Determination of galactose and mannose residues in natural galactomannans using a fast and efficient high-performance liquid chromatography/UV detection.
Identifieur interne : 000201 ( Ncbi/Merge ); précédent : 000200; suivant : 000202Determination of galactose and mannose residues in natural galactomannans using a fast and efficient high-performance liquid chromatography/UV detection.
Auteurs : N. Tapie [France] ; C. Malhiac ; N. Hucher ; M. GriselSource :
- Journal of chromatography. A [ 0021-9673 ] ; 2008.
English descriptors
- KwdEn :
- MESH :
- chemical , analysis : Galactose, Mannose.
- chemical , chemistry : Galactans, Mannans, Plant Gums, Polysaccharides.
- chemical , metabolism : Mannans, beta-Mannosidase.
- methods : Chromatography, High Pressure Liquid.
- Reproducibility of Results, Ultraviolet Rays.
Abstract
The present work describes the validation of an easy, fast and efficient precolumn derivatization method for the quantification of oligosides, mannose and galactose obtained by degradation of galactomannans. This work combines an acid hydrolysis and an enzymatic degradation of natural galactomannans with the quantification of released residues by reversed-phase HPLC-UV, the most usual HPLC system in laboratories. In case of enzymatic degradation, mannotetraose has been detected and quantified for the first time, and an application to the evaluation of the galactosyl distribution in galactomannans is proposed. After an acidic hydrolysis, this method also allowed to obtain the mannose/galactose (M/G) ratio.
DOI: 10.1016/j.chroma.2007.12.027
PubMed: 18177885
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Tapie</name><affiliation wicri:level="4"><nlm:affiliation>Unité de Recherche en Chimie Organique et Macromoléculaire, URCOM, EA 3221, Université du Havre, Le Havre cedex, France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>Unité de Recherche en Chimie Organique et Macromoléculaire, URCOM, EA 3221, Université du Havre, Le Havre cedex</wicri:regionArea><wicri:noRegion>Le Havre cedex</wicri:noRegion><orgName type="university">Université du Havre</orgName><placeName><settlement type="city">Le Havre</settlement><region type="region" nuts="2">Région Normandie</region><region type="old region" nuts="2">Haute-Normandie</region></placeName></affiliation></author><author><name sortKey="Malhiac, C" sort="Malhiac, C" uniqKey="Malhiac C" first="C" last="Malhiac">C. Malhiac</name></author><author><name sortKey="Hucher, N" sort="Hucher, N" uniqKey="Hucher N" first="N" last="Hucher">N. 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Hucher</name></author><author><name sortKey="Grisel, M" sort="Grisel, M" uniqKey="Grisel M" first="M" last="Grisel">M. Grisel</name></author></analytic><series><title level="j">Journal of chromatography. A</title><idno type="ISSN">0021-9673</idno><imprint><date when="2008" type="published">2008</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Chromatography, High Pressure Liquid (methods)</term><term>Galactans (chemistry)</term><term>Galactose (analysis)</term><term>Mannans (chemistry)</term><term>Mannans (metabolism)</term><term>Mannose (analysis)</term><term>Plant Gums (chemistry)</term><term>Polysaccharides (chemistry)</term><term>Reproducibility of Results</term><term>Ultraviolet Rays</term><term>beta-Mannosidase (metabolism)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Galactose</term><term>Mannose</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Galactans</term><term>Mannans</term><term>Plant Gums</term><term>Polysaccharides</term></keywords><keywords scheme="MESH" type="chemical" qualifier="metabolism" xml:lang="en"><term>Mannans</term><term>beta-Mannosidase</term></keywords><keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Chromatography, High Pressure Liquid</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Reproducibility of Results</term><term>Ultraviolet Rays</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The present work describes the validation of an easy, fast and efficient precolumn derivatization method for the quantification of oligosides, mannose and galactose obtained by degradation of galactomannans. This work combines an acid hydrolysis and an enzymatic degradation of natural galactomannans with the quantification of released residues by reversed-phase HPLC-UV, the most usual HPLC system in laboratories. In case of enzymatic degradation, mannotetraose has been detected and quantified for the first time, and an application to the evaluation of the galactosyl distribution in galactomannans is proposed. After an acidic hydrolysis, this method also allowed to obtain the mannose/galactose (M/G) ratio.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">18177885</PMID><DateCreated><Year>2008</Year><Month>2</Month><Day>4</Day></DateCreated><DateCompleted><Year>2008</Year><Month>03</Month><Day>25</Day></DateCompleted><DateRevised><Year>2015</Year><Month>11</Month><Day>19</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Print">0021-9673</ISSN><JournalIssue CitedMedium="Print"><Volume>1181</Volume><Issue>1-2</Issue><PubDate><Year>2008</Year><Month>Feb</Month><Day>15</Day></PubDate></JournalIssue><Title>Journal of chromatography. A</Title><ISOAbbreviation>J Chromatogr A</ISOAbbreviation></Journal><ArticleTitle>Determination of galactose and mannose residues in natural galactomannans using a fast and efficient high-performance liquid chromatography/UV detection.</ArticleTitle><Pagination><MedlinePgn>45-50</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.chroma.2007.12.027</ELocationID><Abstract><AbstractText>The present work describes the validation of an easy, fast and efficient precolumn derivatization method for the quantification of oligosides, mannose and galactose obtained by degradation of galactomannans. This work combines an acid hydrolysis and an enzymatic degradation of natural galactomannans with the quantification of released residues by reversed-phase HPLC-UV, the most usual HPLC system in laboratories. In case of enzymatic degradation, mannotetraose has been detected and quantified for the first time, and an application to the evaluation of the galactosyl distribution in galactomannans is proposed. After an acidic hydrolysis, this method also allowed to obtain the mannose/galactose (M/G) ratio.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Tapie</LastName><ForeName>N</ForeName><Initials>N</Initials><AffiliationInfo><Affiliation>Unité de Recherche en Chimie Organique et Macromoléculaire, URCOM, EA 3221, Université du Havre, Le Havre cedex, France.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Malhiac</LastName><ForeName>C</ForeName><Initials>C</Initials></Author><Author ValidYN="Y"><LastName>Hucher</LastName><ForeName>N</ForeName><Initials>N</Initials></Author><Author ValidYN="Y"><LastName>Grisel</LastName><ForeName>M</ForeName><Initials>M</Initials></Author></AuthorList><Language>ENG</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D023361">Validation Studies</PublicationType></PublicationTypeList><ArticleDate 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MajorTopicYN="N">Galactose</DescriptorName><QualifierName UI="Q000032" MajorTopicYN="Y">analysis</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D008351" MajorTopicYN="N">Mannans</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName><QualifierName UI="Q000378" MajorTopicYN="N">metabolism</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D008358" MajorTopicYN="N">Mannose</DescriptorName><QualifierName UI="Q000032" MajorTopicYN="Y">analysis</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D053149" MajorTopicYN="N">Plant Gums</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D011134" MajorTopicYN="N">Polysaccharides</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D015203" MajorTopicYN="N">Reproducibility of Results</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D014466" MajorTopicYN="N">Ultraviolet Rays</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D044902" MajorTopicYN="N">beta-Mannosidase</DescriptorName><QualifierName UI="Q000378" MajorTopicYN="N">metabolism</QualifierName></MeshHeading></MeshHeadingList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2007</Year><Month>7</Month><Day>31</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2007</Year><Month>12</Month><Day>5</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2007</Year><Month>12</Month><Day>12</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2008</Year><Month>1</Month><Day>8</Day><Hour>9</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2008</Year><Month>3</Month><Day>26</Day><Hour>9</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2008</Year><Month>1</Month><Day>8</Day><Hour>9</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">18177885</ArticleId><ArticleId IdType="pii">S0021-9673(07)02186-3</ArticleId><ArticleId IdType="doi">10.1016/j.chroma.2007.12.027</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>France</li></country><region><li>Haute-Normandie</li><li>Région Normandie</li></region><settlement><li>Le Havre</li></settlement><orgName><li>Université du Havre</li></orgName></list><tree><noCountry><name sortKey="Grisel, M" sort="Grisel, M" uniqKey="Grisel M" first="M" last="Grisel">M. Grisel</name><name sortKey="Hucher, N" sort="Hucher, N" uniqKey="Hucher N" first="N" last="Hucher">N. Hucher</name><name sortKey="Malhiac, C" sort="Malhiac, C" uniqKey="Malhiac C" first="C" last="Malhiac">C. Malhiac</name></noCountry><country name="France"><region name="Région Normandie"><name sortKey="Tapie, N" sort="Tapie, N" uniqKey="Tapie N" first="N" last="Tapie">N. Tapie</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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