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Continuous hydrothermal synthesis of inorganic nanopowders in supercritical water : Towards a better control of the process

Identifieur interne : 000327 ( PascalFrancis/Corpus ); précédent : 000326; suivant : 000328

Continuous hydrothermal synthesis of inorganic nanopowders in supercritical water : Towards a better control of the process

Auteurs : A. Aimable ; H. Muhr ; C. Gentric ; F. Bernard ; F. Le Cras ; D. Aymes

Source :

RBID : Pascal:09-0182775

Descripteurs français

English descriptors

Abstract

A hydrothermal synthesis process working in supercritical conditions (T>374 °C, P>22 MPa) and in a continuous mode has been developed for inorganic nanopowder synthesis. This paper presents a review of the past 5 years of research conducted on this process. Numerous materials (oxides: ZrO2, TiO2, Fe2O3..., ferrites: Fe2CoO4..., or BaZrO3) were obtained with specific features. Some technical issues have been solved, that are presented here. Heat transfer was studied, leading to a more efficient design of the reactor. Future developments have been examined through process engineering, in which our group is engaged, especially through CFD modelling.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

pA  
A01 01  1    @0 0032-5910
A02 01      @0 POTEBX
A03   1    @0 Powder technol.
A05       @2 190
A06       @2 1-2
A08 01  1  ENG  @1 Continuous hydrothermal synthesis of inorganic nanopowders in supercritical water : Towards a better control of the process
A09 01  1  ENG  @1 Selection of Papers from the Symposium Powder Science and Technology - Powders and Sintered Material, STP-PMF 2007, Ecole des Mines d'Albi, 23-25 May 2007
A11 01  1    @1 AIMABLE (A.)
A11 02  1    @1 MUHR (H.)
A11 03  1    @1 GENTRIC (C.)
A11 04  1    @1 BERNARD (F.)
A11 05  1    @1 LE CRAS (F.)
A11 06  1    @1 AYMES (D.)
A12 01  1    @1 DODDS (John) @9 ed.
A14 01      @1 Institut Camot de Bourgogne, UMR 5209 CNRS, Université de Bourgogne, 9 avenue Alain Savary, BP 47870 @2 21078 Dijon @3 FRA @Z 1 aut. @Z 4 aut. @Z 6 aut.
A14 02      @1 LSGC UPR 6811 CNRS, Nancy Université, rue Grandville, BP 20451 @2 54001 Nancy @3 FRA @Z 1 aut. @Z 2 aut. @Z 3 aut.
A14 03      @1 CEA, DRT/DTNM/LCE, 17 rue des Martyrs @2 38054 Grenoble @3 FRA @Z 1 aut. @Z 5 aut.
A15 01      @1 UMR-CNRS-EMAC 2392 Ecole des Mines d'Albi, Campus Jarlard @2 81013 Albi @3 FRA @Z 1 aut.
A20       @1 99-106
A21       @1 2009
A23 01      @0 ENG
A43 01      @1 INIST @2 13653 @5 354000187051530190
A44       @0 0000 @1 © 2009 INIST-CNRS. All rights reserved.
A45       @0 26 ref.
A47 01  1    @0 09-0182775
A60       @1 P @2 C
A61       @0 A
A64 01  1    @0 Powder technology
A66 01      @0 CHE
C01 01    ENG  @0 A hydrothermal synthesis process working in supercritical conditions (T>374 °C, P>22 MPa) and in a continuous mode has been developed for inorganic nanopowder synthesis. This paper presents a review of the past 5 years of research conducted on this process. Numerous materials (oxides: ZrO2, TiO2, Fe2O3..., ferrites: Fe2CoO4..., or BaZrO3) were obtained with specific features. Some technical issues have been solved, that are presented here. Heat transfer was studied, leading to a more efficient design of the reactor. Future developments have been examined through process engineering, in which our group is engaged, especially through CFD modelling.
C02 01  X    @0 001D07Q07
C02 02  X    @0 001D07G
C02 03  X    @0 001D07H
C03 01  X  FRE  @0 Etat supercritique @5 01
C03 01  X  ENG  @0 Supercritical state @5 01
C03 01  X  SPA  @0 Estado supercrítico @5 01
C03 02  X  FRE  @0 Oxyde de titane @5 02
C03 02  X  ENG  @0 Titanium oxide @5 02
C03 02  X  SPA  @0 Titanio óxido @5 02
C03 03  X  FRE  @0 Transfert chaleur @5 03
C03 03  X  ENG  @0 Heat transfer @5 03
C03 03  X  SPA  @0 Transferencia térmica @5 03
C03 04  X  FRE  @0 Conception @5 04
C03 04  X  ENG  @0 Design @5 04
C03 04  X  SPA  @0 Diseño @5 04
C03 05  X  FRE  @0 Réacteur @5 05
C03 05  X  ENG  @0 Reactor @5 05
C03 05  X  SPA  @0 Reactor @5 05
C03 06  X  FRE  @0 Génie des procédés @5 06
C03 06  X  ENG  @0 Process engineering @5 06
C03 06  X  SPA  @0 Ingeniería procesos @5 06
C03 07  X  FRE  @0 Mécanique fluide numérique @5 07
C03 07  X  ENG  @0 Computational fluid dynamics @5 07
C03 07  X  SPA  @0 Mecánica fluido numérica @5 07
C03 08  X  FRE  @0 Modélisation @5 08
C03 08  X  ENG  @0 Modeling @5 08
C03 08  X  SPA  @0 Modelización @5 08
C03 09  X  FRE  @0 Nanoparticule @5 09
C03 09  X  ENG  @0 Nanoparticle @5 09
C03 09  X  SPA  @0 Nanopartícula @5 09
N21       @1 131
N44 01      @1 OTO
N82       @1 OTO
pR  
A30 01  1  ENG  @1 Symposium Powder Science and Technology - Powders and Sintered Material, STP-PMF 2007 @3 Albi FRA @4 2007-05-23

Format Inist (serveur)

NO : PASCAL 09-0182775 INIST
ET : Continuous hydrothermal synthesis of inorganic nanopowders in supercritical water : Towards a better control of the process
AU : AIMABLE (A.); MUHR (H.); GENTRIC (C.); BERNARD (F.); LE CRAS (F.); AYMES (D.); DODDS (John)
AF : Institut Camot de Bourgogne, UMR 5209 CNRS, Université de Bourgogne, 9 avenue Alain Savary, BP 47870/21078 Dijon/France (1 aut., 4 aut., 6 aut.); LSGC UPR 6811 CNRS, Nancy Université, rue Grandville, BP 20451/54001 Nancy/France (1 aut., 2 aut., 3 aut.); CEA, DRT/DTNM/LCE, 17 rue des Martyrs/38054 Grenoble/France (1 aut., 5 aut.); UMR-CNRS-EMAC 2392 Ecole des Mines d'Albi, Campus Jarlard/81013 Albi/France (1 aut.)
DT : Publication en série; Congrès; Niveau analytique
SO : Powder technology; ISSN 0032-5910; Coden POTEBX; Suisse; Da. 2009; Vol. 190; No. 1-2; Pp. 99-106; Bibl. 26 ref.
LA : Anglais
EA : A hydrothermal synthesis process working in supercritical conditions (T>374 °C, P>22 MPa) and in a continuous mode has been developed for inorganic nanopowder synthesis. This paper presents a review of the past 5 years of research conducted on this process. Numerous materials (oxides: ZrO2, TiO2, Fe2O3..., ferrites: Fe2CoO4..., or BaZrO3) were obtained with specific features. Some technical issues have been solved, that are presented here. Heat transfer was studied, leading to a more efficient design of the reactor. Future developments have been examined through process engineering, in which our group is engaged, especially through CFD modelling.
CC : 001D07Q07; 001D07G; 001D07H
FD : Etat supercritique; Oxyde de titane; Transfert chaleur; Conception; Réacteur; Génie des procédés; Mécanique fluide numérique; Modélisation; Nanoparticule
ED : Supercritical state; Titanium oxide; Heat transfer; Design; Reactor; Process engineering; Computational fluid dynamics; Modeling; Nanoparticle
SD : Estado supercrítico; Titanio óxido; Transferencia térmica; Diseño; Reactor; Ingeniería procesos; Mecánica fluido numérica; Modelización; Nanopartícula
LO : INIST-13653.354000187051530190
ID : 09-0182775

Links to Exploration step

Pascal:09-0182775

Le document en format XML

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<sub>2</sub>
, TiO
<sub>2</sub>
, Fe
<sub>2</sub>
O
<sub>3</sub>
..., ferrites: Fe
<sub>2</sub>
CoO
<sub>4</sub>
..., or BaZrO
<sub>3</sub>
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</fC02>
<fC03 i1="01" i2="X" l="FRE">
<s0>Etat supercritique</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG">
<s0>Supercritical state</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA">
<s0>Estado supercrítico</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE">
<s0>Oxyde de titane</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG">
<s0>Titanium oxide</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA">
<s0>Titanio óxido</s0>
<s5>02</s5>
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<fC03 i1="03" i2="X" l="FRE">
<s0>Transfert chaleur</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG">
<s0>Heat transfer</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA">
<s0>Transferencia térmica</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE">
<s0>Conception</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG">
<s0>Design</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA">
<s0>Diseño</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE">
<s0>Réacteur</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG">
<s0>Reactor</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA">
<s0>Reactor</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE">
<s0>Génie des procédés</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG">
<s0>Process engineering</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA">
<s0>Ingeniería procesos</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE">
<s0>Mécanique fluide numérique</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG">
<s0>Computational fluid dynamics</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA">
<s0>Mecánica fluido numérica</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE">
<s0>Modélisation</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG">
<s0>Modeling</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA">
<s0>Modelización</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE">
<s0>Nanoparticule</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG">
<s0>Nanoparticle</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA">
<s0>Nanopartícula</s0>
<s5>09</s5>
</fC03>
<fN21>
<s1>131</s1>
</fN21>
<fN44 i1="01">
<s1>OTO</s1>
</fN44>
<fN82>
<s1>OTO</s1>
</fN82>
</pA>
<pR>
<fA30 i1="01" i2="1" l="ENG">
<s1>Symposium Powder Science and Technology - Powders and Sintered Material, STP-PMF 2007</s1>
<s3>Albi FRA</s3>
<s4>2007-05-23</s4>
</fA30>
</pR>
</standard>
<server>
<NO>PASCAL 09-0182775 INIST</NO>
<ET>Continuous hydrothermal synthesis of inorganic nanopowders in supercritical water : Towards a better control of the process</ET>
<AU>AIMABLE (A.); MUHR (H.); GENTRIC (C.); BERNARD (F.); LE CRAS (F.); AYMES (D.); DODDS (John)</AU>
<AF>Institut Camot de Bourgogne, UMR 5209 CNRS, Université de Bourgogne, 9 avenue Alain Savary, BP 47870/21078 Dijon/France (1 aut., 4 aut., 6 aut.); LSGC UPR 6811 CNRS, Nancy Université, rue Grandville, BP 20451/54001 Nancy/France (1 aut., 2 aut., 3 aut.); CEA, DRT/DTNM/LCE, 17 rue des Martyrs/38054 Grenoble/France (1 aut., 5 aut.); UMR-CNRS-EMAC 2392 Ecole des Mines d'Albi, Campus Jarlard/81013 Albi/France (1 aut.)</AF>
<DT>Publication en série; Congrès; Niveau analytique</DT>
<SO>Powder technology; ISSN 0032-5910; Coden POTEBX; Suisse; Da. 2009; Vol. 190; No. 1-2; Pp. 99-106; Bibl. 26 ref.</SO>
<LA>Anglais</LA>
<EA>A hydrothermal synthesis process working in supercritical conditions (T>374 °C, P>22 MPa) and in a continuous mode has been developed for inorganic nanopowder synthesis. This paper presents a review of the past 5 years of research conducted on this process. Numerous materials (oxides: ZrO
<sub>2</sub>
, TiO
<sub>2</sub>
, Fe
<sub>2</sub>
O
<sub>3</sub>
..., ferrites: Fe
<sub>2</sub>
CoO
<sub>4</sub>
..., or BaZrO
<sub>3</sub>
) were obtained with specific features. Some technical issues have been solved, that are presented here. Heat transfer was studied, leading to a more efficient design of the reactor. Future developments have been examined through process engineering, in which our group is engaged, especially through CFD modelling.</EA>
<CC>001D07Q07; 001D07G; 001D07H</CC>
<FD>Etat supercritique; Oxyde de titane; Transfert chaleur; Conception; Réacteur; Génie des procédés; Mécanique fluide numérique; Modélisation; Nanoparticule</FD>
<ED>Supercritical state; Titanium oxide; Heat transfer; Design; Reactor; Process engineering; Computational fluid dynamics; Modeling; Nanoparticle</ED>
<SD>Estado supercrítico; Titanio óxido; Transferencia térmica; Diseño; Reactor; Ingeniería procesos; Mecánica fluido numérica; Modelización; Nanopartícula</SD>
<LO>INIST-13653.354000187051530190</LO>
<ID>09-0182775</ID>
</server>
</inist>
</record>

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