Effects of factors and interacted factors on the optimal decolorization process of methyl orange by ozone
Identifieur interne : 000188 ( Istex/Corpus ); précédent : 000187; suivant : 000189Effects of factors and interacted factors on the optimal decolorization process of methyl orange by ozone
Auteurs : Lung-Chyuan ChenSource :
- Water Research [ 0043-1354 ] ; 1999.
English descriptors
Abstract
The decolorization of methyl orange by ozone is effectively carried out in this study. Factors affecting the decolorization rate of methyl orange are investigated by a 25−1 fractional factorial design method. The influences of the main factor and two-factor interaction effects of the operating variables of pH, reaction temperature, agitation rate and concentrations of methyl orange and ozone stream on decolorization are established. The results show that the effect of concentration of ozone stream is the most important among the five main factor effects. Interaction between temperature and ozone stream concentration is the most significant effect among the ten two-factor interaction effects. A quadratic form fit using a modified central composite experimental design is obtained, and it is proved to be adequate for this system according to the multiple correlation coefficient and variance analysis.
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DOI: 10.1016/S0043-1354(99)00188-8
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<front><div type="abstract" xml:lang="en">The decolorization of methyl orange by ozone is effectively carried out in this study. Factors affecting the decolorization rate of methyl orange are investigated by a 25−1 fractional factorial design method. The influences of the main factor and two-factor interaction effects of the operating variables of pH, reaction temperature, agitation rate and concentrations of methyl orange and ozone stream on decolorization are established. The results show that the effect of concentration of ozone stream is the most important among the five main factor effects. Interaction between temperature and ozone stream concentration is the most significant effect among the ten two-factor interaction effects. A quadratic form fit using a modified central composite experimental design is obtained, and it is proved to be adequate for this system according to the multiple correlation coefficient and variance analysis.</div>
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<notesStmt><note type="content">Fig. 1: The typical runs of the decolorization of methyl orange. Volume of solution: 300ml, temperature: 29°C, stir rate: 400rpm. Line 1: air: 980ml/min, pH: 9.25, line 2: ozone: 8.0mg/l, 980ml/min, pH: 9.25, line 3: ozone: 8.0mg/l, 980ml/min, pH: 8.0</note>
<note type="content">Fig. 2: The UV–Vis spectroscopy of methyl orange solution during the run. Temperature: 29°C, initial pH: 8.5, stir rate: 400rpm, volume of solution: 300ml, ozone: 8.0mg/l, 980ml/min, concentration of methyl orange: 40mg/l.</note>
<note type="content">Fig. 3: The single factor effect of pH on the decolorization rate. Concentration of methyl orange: 40mg/l, stir rate: 400rpm, temperature: 29°C, ozone: 8.0mg/l, 980ml/min, volume of solution: 300ml.</note>
<note type="content">Fig. 4: The change of pH of methyl orange solution with decolorization time. Concentration of methyl orange: 32.5mg/l, temperature:29°C, ozone: 8.0mg/l, 980ml/min, stir rate: 400rpm.</note>
<note type="content">Fig. 5: Illustrations of the combination effects of temperature, concentrations of methyl orange and ozone on the decolorization rate.</note>
<note type="content">Fig. 6: The single factor effect of temperature on the decolorization rate. concentration of methyl orange: 40mg/l, stir rate: 400rpm, ozone: 8.0mg/l, 980ml/min, initial pH: 10.0.</note>
<note type="content">Fig. 7: The contour lines of decolorization rate from the concentrations of methyl orange and ozone applying 34°C as the reaction temperature.</note>
<note type="content">Table 1: Factors and levels for the 25−1 fractional factorial design</note>
<note type="content">Table 2: The experimental results of the 25−1 fractional factorial design matrix according to the defining relation of I=−ABCDE</note>
<note type="content">Table 3: Estimates of the effects for the 25−1 fractional factorial design with the defining relation of I=−ABCDE by Yates' algorithm</note>
<note type="content">Table 4: Factors and levels for the modified central composite design</note>
<note type="content">Table 5: The experimental data for the empirical model building by the modified central composite design</note>
<note type="content">Table 6: Variance analysis for the quadratic form fit of average decolorization rate</note>
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<head><ce:title>Effects of factors and interacted factors on the optimal decolorization process of methyl orange by ozone</ce:title>
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<ce:abstract-sec><ce:simple-para>The decolorization of methyl orange by ozone is effectively carried out in this study. Factors affecting the decolorization rate of methyl orange are investigated by a 2<ce:sup>5−1</ce:sup>
fractional factorial design method. The influences of the main factor and two-factor interaction effects of the operating variables of pH, reaction temperature, agitation rate and concentrations of methyl orange and ozone stream on decolorization are established. The results show that the effect of concentration of ozone stream is the most important among the five main factor effects. Interaction between temperature and ozone stream concentration is the most significant effect among the ten two-factor interaction effects. A quadratic form fit using a modified central composite experimental design is obtained, and it is proved to be adequate for this system according to the multiple correlation coefficient and variance analysis.</ce:simple-para>
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<abstract lang="en">The decolorization of methyl orange by ozone is effectively carried out in this study. Factors affecting the decolorization rate of methyl orange are investigated by a 25−1 fractional factorial design method. The influences of the main factor and two-factor interaction effects of the operating variables of pH, reaction temperature, agitation rate and concentrations of methyl orange and ozone stream on decolorization are established. The results show that the effect of concentration of ozone stream is the most important among the five main factor effects. Interaction between temperature and ozone stream concentration is the most significant effect among the ten two-factor interaction effects. A quadratic form fit using a modified central composite experimental design is obtained, and it is proved to be adequate for this system according to the multiple correlation coefficient and variance analysis.</abstract>
<note type="content">Fig. 1: The typical runs of the decolorization of methyl orange. Volume of solution: 300ml, temperature: 29°C, stir rate: 400rpm. Line 1: air: 980ml/min, pH: 9.25, line 2: ozone: 8.0mg/l, 980ml/min, pH: 9.25, line 3: ozone: 8.0mg/l, 980ml/min, pH: 8.0</note>
<note type="content">Fig. 2: The UV–Vis spectroscopy of methyl orange solution during the run. Temperature: 29°C, initial pH: 8.5, stir rate: 400rpm, volume of solution: 300ml, ozone: 8.0mg/l, 980ml/min, concentration of methyl orange: 40mg/l.</note>
<note type="content">Fig. 3: The single factor effect of pH on the decolorization rate. Concentration of methyl orange: 40mg/l, stir rate: 400rpm, temperature: 29°C, ozone: 8.0mg/l, 980ml/min, volume of solution: 300ml.</note>
<note type="content">Fig. 4: The change of pH of methyl orange solution with decolorization time. Concentration of methyl orange: 32.5mg/l, temperature:29°C, ozone: 8.0mg/l, 980ml/min, stir rate: 400rpm.</note>
<note type="content">Fig. 5: Illustrations of the combination effects of temperature, concentrations of methyl orange and ozone on the decolorization rate.</note>
<note type="content">Fig. 6: The single factor effect of temperature on the decolorization rate. concentration of methyl orange: 40mg/l, stir rate: 400rpm, ozone: 8.0mg/l, 980ml/min, initial pH: 10.0.</note>
<note type="content">Fig. 7: The contour lines of decolorization rate from the concentrations of methyl orange and ozone applying 34°C as the reaction temperature.</note>
<note type="content">Table 1: Factors and levels for the 25−1 fractional factorial design</note>
<note type="content">Table 2: The experimental results of the 25−1 fractional factorial design matrix according to the defining relation of I=−ABCDE</note>
<note type="content">Table 3: Estimates of the effects for the 25−1 fractional factorial design with the defining relation of I=−ABCDE by Yates' algorithm</note>
<note type="content">Table 4: Factors and levels for the modified central composite design</note>
<note type="content">Table 5: The experimental data for the empirical model building by the modified central composite design</note>
<note type="content">Table 6: Variance analysis for the quadratic form fit of average decolorization rate</note>
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