Chemical Equilibria in the Titanium(ll) Hydride‐Boron Nitride System
Identifieur interne : 000B27 ( Istex/Corpus ); précédent : 000B26; suivant : 000B28Chemical Equilibria in the Titanium(ll) Hydride‐Boron Nitride System
Auteurs : Ewa BenkoSource :
- Journal of the American Ceramic Society [ 0002-7820 ] ; 1995-03.
Abstract
Calculations of chemical equilibria for the TiH2‐BN system using the Villars, Cruise, Smith (VCS) algorithm were carried out for the 27–2027°C temperature range and the 1.3 × 10−3‐1 × 107 Pa pressure range. Two BN:TiH2 molar ratios were selected, 1:1 and 2:1. It follows from these studies that TiH2 can react with BN in a very wide range of pressures and temperatures, giving new phases, namely TiB2, TiB, and TiN. The formation of these phases is strongly influenced by pressure‐temperature parameters. In order to verify theoretical calculations by experiment, equimolar and 2:1 BN:TiH2 batches were prepared and heated at 1427°C under vacuum, in an argon atmosphere, and under high pressure. Phase identification carried out by X‐ray diffraction fully corroborated the computational results.
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DOI: 10.1111/j.1151-2916.1995.tb08233.x
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Two BN:TiH2 molar ratios were selected, 1:1 and 2:1. It follows from these studies that TiH2 can react with BN in a very wide range of pressures and temperatures, giving new phases, namely TiB2, TiB, and TiN. The formation of these phases is strongly influenced by pressure‐temperature parameters. In order to verify theoretical calculations by experiment, equimolar and 2:1 BN:TiH2 batches were prepared and heated at 1427°C under vacuum, in an argon atmosphere, and under high pressure. 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Received May 26, 1994; approved September 14, 1994</unparsedEditorialHistory><countGroup><count type="referenceTotal" number="7"></count><count type="linksCrossRef" number="1"></count></countGroup><titleGroup><title type="main">Chemical Equilibria in the Titanium(ll) Hydride‐Boron Nitride System</title></titleGroup><creators><creator creatorRole="author" xml:id="cr1" affiliationRef="#a1"><personName><givenNames>Ewa</givenNames><familyName>Benko</familyName></personName></creator></creators><affiliationGroup><affiliation xml:id="a1" countryCode="PL"><unparsedAffiliation>Institute of Metal Cutting, 30–011 Krakow Wroclawska 37A, Poland</unparsedAffiliation></affiliation></affiliationGroup><abstractGroup><abstract type="main" xml:lang="en"><p>Calculations of chemical equilibria for the TiH<sub>2</sub>‐BN system using the Villars, Cruise, Smith (VCS) algorithm were carried out for the 27–2027°C temperature range and the 1.3 × 10<sup>−3</sup>‐1 × 10<sup>7</sup> Pa pressure range. Two BN:TiH<sub>2</sub> molar ratios were selected, 1:1 and 2:1. It follows from these studies that TiH<sub>2</sub> can react with BN in a very wide range of pressures and temperatures, giving new phases, namely TiB<sub>2</sub>, TiB, and TiN. The formation of these phases is strongly influenced by pressure‐temperature parameters. In order to verify theoretical calculations by experiment, equimolar and 2:1 BN:TiH<sub>2</sub> batches were prepared and heated at 1427°C under vacuum, in an argon atmosphere, and under high pressure. Phase identification carried out by X‐ray diffraction fully corroborated the computational results.</p></abstract></abstractGroup></contentMeta><noteGroup><note xml:id="n-fnt-1" numbered="no"><p>Z. Munir‐contributing editor</p></note><note xml:id="n-fnt-2" numbered="no"><p>Supported by the Polish State Committee for Scientific Research under Grant No. 77339203.</p></note></noteGroup></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Chemical Equilibria in the Titanium(ll) Hydride‐Boron Nitride System</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Chemical Equilibria in the Titanium(ll) Hydride‐Boron Nitride System</title></titleInfo><name type="personal"><namePart type="given">Ewa</namePart><namePart type="family">Benko</namePart><affiliation>Institute of Metal Cutting, 30–011 Krakow Wroclawska 37A, Poland</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article" displayLabel="article" authority="ISTEX" authorityURI="https://content-type.data.istex.fr" valueURI="https://content-type.data.istex.fr/ark:/67375/XTP-6N5SZHKN-D">article</genre><originInfo><publisher>Blackwell Publishing Ltd</publisher><place><placeTerm type="text">Oxford, UK</placeTerm></place><dateIssued encoding="w3cdtf">1995-03</dateIssued><edition>Manuscript No. 193544. Received May 26, 1994; approved September 14, 1994</edition><copyrightDate encoding="w3cdtf">1995</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><extent unit="references">7</extent><extent unit="linksCrossRef">1</extent></physicalDescription><abstract lang="en">Calculations of chemical equilibria for the TiH2‐BN system using the Villars, Cruise, Smith (VCS) algorithm were carried out for the 27–2027°C temperature range and the 1.3 × 10−3‐1 × 107 Pa pressure range. Two BN:TiH2 molar ratios were selected, 1:1 and 2:1. It follows from these studies that TiH2 can react with BN in a very wide range of pressures and temperatures, giving new phases, namely TiB2, TiB, and TiN. The formation of these phases is strongly influenced by pressure‐temperature parameters. In order to verify theoretical calculations by experiment, equimolar and 2:1 BN:TiH2 batches were prepared and heated at 1427°C under vacuum, in an argon atmosphere, and under high pressure. Phase identification carried out by X‐ray diffraction fully corroborated the computational results.</abstract><relatedItem type="host"><titleInfo><title>Journal of the American Ceramic Society</title></titleInfo><genre type="journal" authority="ISTEX" authorityURI="https://publication-type.data.istex.fr" valueURI="https://publication-type.data.istex.fr/ark:/67375/JMC-0GLKJH51-B">journal</genre><identifier type="ISSN">0002-7820</identifier><identifier type="eISSN">1551-2916</identifier><identifier type="DOI">10.1111/(ISSN)1551-2916</identifier><identifier type="PublisherID">JACE</identifier><part><date>1995</date><detail type="volume"><caption>vol.</caption><number>78</number></detail><detail type="issue"><caption>no.</caption><number>3</number></detail><extent unit="pages"><start>685</start><end>688</end><total>4</total></extent></part></relatedItem><relatedItem type="references" displayLabel="cit1"><titleInfo><title>Issledovanie Vzaimodejstvija Kubiceskogo Nitrida Bora z Perechodnym Metallami i Ich KarbidamiSint. Almazy</title></titleInfo><name type="personal"><namePart type="given">W. P.</namePart><namePart type="family">Bondarenko</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>other</genre><part><date>1978</date></part></relatedItem><relatedItem type="references" displayLabel="cit2"><titleInfo><title>Termodinamiceskoe Issledovanie Vzaimodejstvija Nitrida Bora z Perechodnymi MetallamiSint. Almazy</title></titleInfo><name type="personal"><namePart type="given">W. P.</namePart><namePart type="family">Bondarenko</namePart><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">A. P.</namePart><namePart type="family">Chalepa</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>other</genre><part><date>1977</date></part></relatedItem><relatedItem type="references" displayLabel="cit3"><titleInfo><title>Vzaimodejstvie Nitrida Bora z Perechodnymi Metallami, Ich Boridami i NitridamiPoroshk. Metall</title></titleInfo><name type="personal"><namePart type="given">G. V.</namePart><namePart type="family">Samsonov</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>other</genre><part><date>1973</date></part></relatedItem><relatedItem type="references" displayLabel="cit4"><titleInfo><title>Vzaimodejstvie Nitrida Bora, Alumnija i Materialov Na Ich Osnove z Fugoplavkimi MetallamiPoroshk. Metall</title></titleInfo><name type="personal"><namePart type="given">A. L.</namePart><namePart type="family">Borisova</namePart><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">I. S.</namePart><namePart type="family">Marceniuk</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>other</genre><part><date>1975</date></part></relatedItem><relatedItem type="references" displayLabel="cit5"><titleInfo><title>W. P. Smith and R. W. Missen, Chemical Reaction Equilibrium Analysis: Theory and Algorithms. 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Prophet, Janaf Thermochemical Tables, 2nd ed., NSRDS‐NBS37, National Bureau of Standards, Washington , DC , 1971.</note><name type="personal"><namePart type="given">D. R.</namePart><namePart type="family">Stull</namePart><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">H.</namePart><namePart type="family">Prophet</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>book</genre><originInfo><publisher>National Bureau of Standards</publisher></originInfo><part><date>1971</date></part></relatedItem><relatedItem type="references" displayLabel="cit7"><titleInfo><title>B. D. Cullity, Elements of X‐ray Diffraction. Addison‐Wesley Publishing Co., London , U.K. , 1959.</title></titleInfo><note type="citation/reference">B. D. Cullity, Elements of X‐ray Diffraction. Addison‐Wesley Publishing Co., London , U.K. , 1959.</note><name type="personal"><namePart type="given">B. D.</namePart><namePart type="family">Cullity</namePart><role><roleTerm type="text">author</roleTerm></role></name><genre>book</genre><originInfo><publisher>Addison‐Wesley Publishing Co.</publisher></originInfo><part><date>1959</date></part></relatedItem><identifier type="istex">86B837F6C08E6DDACB9E493D149F13025A8D6486</identifier><identifier type="ark">ark:/67375/WNG-Z57SF0T7-X</identifier><identifier type="DOI">10.1111/j.1151-2916.1995.tb08233.x</identifier><identifier type="ArticleID">JACE685</identifier><accessCondition type="use and reproduction" contentType="copyright">© Wiley. 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