, Hydrogen cyanide, Iron atoms, Iron core, John wiley sons, Ligand, Mass spectrom, Mass spectrum, Medical university, Metastable ions, Multipath fragmentation, Next step, Nitrogen atoms, Organic ligand, Organic ligands, Pathway, Phenyl substituents, Physical chemistry, Room temperature, Schematic structures, Sequential expulsion, Spectrom, Subsequent elimination, Subsequent loss, Tetrahedral core, Zimniak.
Abstract
Two binuclear bis(tricarbonyliron) title complexes with N2Fe2 tetrahedral cores, 1 and 2, respectively, which show different molecular folding resulting from the appearance (in 1), and absence (in 2) of the NN σ‐bond, were compared in terms of mass spectral fragmentation routes. A multipath fragmentation noted for the molecule 1 revealing internal stress contrasts with the single‐route fragmentation of 2. The fragmentation paths resulting from the admixtures were defined and analyzed from the fragment ion B/E and parent ion B2/E linked scan spectra. Copyright © 2002 John Wiley & Sons, Ltd.
Url:
DOI: 10.1002/jms.377
Links to Exploration step
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<titleGroup><title type="main" xml:lang="en">Electron ionization‐induced fragmentation of R<sub>2</sub>
N<sub>2</sub>
Fe<sub>2</sub>
(CO)<sub>6</sub>
complexes with distinct geometries of the tetrahedral core: investigation of µ‐1,2‐(1,2‐diaza‐3‐methylcyclopentane)diylbis(tricarbonyliron) and bis(µ<sub>2</sub>
‐acetophenoniminato)bis(tricarbonyliron)</title>
<title type="short" xml:lang="en">EI‐induced fragmentation R<sub>2</sub>
N<sub>2</sub>
Fe<sub>2</sub>
(CO)<sub>6</sub>
</title>
</titleGroup>
<creators><creator xml:id="au1" creatorRole="author" affiliationRef="#af1" corresponding="yes"><personName><givenNames>Andrzej</givenNames>
<familyName>Zimniak</familyName>
</personName>
<contactDetails><email>axzimni@farm.amwaw.edu.pl</email>
</contactDetails>
</creator>
</creators>
<affiliationGroup><affiliation xml:id="af1" countryCode="PL" type="organization"><unparsedAffiliation>Department of Physical Chemistry, Faculty of Pharmacy, Medical University of Warsaw, 02‐097 Warsaw, Poland</unparsedAffiliation>
</affiliation>
</affiliationGroup>
<keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1">iron</keyword>
<keyword xml:id="kwd2">bis(tricarbonyliron)</keyword>
<keyword xml:id="kwd3">complexes</keyword>
<keyword xml:id="kwd4">fragmentation</keyword>
<keyword xml:id="kwd5">electron ionization</keyword>
</keywordGroup>
<abstractGroup><abstract type="main" xml:lang="en"><title type="main">Abstract</title>
<p>Two binuclear bis(tricarbonyliron) title complexes with N<sub>2</sub>
Fe<sub>2</sub>
tetrahedral cores, <b>1</b>
and <b>2</b>
, respectively, which show different molecular folding resulting from the appearance (in <b>1</b>
), and absence (in <b>2</b>
) of the NN σ‐bond, were compared in terms of mass spectral fragmentation routes. A multipath fragmentation noted for the molecule <b>1</b>
revealing internal stress contrasts with the single‐route fragmentation of <b>2</b>
. The fragmentation paths resulting from the admixtures were defined and analyzed from the fragment ion <i>B</i>
/<i>E</i>
and parent ion <i>B</i>
<sup>2</sup>
/<i>E</i>
linked scan spectra. Copyright © 2002 John Wiley & Sons, Ltd.</p>
</abstract>
</abstractGroup>
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<mods version="3.6"><titleInfo lang="en"><title>Electron ionization‐induced fragmentation of R2N2Fe2(CO)6 complexes with distinct geometries of the tetrahedral core: investigation of µ‐1,2‐(1,2‐diaza‐3‐methylcyclopentane)diylbis(tricarbonyliron) and bis(µ2‐acetophenoniminato)bis(tricarbonyliron)</title>
</titleInfo>
<titleInfo type="abbreviated" lang="en"><title>EI‐induced fragmentation R2N2Fe2(CO)6</title>
</titleInfo>
<titleInfo type="alternative" contentType="CDATA" lang="en"><title>Electron ionization‐induced fragmentation of R2N2Fe2(CO)6 complexes with distinct geometries of the tetrahedral core: investigation of µ‐1,2‐(1,2‐diaza‐3‐methylcyclopentane)diylbis(tricarbonyliron) and bis(µ2‐acetophenoniminato)bis(tricarbonyliron)</title>
</titleInfo>
<name type="personal"><namePart type="given">Andrzej</namePart>
<namePart type="family">Zimniak</namePart>
<affiliation>Department of Physical Chemistry, Faculty of Pharmacy, Medical University of Warsaw, 02‐097 Warsaw, Poland</affiliation>
<affiliation>E-mail: axzimni@farm.amwaw.edu.pl</affiliation>
<affiliation>Correspondence address: Department of Physical Chemistry, Faculty of Pharmacy, Medical University of Warsaw, Banacha 1, 02‐097 Warsaw, Poland.===</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
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<place><placeTerm type="text">Chichester, UK</placeTerm>
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<dateIssued encoding="w3cdtf">2002-11</dateIssued>
<dateCaptured encoding="w3cdtf">2002-04-16</dateCaptured>
<dateValid encoding="w3cdtf">2002-08-22</dateValid>
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<abstract lang="en">Two binuclear bis(tricarbonyliron) title complexes with N2Fe2 tetrahedral cores, 1 and 2, respectively, which show different molecular folding resulting from the appearance (in 1), and absence (in 2) of the NN σ‐bond, were compared in terms of mass spectral fragmentation routes. A multipath fragmentation noted for the molecule 1 revealing internal stress contrasts with the single‐route fragmentation of 2. The fragmentation paths resulting from the admixtures were defined and analyzed from the fragment ion B/E and parent ion B2/E linked scan spectra. Copyright © 2002 John Wiley & Sons, Ltd.</abstract>
<subject lang="en"><genre>keywords</genre>
<topic>iron</topic>
<topic>bis(tricarbonyliron)</topic>
<topic>complexes</topic>
<topic>fragmentation</topic>
<topic>electron ionization</topic>
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<relatedItem type="host"><titleInfo><title>Journal of Mass Spectrometry</title>
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<subject><genre>article-category</genre>
<topic>Research Article</topic>
<topic>Research Articles</topic>
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<identifier type="ISSN">1076-5174</identifier>
<identifier type="eISSN">1096-9888</identifier>
<identifier type="DOI">10.1002/(ISSN)1096-9888c</identifier>
<identifier type="PublisherID">JMS</identifier>
<part><date>2002</date>
<detail type="volume"><caption>vol.</caption>
<number>37</number>
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<detail type="issue"><caption>no.</caption>
<number>11</number>
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