Recyclable Keggin Heteropolyacids as an Environmentally Benign Catalyst for the Synthesis of New 2-Benzoylamino-N-phenyl-benzamide Derivatives under Microwave Irradiations at Solvent-Free Conditions and the Evaluation of Biological Activity
Identifieur interne : 000E70 ( Main/Merge ); précédent : 000E69; suivant : 000E71Recyclable Keggin Heteropolyacids as an Environmentally Benign Catalyst for the Synthesis of New 2-Benzoylamino-N-phenyl-benzamide Derivatives under Microwave Irradiations at Solvent-Free Conditions and the Evaluation of Biological Activity
Auteurs : Karima Ighilahriz-Boubchir [Algérie] ; Baya Boutemeur-Kheddis ; Cherifa Rabia ; Malika Makhloufi-Chebli [Algérie] ; Maamar Hamdi ; Artur M. S. SilvaSource :
- Molecules : A Journal of Synthetic Chemistry and Natural Product Chemistry [ 1420-3049 ] ; 2017.
Abstract
2-Benzoylamino-
Url:
DOI: 10.3390/molecules23010008
PubMed: 29267237
PubMed Central: 5943967
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PMC:5943967Le document en format XML
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-phenyl-benzamide Derivatives under Microwave Irradiations at Solvent-Free Conditions and the Evaluation of Biological Activity</title>
<author><name sortKey="Ighilahriz Boubchir, Karima" sort="Ighilahriz Boubchir, Karima" uniqKey="Ighilahriz Boubchir K" first="Karima" last="Ighilahriz-Boubchir">Karima Ighilahriz-Boubchir</name>
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(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
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<author><name sortKey="Rabia, Cherifa" sort="Rabia, Cherifa" uniqKey="Rabia C" first="Cherifa" last="Rabia">Cherifa Rabia</name>
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(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
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<author><name sortKey="Silva, Artur M S" sort="Silva, Artur M S" uniqKey="Silva A" first="Artur M. S." last="Silva">Artur M. S. Silva</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Recyclable Keggin Heteropolyacids as an Environmentally Benign Catalyst for the Synthesis of New 2-Benzoylamino-<italic>N</italic>
-phenyl-benzamide Derivatives under Microwave Irradiations at Solvent-Free Conditions and the Evaluation of Biological Activity</title>
<author><name sortKey="Ighilahriz Boubchir, Karima" sort="Ighilahriz Boubchir, Karima" uniqKey="Ighilahriz Boubchir K" first="Karima" last="Ighilahriz-Boubchir">Karima Ighilahriz-Boubchir</name>
<affiliation><nlm:aff id="af1-molecules-23-00008">Laboratoire de Chimie Organique Appliquée (Equipe Hétérocycles), Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediène, BP 32, El-Alia, Bab-Ezzouar 16111, Algeria;<email>karima_ighil@yahoo.fr</email>
(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
(M.M.-C.);<email>prhamdi@gmail.com</email>
(M.H.)</nlm:aff>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="af2-molecules-23-00008">Laboratoire de Physique et Chimie des Matériaux (LPCM), Université Mouloud Mammeri, BP17RP, Tizi Ouzou 15000, Algeria</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea>Laboratoire de Physique et Chimie des Matériaux (LPCM), Université Mouloud Mammeri, BP17RP, Tizi Ouzou 15000</wicri:regionArea>
<wicri:noRegion>Tizi Ouzou 15000</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Boutemeur Kheddis, Baya" sort="Boutemeur Kheddis, Baya" uniqKey="Boutemeur Kheddis B" first="Baya" last="Boutemeur-Kheddis">Baya Boutemeur-Kheddis</name>
<affiliation><nlm:aff id="af1-molecules-23-00008">Laboratoire de Chimie Organique Appliquée (Equipe Hétérocycles), Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediène, BP 32, El-Alia, Bab-Ezzouar 16111, Algeria;<email>karima_ighil@yahoo.fr</email>
(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
(M.M.-C.);<email>prhamdi@gmail.com</email>
(M.H.)</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Rabia, Cherifa" sort="Rabia, Cherifa" uniqKey="Rabia C" first="Cherifa" last="Rabia">Cherifa Rabia</name>
<affiliation><nlm:aff id="af3-molecules-23-00008">Laboratoire de Chimie du Gaz Naturel, Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediène, BP 32, El-Alia, Bab-Ezzouar 16111, Algeria;<email>c_rabia@yahoo.fr</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Makhloufi Chebli, Malika" sort="Makhloufi Chebli, Malika" uniqKey="Makhloufi Chebli M" first="Malika" last="Makhloufi-Chebli">Malika Makhloufi-Chebli</name>
<affiliation><nlm:aff id="af1-molecules-23-00008">Laboratoire de Chimie Organique Appliquée (Equipe Hétérocycles), Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediène, BP 32, El-Alia, Bab-Ezzouar 16111, Algeria;<email>karima_ighil@yahoo.fr</email>
(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
(M.M.-C.);<email>prhamdi@gmail.com</email>
(M.H.)</nlm:aff>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="af2-molecules-23-00008">Laboratoire de Physique et Chimie des Matériaux (LPCM), Université Mouloud Mammeri, BP17RP, Tizi Ouzou 15000, Algeria</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea>Laboratoire de Physique et Chimie des Matériaux (LPCM), Université Mouloud Mammeri, BP17RP, Tizi Ouzou 15000</wicri:regionArea>
<wicri:noRegion>Tizi Ouzou 15000</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Hamdi, Maamar" sort="Hamdi, Maamar" uniqKey="Hamdi M" first="Maamar" last="Hamdi">Maamar Hamdi</name>
<affiliation><nlm:aff id="af1-molecules-23-00008">Laboratoire de Chimie Organique Appliquée (Equipe Hétérocycles), Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediène, BP 32, El-Alia, Bab-Ezzouar 16111, Algeria;<email>karima_ighil@yahoo.fr</email>
(K.I.-B.);<email>makhloufi_malika@yahoo.fr</email>
(M.M.-C.);<email>prhamdi@gmail.com</email>
(M.H.)</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Silva, Artur M S" sort="Silva, Artur M S" uniqKey="Silva A" first="Artur M. S." last="Silva">Artur M. S. Silva</name>
<affiliation><nlm:aff id="af4-molecules-23-00008">Department of Chemistry & QOPNA, University of Aveiro, 3810-193 Aveiro, Portugal;<email>artur.silva@ua.pt</email>
</nlm:aff>
</affiliation>
</author>
</analytic>
<series><title level="j">Molecules : A Journal of Synthetic Chemistry and Natural Product Chemistry</title>
<idno type="eISSN">1420-3049</idno>
<imprint><date when="2017">2017</date>
</imprint>
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<front><div type="abstract" xml:lang="en"><p>2-Benzoylamino-<italic>N</italic>
-phenyl-benzamide derivatives (<bold>5a</bold>
–<bold>h</bold>
) were prepared from 2-phenyl-3,1-(4<italic>H</italic>
)-benzoxazin-4-one <bold>3</bold>
and substituted anilines <bold>4a</bold>
–<bold>h</bold>
in the presence of a Keggin-type heteropolyacids series (H<sub>3</sub>
PW<sub>12</sub>
O<sub>40</sub>
·13H<sub>2</sub>
O; H<sub>4</sub>
SiW<sub>12</sub>
O<sub>40</sub>
·13H<sub>2</sub>
O; H<sub>4</sub>
SiMo<sub>12</sub>
O<sub>40</sub>
·13H<sub>2</sub>
O; and H<sub>3</sub>
PMo<sub>12</sub>
O<sub>40</sub>
·13H<sub>2</sub>
O) as catalysts without solvent and under microwave irradiation. We found that the use of H<sub>3</sub>
PW<sub>12</sub>
O<sub>40</sub>
·13H<sub>2</sub>
O acid coupled to microwave irradiation allowed obtaining a high-yielding reaction with a short time. The compound structures were established by <sup>1</sup>
H-NMR and <sup>13</sup>
C-NMR. The antibacterial and antifungal activities of the synthesized compounds exhibited an inhibition of the growth of bacteria and fungi.</p>
</div>
</front>
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