Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate
Identifieur interne : 000376 ( Istex/Corpus ); précédent : 000375; suivant : 000377Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate
Auteurs : M. Belhouchet ; T. MhiriSource :
- Crystallography Reports [ 1063-7745 ] ; 2013-01-01.
Abstract
Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.
Url:
DOI: 10.1134/S106377451301015X
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Mhiri</name><affiliation><mods:affiliation>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:E92BB3CEAF6E1EB05C104ACA2830249CFE849304</idno><date when="2013" year="2013">2013</date><idno type="doi">10.1134/S106377451301015X</idno><idno type="url">https://api.istex.fr/ark:/67375/VQC-3RWRKJQQ-7/fulltext.pdf</idno><idno type="wicri:Area/Istex/Corpus">000376</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000376</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main" xml:lang="en">Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate</title><author><name sortKey="Belhouchet, M" sort="Belhouchet, M" uniqKey="Belhouchet M" first="M." last="Belhouchet">M. Belhouchet</name><affiliation><mods:affiliation>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</mods:affiliation></affiliation><affiliation><mods:affiliation>E-mail: belhouchet2002@yahoo.fr</mods:affiliation></affiliation></author><author><name sortKey="Mhiri, T" sort="Mhiri, T" uniqKey="Mhiri T" first="T." last="Mhiri">T. Mhiri</name><affiliation><mods:affiliation>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Crystallography Reports</title><title level="j" type="abbrev">Crystallogr. Rep.</title><idno type="ISSN">1063-7745</idno><idno type="eISSN">1562-689X</idno><imprint><publisher>SP MAIK Nauka/Interperiodica</publisher><pubPlace>Dordrecht</pubPlace><date type="published" when="2013-01-01">2013-01-01</date><biblScope unit="volume">58</biblScope><biblScope unit="issue">1</biblScope><biblScope unit="page" from="115">115</biblScope><biblScope unit="page" to="118">118</biblScope></imprint><idno type="ISSN">1063-7745</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1063-7745</idno></seriesStmt></fileDesc><profileDesc><textClass></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.</div></front></TEI><istex><corpusName>springer-journals</corpusName><author><json:item><name>M. Belhouchet</name><affiliations><json:string>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</json:string><json:string>E-mail: belhouchet2002@yahoo.fr</json:string></affiliations></json:item><json:item><name>T. Mhiri</name><affiliations><json:string>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</json:string></affiliations></json:item></author><articleId><json:string>7715</json:string><json:string>S106377451301015X</json:string></articleId><arkIstex>ark:/67375/VQC-3RWRKJQQ-7</arkIstex><language><json:string>eng</json:string></language><originalGenre><json:string>OriginalPaper</json:string></originalGenre><abstract>Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. 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Rep.</title><idno type="pISSN">1063-7745</idno><idno type="eISSN">1562-689X</idno><idno type="journal-ID">true</idno><idno type="issue-article-count">29</idno><idno type="volume-issue-count">7</idno><imprint><publisher>SP MAIK Nauka/Interperiodica</publisher><pubPlace>Dordrecht</pubPlace><date type="published" when="2013-01-01"></date><biblScope unit="volume">58</biblScope><biblScope unit="issue">1</biblScope><biblScope unit="page" from="115">115</biblScope><biblScope unit="page" to="118">118</biblScope></imprint></monogr></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>2011-09-29</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.</p></abstract><textClass><keywords scheme="Journal-Subject-Collection"><list><label>SC12</label><item><term>Physics and Astronomy</term></item></list></keywords></textClass><textClass><keywords scheme="Journal-Subject-Group"><list><label>SCP</label><item><term>Physics</term></item><label>SCP25056</label><item><term>Crystallography</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="2011-09-29">Created</change><change when="2013-01-01">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><extension>txt</extension><original>false</original><mimetype>text/plain</mimetype><uri>https://api.istex.fr/ark:/67375/VQC-3RWRKJQQ-7/fulltext.txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="corpus springer-journals not found" wicri:toSee="no header"><istex:xmlDeclaration>version="1.0" encoding="UTF-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//Springer-Verlag//DTD A++ V2.4//EN" URI="http://devel.springer.de/A++/V2.4/DTD/A++V2.4.dtd" name="istex:docType"></istex:docType><istex:document><Publisher><PublisherInfo><PublisherName>SP MAIK Nauka/Interperiodica</PublisherName><PublisherLocation>Dordrecht</PublisherLocation><PublisherImprintName>MAIK Nauka/Interperiodica</PublisherImprintName></PublisherInfo><Journal OutputMedium="All"><JournalInfo JournalProductType="ArchiveJournal" NumberingStyle="Unnumbered"><JournalID>11445</JournalID><JournalPrintISSN>1063-7745</JournalPrintISSN><JournalElectronicISSN>1562-689X</JournalElectronicISSN><JournalTitle>Crystallography Reports</JournalTitle><JournalAbbreviatedTitle>Crystallogr. Rep.</JournalAbbreviatedTitle><JournalSubjectGroup><JournalSubject Code="SCP" Type="Primary">Physics</JournalSubject><JournalSubject Code="SCP25056" Priority="1" Type="Secondary">Crystallography</JournalSubject><SubjectCollection Code="SC12">Physics and Astronomy</SubjectCollection></JournalSubjectGroup></JournalInfo><Volume OutputMedium="All"><VolumeInfo TocLevels="0" VolumeType="Regular"><VolumeIDStart>58</VolumeIDStart><VolumeIDEnd>58</VolumeIDEnd><VolumeIssueCount>7</VolumeIssueCount></VolumeInfo><Issue IssueType="Regular" OutputMedium="All"><IssueInfo IssueType="Regular" TocLevels="0"><IssueIDStart>1</IssueIDStart><IssueIDEnd>1</IssueIDEnd><IssueArticleCount>29</IssueArticleCount><IssueHistory><OnlineDate><Year>2013</Year><Month>1</Month><Day>25</Day></OnlineDate><CoverDate><Year>2013</Year><Month>1</Month></CoverDate><PricelistYear>2013</PricelistYear></IssueHistory><IssueCopyright><CopyrightHolderName>Pleiades Publishing, Ltd.</CopyrightHolderName><CopyrightYear>2013</CopyrightYear></IssueCopyright></IssueInfo><Article ID="S106377451301015X" OutputMedium="All"><ArticleInfo ArticleType="OriginalPaper" ContainsESM="No" Language="En" NumberingStyle="Unnumbered" TocLevels="0"><ArticleID>7715</ArticleID><ArticleDOI>10.1134/S106377451301015X</ArticleDOI><ArticleSequenceNumber>15</ArticleSequenceNumber><ArticleTitle Language="En">Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate</ArticleTitle><ArticleCategory>Structure of Organic Compounds</ArticleCategory><ArticleFirstPage>115</ArticleFirstPage><ArticleLastPage>118</ArticleLastPage><ArticleHistory><RegistrationDate><Year>2013</Year><Month>1</Month><Day>22</Day></RegistrationDate><Received><Year>2011</Year><Month>9</Month><Day>29</Day></Received><OnlineDate><Year>2013</Year><Month>1</Month><Day>25</Day></OnlineDate></ArticleHistory><ArticleCopyright><CopyrightHolderName>Pleiades Publishing, Ltd.</CopyrightHolderName><CopyrightYear>2013</CopyrightYear></ArticleCopyright><ArticleGrants Type="Regular"><MetadataGrant Grant="OpenAccess"></MetadataGrant><AbstractGrant Grant="OpenAccess"></AbstractGrant><BodyPDFGrant Grant="Restricted"></BodyPDFGrant><BodyHTMLGrant Grant="Restricted"></BodyHTMLGrant><BibliographyGrant Grant="Restricted"></BibliographyGrant><ESMGrant Grant="Restricted"></ESMGrant></ArticleGrants></ArticleInfo><ArticleHeader><AuthorGroup><Author AffiliationIDS="Aff1" CorrespondingAffiliationID="Aff1"><AuthorName DisplayOrder="Western"><GivenName>M.</GivenName><FamilyName>Belhouchet</FamilyName></AuthorName><Contact><Email>belhouchet2002@yahoo.fr</Email></Contact></Author><Author AffiliationIDS="Aff1"><AuthorName DisplayOrder="Western"><GivenName>T.</GivenName><FamilyName>Mhiri</FamilyName></AuthorName></Author><Affiliation ID="Aff1"><OrgDivision>Solid State Laboratory, Sfax Faculty of Science</OrgDivision><OrgName>University of Sfax</OrgName><OrgAddress><Postbox>BP 1171</Postbox><Postcode>3000</Postcode><City>Sfax</City><Country Code="TN">Tunisia</Country></OrgAddress></Affiliation></AuthorGroup><Abstract ID="Abs1" Language="En"><Heading>Abstract</Heading><Para>The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C<Subscript>6</Subscript>H<Subscript>3</Subscript>(NH<Subscript>3</Subscript>)(OH)SO<Subscript>3</Subscript> · 0.5H<Subscript>2</Subscript>O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: <Emphasis Type="Italic">a</Emphasis> = 11.2395(3), <Emphasis Type="Italic">b</Emphasis> = 10.3814(3), <Emphasis Type="Italic">c</Emphasis> = 13.7509(4) Å, β = 100.326(1)°, <Emphasis Type="Italic">V</Emphasis> = 1578.49(8) Å<Superscript>3</Superscript>, space group <Emphasis Type="Italic">P</Emphasis>2<Subscript>1</Subscript>/<Emphasis Type="Italic">n</Emphasis>, <Emphasis Type="Italic">Z</Emphasis> = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.</Para></Abstract><ArticleNote Type="Misc"><SimplePara>The article is published in the original.</SimplePara></ArticleNote></ArticleHeader><NoBody></NoBody></Article></Issue></Volume></Journal></Publisher></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate</title></titleInfo><titleInfo type="alternative" contentType="CDATA"><title>Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate</title></titleInfo><name type="personal" displayLabel="corresp"><namePart type="given">M.</namePart><namePart type="family">Belhouchet</namePart><affiliation>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</affiliation><affiliation>E-mail: belhouchet2002@yahoo.fr</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">T.</namePart><namePart type="family">Mhiri</namePart><affiliation>Solid State Laboratory, Sfax Faculty of Science, University of Sfax, BP 1171, 3000, Sfax, Tunisia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="OriginalPaper" authority="ISTEX" authorityURI="https://content-type.data.istex.fr" valueURI="https://content-type.data.istex.fr/ark:/67375/XTP-1JC4F85T-7">research-article</genre><originInfo><publisher>SP MAIK Nauka/Interperiodica</publisher><place><placeTerm type="text">Dordrecht</placeTerm></place><dateCreated encoding="w3cdtf">2011-09-29</dateCreated><dateIssued encoding="w3cdtf">2013-01-01</dateIssued><copyrightDate encoding="w3cdtf">2013</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><abstract lang="en">Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.</abstract><note>Structure of Organic Compounds</note><relatedItem type="host"><titleInfo><title>Crystallography Reports</title></titleInfo><titleInfo type="abbreviated"><title>Crystallogr. 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