The amperometric titration of plasma chloride and urine chloride
Identifieur interne : 003899 ( Istex/Corpus ); précédent : 003898; suivant : 003900The amperometric titration of plasma chloride and urine chloride
Auteurs : Charles W. CarrSource :
- Archives of Biochemistry and Biophysics [ 0003-9861 ] ; 1951.
Abstract
It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 N in nitric acid. Silver nitrate, 0.0100 N, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.
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DOI: 10.1016/0003-9861(51)90009-4
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Carr</name><affiliation><mods:affiliation>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF</idno><date when="1951" year="1951">1951</date><idno type="doi">10.1016/0003-9861(51)90009-4</idno><idno type="url">https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">003899</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main" xml:lang="en">The amperometric titration of plasma chloride and urine chloride</title><author><name sortKey="Carr, Charles W" sort="Carr, Charles W" uniqKey="Carr C" first="Charles W." last="Carr">Charles W. Carr</name><affiliation><mods:affiliation>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Archives of Biochemistry and Biophysics</title><title level="j" type="abbrev">YABBI</title><idno type="ISSN">0003-9861</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1951">1951</date><biblScope unit="volume">34</biblScope><biblScope unit="issue">2</biblScope><biblScope unit="page" from="299">299</biblScope><biblScope unit="page" to="304">304</biblScope></imprint><idno type="ISSN">0003-9861</idno></series><idno type="istex">2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF</idno><idno type="DOI">10.1016/0003-9861(51)90009-4</idno><idno type="PII">0003-9861(51)90009-4</idno><idno type="ArticleID">51900094</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0003-9861</idno></seriesStmt></fileDesc><profileDesc><textClass></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 N in nitric acid. Silver nitrate, 0.0100 N, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.</div></front></TEI><istex><corpusName>elsevier</corpusName><author><json:item><name>Charles W. Carr</name><affiliations><json:string>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</json:string></affiliations></json:item></author><articleId><json:string>51900094</json:string></articleId><language><json:string>eng</json:string></language><abstract>It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 N in nitric acid. Silver nitrate, 0.0100 N, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.</abstract><qualityIndicators><score>3.012</score><pdfVersion>1.3</pdfVersion><pdfPageSize>396.28 x 576 pts</pdfPageSize><refBibsNative>true</refBibsNative><keywordCount>0</keywordCount><abstractCharCount>722</abstractCharCount><pdfWordCount>1572</pdfWordCount><pdfCharCount>9697</pdfCharCount><pdfPageCount>6</pdfPageCount><abstractWordCount>120</abstractWordCount></qualityIndicators><title>The amperometric titration of plasma chloride and urine chloride</title><pii><json:string>0003-9861(51)90009-4</json:string></pii><genre><json:string>research-article</json:string></genre><host><volume>34</volume><pii><json:string>S0003-9861(00)X0669-8</json:string></pii><pages><last>304</last><first>299</first></pages><issn><json:string>0003-9861</json:string></issn><issue>2</issue><genre><json:string>Journal</json:string></genre><language><json:string>unknown</json:string></language><title>Archives of Biochemistry and Biophysics</title><publicationDate>1951</publicationDate></host><publicationDate>1951</publicationDate><copyrightDate>1951</copyrightDate><doi><json:string>10.1016/0003-9861(51)90009-4</json:string></doi><id>2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF</id><fulltext><json:item><original>true</original><mimetype>application/pdf</mimetype><extension>pdf</extension><uri>https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/fulltext/pdf</uri></json:item><json:item><original>true</original><mimetype>text/plain</mimetype><extension>txt</extension><uri>https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/fulltext/txt</uri></json:item><json:item><original>false</original><mimetype>application/zip</mimetype><extension>zip</extension><uri>https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/fulltext/zip</uri></json:item><istex:fulltextTEI uri="https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/fulltext/tei"><teiHeader><fileDesc><titleStmt><title level="a" type="main" xml:lang="en">The amperometric titration of plasma chloride and urine chloride</title></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>ELSEVIER</publisher><availability><p>ELSEVIER</p></availability><date>1951</date></publicationStmt><sourceDesc><biblStruct type="inbook"><analytic><title level="a" type="main" xml:lang="en">The amperometric titration of plasma chloride and urine chloride</title><author><persName><forename type="first">Charles W.</forename><surname>Carr</surname></persName><affiliation>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</affiliation></author></analytic><monogr><title level="j">Archives of Biochemistry and Biophysics</title><title level="j" type="abbrev">YABBI</title><idno type="pISSN">0003-9861</idno><idno type="PII">S0003-9861(00)X0669-8</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1951"></date><biblScope unit="volume">34</biblScope><biblScope unit="issue">2</biblScope><biblScope unit="page" from="299">299</biblScope><biblScope unit="page" to="304">304</biblScope></imprint></monogr><idno type="istex">2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF</idno><idno type="DOI">10.1016/0003-9861(51)90009-4</idno><idno type="PII">0003-9861(51)90009-4</idno><idno type="ArticleID">51900094</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1951</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 N in nitric acid. Silver nitrate, 0.0100 N, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.</p></abstract></profileDesc><revisionDesc><change when="1951-04-18">Received</change><change when="1951">Published</change></revisionDesc></teiHeader></istex:fulltextTEI></fulltext><metadata><istex:metadataXml wicri:clean="Elsevier, elements deleted: tail"><istex:xmlDeclaration>version="1.0" encoding="UTF-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//ES//DTD journal article DTD version 4.5.2//EN//XML" URI="art452.dtd" name="istex:docType"></istex:docType><istex:document><converted-article version="4.5.2" docsubtype="fla" xml:lang="en"><item-info><jid>YABBI</jid><aid>51900094</aid><ce:pii>0003-9861(51)90009-4</ce:pii><ce:doi>10.1016/0003-9861(51)90009-4</ce:doi><ce:copyright type="unknown" year="1951"></ce:copyright></item-info><head><ce:title>The amperometric titration of plasma chloride and urine chloride</ce:title><ce:author-group><ce:author><ce:given-name>Charles W.</ce:given-name><ce:surname>Carr</ce:surname></ce:author><ce:affiliation><ce:textfn>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</ce:textfn></ce:affiliation></ce:author-group><ce:date-received day="18" month="4" year="1951"></ce:date-received><ce:abstract class="author"><ce:section-title>Abstract</ce:section-title><ce:abstract-sec><ce:simple-para view="all" id="simple-para.0010">It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 <ce:italic>N</ce:italic> in nitric acid. Silver nitrate, 0.0100 <ce:italic>N</ce:italic>, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.</ce:simple-para><ce:simple-para view="all" id="simple-para.0015">When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.</ce:simple-para><ce:simple-para view="all" id="simple-para.0020">The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.</ce:simple-para></ce:abstract-sec></ce:abstract></head></converted-article></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>The amperometric titration of plasma chloride and urine chloride</title></titleInfo><titleInfo type="alternative" lang="en" contentType="CDATA"><title>The amperometric titration of plasma chloride and urine chloride</title></titleInfo><name type="personal"><namePart type="given">Charles W.</namePart><namePart type="family">Carr</namePart><affiliation>From the Department of Physiological Chemistry, Medical School, University of Minnesota, Minneapolis, MinnesotaU.S.A.</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="Full-length article"></genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">1951</dateIssued><dateCaptured encoding="w3cdtf">1951-04-18</dateCaptured><copyrightDate encoding="w3cdtf">1951</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm><languageTerm type="code" authority="rfc3066">en</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">It has been shown that the method of Laitinen, Jennings, and Parks for the amperometric titration of chloride can be easily adapted to analyses of plasma (serum) and urine chlorides. For the procedure 1.0-ml. samples are diluted so that the mixture being titrated is 50% in acetone and 0.8 N in nitric acid. Silver nitrate, 0.0100 N, is used as the titrant, and the rotating platinum electrode is used as the indicator electrode. The method is simple, rapid, and as accurate as existing methods.When 0.1-ml. samples are analyzed, the accuracy is decreased a little over that obtained when 1.0-ml. samples are used.The method is not satisfactory for the analysis of chloride in the presence of whole blood or muscle tissue.</abstract><relatedItem type="host"><titleInfo><title>Archives of Biochemistry and Biophysics</title></titleInfo><titleInfo type="abbreviated"><title>YABBI</title></titleInfo><genre type="Journal">journal</genre><originInfo><dateIssued encoding="w3cdtf">195112</dateIssued></originInfo><identifier type="ISSN">0003-9861</identifier><identifier type="PII">S0003-9861(00)X0669-8</identifier><part><date>195112</date><detail type="volume"><number>34</number><caption>vol.</caption></detail><detail type="issue"><number>2</number><caption>no.</caption></detail><extent unit="issue pages"><start>239</start><end>494</end></extent><extent unit="pages"><start>299</start><end>304</end></extent></part></relatedItem><identifier type="istex">2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF</identifier><identifier type="DOI">10.1016/0003-9861(51)90009-4</identifier><identifier type="PII">0003-9861(51)90009-4</identifier><identifier type="ArticleID">51900094</identifier><recordInfo><recordContentSource>ELSEVIER</recordContentSource></recordInfo></mods></metadata><enrichments><istex:refBibTEI uri="https://api.istex.fr/document/2429DE6BB4A4F9FD7C9AE7EF06E2D48328A9F2CF/enrichments/refBib"><teiHeader></teiHeader><text><front></front><body></body><back><listBibl><biblStruct><monogr><author><persName><forename type="first">I</forename><forename type="middle">Ai</forename><surname>Kolthofp</surname></persName></author><author><persName><forename type="first">J</forename><surname>And Lingane</surname></persName></author><author><persName><forename type="first">J</forename></persName></author><imprint><date type="published" when="1941"></date><publisher>Polarography. 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