Determination of Thiocyanate in Plasma by Ion Chromatography and Ultraviolet Detection
Identifieur interne : 000F47 ( Main/Merge ); précédent : 000F46; suivant : 000F48Determination of Thiocyanate in Plasma by Ion Chromatography and Ultraviolet Detection
Auteurs : Elodie Saussereau [France] ; Jean-Pierre Goullé [France] ; Christian Lacroix [France]Source :
- Journal of Analytical Toxicology [ 0146-4760 ] ; 2007-09.
Abstract
A specific and sensitive rapid high-pedormance liquid chromatographic method has been developed for determination of thiocyanate (SCN-) in plasma. This method is based on anion exchange chromatography after a simple ultrafiltration of plasma diluted in water. The detection of SCN- is carried out in ultraviolet (λ = 210 nm). The proposed method is linear in the range 1–30 mg/L. Intra-assay and interassay accuracy and precision were maintained within the designated limit (< 20%). The total recovery of SCN- varied between 97 and 103.9%. The method described should be useful for clinical medicine. Moreover, this method was applied to the analysis of SCN- plasma in deceased subjects, within the context of fire, and could be of interest in forensic science as a useful additional measurement tool for cyanide determination in blood.
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DOI: 10.1093/jat/31.7.383
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<front><div type="abstract">A specific and sensitive rapid high-pedormance liquid chromatographic method has been developed for determination of thiocyanate (SCN-) in plasma. This method is based on anion exchange chromatography after a simple ultrafiltration of plasma diluted in water. The detection of SCN- is carried out in ultraviolet (λ = 210 nm). The proposed method is linear in the range 1–30 mg/L. Intra-assay and interassay accuracy and precision were maintained within the designated limit (< 20%). The total recovery of SCN- varied between 97 and 103.9%. The method described should be useful for clinical medicine. Moreover, this method was applied to the analysis of SCN- plasma in deceased subjects, within the context of fire, and could be of interest in forensic science as a useful additional measurement tool for cyanide determination in blood.</div>
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