LrgpV1, PascalFrancis, Corpus, bibRecord, 000005

Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies

Identifieur interne : 000005 ( PascalFrancis/Corpus ); précédent : 000004; suivant : 000006

Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies

Auteurs : SONGLIN NIU ; Raphaël Schneider ; Loïc Vidal ; Samar Hajjar-Garreau ; Lavinia Balan

Source :

Journal of nanoparticle research [ 1388-0764 ] ; 2014.

RBID : Pascal:14-0272787

Descripteurs français

Pascal (Inist)
- Fonctionnalisation, Argent, Nanoparticule, Nanomatériau, Thiol, Chromophore, Nanostructure, Plan expérience, Diode électroluminescente, Eclairement, Interaction forte, Ligand, Polymérisation photochimique, Monomère, Nanocomposite, Résonance plasmon surface, 8107B, 6865, 8560J, 8560.

English descriptors

KwdEn :
- Chromophores, Experimental design, Functionalization, Illumination, Ligands, Light emitting diodes, Monomers, Nanocomposites, Nanoparticles, Nanostructured materials, Nanostructures, Photopolymerization, Silver, Strong interactions, Surface plasmon resonance, Thiols.

Abstract

In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag⁺ ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

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A03		`1`		`@0 J. nanopart. res.`
A05				`@2 16`
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A08	`01`	`1`	`ENG`	`@1 Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies`
A11	`01`	`1`		`@1 SONGLIN NIU`
A11	`02`	`1`		`@1 SCHNEIDER (Raphaël)`
A11	`03`	`1`		`@1 VIDAL (Loïc)`
A11	`04`	`1`		`@1 HAJJAR-GARREAU (Samar)`
A11	`05`	`1`		`@1 BALAN (Lavinia)`
A14	`01`			`@1 Institut de Sciences des Matériaux de Mulhouse, CNRS UMR 7361, Université de Haute Alsace, 15 rue Jean Starcky @2 68057 Mulhouse @3 FRA @Z 1 aut. @Z 3 aut. @Z 4 aut. @Z 5 aut.`
A14	`02`			`@1 Laboratoire Reactions et Génie des Procédés (LRGP), CNRS UMR 7274, Université de Lorraine, 1 rue Grandville, BP 20451 @2 54001 Nancy @3 FRA @Z 2 aut.`
A20				`@2 2620.1-2620.11`
A21				`@1 2014`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 28202 @5 354000504560870380`
A44				`@0 0000 @1 © 2014 INIST-CNRS. All rights reserved.`
A45				`@0 1 p.1/4`
A47	`01`	`1`		`@0 14-0272787`
A60				`@1 P @3 PR`
A61				`@0 A`
A64	`01`	`1`		`@0 Journal of nanoparticle research`
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C01	`01`		`ENG`	@0 In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag⁺ ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.
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C03	`01`	`X`	`FRE`	`@0 Fonctionnalisation @5 01`
C03	`01`	`X`	`ENG`	`@0 Functionalization @5 01`
C03	`01`	`X`	`SPA`	`@0 Funciónalización @5 01`
C03	`02`	`3`	`FRE`	`@0 Argent @2 NC @5 02`
C03	`02`	`3`	`ENG`	`@0 Silver @2 NC @5 02`
C03	`03`	`3`	`FRE`	`@0 Nanoparticule @5 03`
C03	`03`	`3`	`ENG`	`@0 Nanoparticles @5 03`
C03	`04`	`3`	`FRE`	`@0 Nanomatériau @5 04`
C03	`04`	`3`	`ENG`	`@0 Nanostructured materials @5 04`
C03	`05`	`3`	`FRE`	`@0 Thiol @5 05`
C03	`05`	`3`	`ENG`	`@0 Thiols @5 05`
C03	`06`	`3`	`FRE`	`@0 Chromophore @5 06`
C03	`06`	`3`	`ENG`	`@0 Chromophores @5 06`
C03	`07`	`3`	`FRE`	`@0 Nanostructure @5 07`
C03	`07`	`3`	`ENG`	`@0 Nanostructures @5 07`
C03	`08`	`3`	`FRE`	`@0 Plan expérience @5 08`
C03	`08`	`3`	`ENG`	`@0 Experimental design @5 08`
C03	`09`	`3`	`FRE`	`@0 Diode électroluminescente @5 09`
C03	`09`	`3`	`ENG`	`@0 Light emitting diodes @5 09`
C03	`10`	`3`	`FRE`	`@0 Eclairement @5 10`
C03	`10`	`3`	`ENG`	`@0 Illumination @5 10`
C03	`11`	`3`	`FRE`	`@0 Interaction forte @5 11`
C03	`11`	`3`	`ENG`	`@0 Strong interactions @5 11`
C03	`12`	`3`	`FRE`	`@0 Ligand @5 12`
C03	`12`	`3`	`ENG`	`@0 Ligands @5 12`
C03	`13`	`3`	`FRE`	`@0 Polymérisation photochimique @5 13`
C03	`13`	`3`	`ENG`	`@0 Photopolymerization @5 13`
C03	`14`	`3`	`FRE`	`@0 Monomère @5 14`
C03	`14`	`3`	`ENG`	`@0 Monomers @5 14`
C03	`15`	`3`	`FRE`	`@0 Nanocomposite @5 29`
C03	`15`	`3`	`ENG`	`@0 Nanocomposites @5 29`
C03	`16`	`3`	`FRE`	`@0 Résonance plasmon surface @5 30`
C03	`16`	`3`	`ENG`	`@0 Surface plasmon resonance @5 30`
C03	`17`	`3`	`FRE`	`@0 8107B @4 INC @5 71`
C03	`18`	`3`	`FRE`	`@0 6865 @4 INC @5 72`
C03	`19`	`3`	`FRE`	`@0 8560J @4 INC @5 73`
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N21				`@1 342`
N44	`01`			`@1 OTO`
N82				`@1 OTO`

Format Inist (serveur)

NO :	PASCAL 14-0272787 INIST
ET :	Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies
AU :	SONGLIN NIU; SCHNEIDER (Raphaël); VIDAL (Loïc); HAJJAR-GARREAU (Samar); BALAN (Lavinia)
AF :	Institut de Sciences des Matériaux de Mulhouse, CNRS UMR 7361, Université de Haute Alsace, 15 rue Jean Starcky/68057 Mulhouse/France (1 aut., 3 aut., 4 aut., 5 aut.); Laboratoire Reactions et Génie des Procédés (LRGP), CNRS UMR 7274, Université de Lorraine, 1 rue Grandville, BP 20451/54001 Nancy/France (2 aut.)
DT :	Publication en série; Papier de recherche; Niveau analytique
SO :	Journal of nanoparticle research; ISSN 1388-0764; Pays-Bas; Da. 2014; Vol. 16; No. 9; 2620.1-2620.11; Bibl. 1 p.1/4
LA :	Anglais
EA :	In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag⁺ ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.
CC :	001B80A07B; 001B60H65; 001D03F15
FD :	Fonctionnalisation; Argent; Nanoparticule; Nanomatériau; Thiol; Chromophore; Nanostructure; Plan expérience; Diode électroluminescente; Eclairement; Interaction forte; Ligand; Polymérisation photochimique; Monomère; Nanocomposite; Résonance plasmon surface; 8107B; 6865; 8560J; 8560
ED :	Functionalization; Silver; Nanoparticles; Nanostructured materials; Thiols; Chromophores; Nanostructures; Experimental design; Light emitting diodes; Illumination; Strong interactions; Ligands; Photopolymerization; Monomers; Nanocomposites; Surface plasmon resonance
SD :	Funciónalización
LO :	INIST-28202.354000504560870380
ID :	14-0272787

Links to Exploration step

Pascal:14-0272787

Le document en format XML

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<front><div type="abstract" xml:lang="en">In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag<sup>+</sup>
 ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.</div>
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<fC01 i1="01" l="ENG"><s0>In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag<sup>+</sup>
 ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.</s0>
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<fC03 i1="03" i2="3" l="ENG"><s0>Nanoparticles</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Nanomatériau</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Nanostructured materials</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Thiol</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Thiols</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Chromophore</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG"><s0>Chromophores</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Nanostructure</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Nanostructures</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Plan expérience</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Experimental design</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Diode électroluminescente</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>Light emitting diodes</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Eclairement</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Illumination</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Interaction forte</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Strong interactions</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Ligand</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Ligands</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Polymérisation photochimique</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>Photopolymerization</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Monomère</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Monomers</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>Nanocomposite</s0>
<s5>29</s5>
</fC03>
<fC03 i1="15" i2="3" l="ENG"><s0>Nanocomposites</s0>
<s5>29</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE"><s0>Résonance plasmon surface</s0>
<s5>30</s5>
</fC03>
<fC03 i1="16" i2="3" l="ENG"><s0>Surface plasmon resonance</s0>
<s5>30</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE"><s0>8107B</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE"><s0>6865</s0>
<s4>INC</s4>
<s5>72</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE"><s0>8560J</s0>
<s4>INC</s4>
<s5>73</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>8560</s0>
<s4>INC</s4>
<s5>74</s5>
</fC03>
<fN21><s1>342</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
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<server><NO>PASCAL 14-0272787 INIST</NO>
<ET>Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies</ET>
<AU>SONGLIN NIU; SCHNEIDER (Raphaël); VIDAL (Loïc); HAJJAR-GARREAU (Samar); BALAN (Lavinia)</AU>
<AF>Institut de Sciences des Matériaux de Mulhouse, CNRS UMR 7361, Université de Haute Alsace, 15 rue Jean Starcky/68057 Mulhouse/France (1 aut., 3 aut., 4 aut., 5 aut.); Laboratoire Reactions et Génie des Procédés (LRGP), CNRS UMR 7274, Université de Lorraine, 1 rue Grandville, BP 20451/54001 Nancy/France (2 aut.)</AF>
<DT>Publication en série; Papier de recherche; Niveau analytique</DT>
<SO>Journal of nanoparticle research; ISSN 1388-0764; Pays-Bas; Da. 2014; Vol. 16; No. 9; 2620.1-2620.11; Bibl. 1 p.1/4</SO>
<LA>Anglais</LA>
<EA>In this study, silver nanoparticles (Ag NPs) were generated, functionalized, and stabilized using a one-step photochemical approach that does not require more than few minutes with a low power near UV LED source. A series of thiol-functionalized thioxanthone (TX) derivatives were prepared and used for the photoinduced synthesis of Ag NPs and their surface functionalization and stabilization. Upon illumination, Ag<sup>+</sup>
 ions are reduced by free radicals generated through an oxidoreductive process occurring between excited TX groups and N-methyldiethanolamine. This process generates monodispersed silver nanoparticles with an average diameter about 2-7 nm depending on the TX derivative used. Due to the strong interaction between Ag atoms and thiol groups of the ligands, AgNPs are capped in situ by TX derivatives and exhibit remarkable stability in solution. Subsequent studies carried out on silver NPs/TX nanoassemblies (designed as AgNPs@S-TX) demonstrated their potentials in free radical photopolymerization of acrylate monomers.</EA>
<CC>001B80A07B; 001B60H65; 001D03F15</CC>
<FD>Fonctionnalisation; Argent; Nanoparticule; Nanomatériau; Thiol; Chromophore; Nanostructure; Plan expérience; Diode électroluminescente; Eclairement; Interaction forte; Ligand; Polymérisation photochimique; Monomère; Nanocomposite; Résonance plasmon surface; 8107B; 6865; 8560J; 8560</FD>
<ED>Functionalization; Silver; Nanoparticles; Nanostructured materials; Thiols; Chromophores; Nanostructures; Experimental design; Light emitting diodes; Illumination; Strong interactions; Ligands; Photopolymerization; Monomers; Nanocomposites; Surface plasmon resonance</ED>
<SD>Funciónalización</SD>
<LO>INIST-28202.354000504560870380</LO>
<ID>14-0272787</ID>
</server>
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Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies

Light-assisted synthesis and functionalization of silver nanoparticles with thiol derivative thioxanthones: new insights into the engineering of metal/chromophore nanoassemblies

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