LrgpV1, PascalFrancis, Checkpoint, bibRecord, 000201

Development of a new method for investigating the mechanisms of solid particle dissolution in nitric acid media: Millifluidic study using fluorescent indicators

Identifieur interne : 000201 ( PascalFrancis/Checkpoint ); précédent : 000200; suivant : 000202

Development of a new method for investigating the mechanisms of solid particle dissolution in nitric acid media: Millifluidic study using fluorescent indicators

Auteurs : Céline Delwaulle [France] ; Alastair Magnaldo [France] ; Andrea Salvatores [France] ; Eric Schaer [France] ; Jean-Léon Houzelot [France] ; Benjamin Rodier [France] ; Emilie Bosse [France]

Source :

Chemical engineering journal : (1996) [ 1385-8947 ] ; 2011.

RBID : Pascal:11-0488242

Descripteurs français

Pascal (Inist)
- Particule solide, Dissolution, Indicateur, Recyclage, Déchet radioactif, Découpage, Combustible, Modélisation, Optimisation, Interface liquide solide, Réacteur, Surveillance, Microscopie confocale, pH, Qualification, In situ, Hydrodynamique, Cinétique, Cartographie, Bulle, Miniaturisation.
Wicri :
- topic : Déchet radioactif, Combustible, Cartographie.

English descriptors

KwdEn :
- Bubble, Cartography, Confocal microscopy, Cutting, Dissolution, Fuel, Hydrodynamics, In situ, Indicator, Kinetics, Liquid solid interface, Miniaturization, Modeling, Optimization, Qualification, Radioactive waste, Reactor, Recycling, Solid particle, Surveillance, pH.

Abstract

A key step in existing industrial recycling processes for spent nuclear fuel, after cutting up the spent fuel assemblies, is the continuous dissolution of uranium dioxide in a dissolver containing concentrated nitric acid. The purpose of this study is to enhance our understanding of the phenomena governing the oxide behavior during dissolution, and to acquire new experimental data suitable for modeling and optimizing spent fuel dissolution. The approach adopted involved small scale experiments, which are indispensable for observing, understanding and modeling the phenomena occurring at the solid/liquid interface which control the dissolution reaction. A millifluidic reactor of about 1 mL was developed for the continuous dissolution of millimeter or submillimeter solid particles in a nitric acid stream. New experimental and analytical monitoring techniques were used (observation at the interface by confocal microscopy and epifluorescence, tracking of the species involved, pH monitoring at the interface by fluorometry). Qualification and experimental implementation of these techniques were first conducted on a nonradioactive surrogate, copper. These observations were used to better understand and quantify continuously and in situ the material dissolution mechanisms and the pH variation at the interface, as well as providing data on the behavior of the off-gases. Intermediate species favorable to the reaction were identified, and made it possible to quantify the coupling between hydrodynamics and dissolution kinetics. We were also able to obtain a pH map of the reaction interface, which is very difficult to implement for this type of reaction in corrosive media.

Affiliations:

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to stream PascalFrancis, to step Corpus: 000168
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Pascal:11-0488242

Le document en format XML

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<front><div type="abstract" xml:lang="en">A key step in existing industrial recycling processes for spent nuclear fuel, after cutting up the spent fuel assemblies, is the continuous dissolution of uranium dioxide in a dissolver containing concentrated nitric acid. The purpose of this study is to enhance our understanding of the phenomena governing the oxide behavior during dissolution, and to acquire new experimental data suitable for modeling and optimizing spent fuel dissolution. The approach adopted involved small scale experiments, which are indispensable for observing, understanding and modeling the phenomena occurring at the solid/liquid interface which control the dissolution reaction. A millifluidic reactor of about 1 mL was developed for the continuous dissolution of millimeter or submillimeter solid particles in a nitric acid stream. New experimental and analytical monitoring techniques were used (observation at the interface by confocal microscopy and epifluorescence, tracking of the species involved, pH monitoring at the interface by fluorometry). Qualification and experimental implementation of these techniques were first conducted on a nonradioactive surrogate, copper. These observations were used to better understand and quantify continuously and in situ the material dissolution mechanisms and the pH variation at the interface, as well as providing data on the behavior of the off-gases. Intermediate species favorable to the reaction were identified, and made it possible to quantify the coupling between hydrodynamics and dissolution kinetics. We were also able to obtain a pH map of the reaction interface, which is very difficult to implement for this type of reaction in corrosive media.</div>
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<fC03 i1="05" i2="X" l="SPA"><s0>Residuos radioactivos</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Découpage</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Cutting</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Troquelado</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Combustible</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Fuel</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Combustible</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Modélisation</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Modeling</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Modelización</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Optimisation</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Optimization</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Optimización</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Interface liquide solide</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Liquid solid interface</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Interfase líquido sólido</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Réacteur</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Reactor</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Reactor</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Surveillance</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Surveillance</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Vigilancia</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Microscopie confocale</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Confocal microscopy</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Microscopía confocal</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>pH</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>pH</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>pH</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Qualification</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Qualification</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Cualificación</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>In situ</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>In situ</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>In situ</s0>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Hydrodynamique</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Hydrodynamics</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Hidrodinámica</s0>
<s5>17</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Cinétique</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Kinetics</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Cinética</s0>
<s5>18</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE"><s0>Cartographie</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG"><s0>Cartography</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA"><s0>Cartografía</s0>
<s5>19</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE"><s0>Bulle</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG"><s0>Bubble</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA"><s0>Ampolla</s0>
<s5>20</s5>
</fC03>
<fC03 i1="21" i2="X" l="FRE"><s0>Miniaturisation</s0>
<s5>21</s5>
</fC03>
<fC03 i1="21" i2="X" l="ENG"><s0>Miniaturization</s0>
<s5>21</s5>
</fC03>
<fC03 i1="21" i2="X" l="SPA"><s0>Miniaturización</s0>
<s5>21</s5>
</fC03>
<fN21><s1>339</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
<affiliations><list><country><li>France</li>
</country>
<region><li>Grand Est</li>
<li>Languedoc-Roussillon</li>
<li>Lorraine (région)</li>
<li>Occitanie (région administrative)</li>
<li>Île-de-France</li>
</region>
<settlement><li>Bagnols sur Cèze</li>
<li>Nancy</li>
<li>Paris La Défense</li>
</settlement>
</list>
<tree><country name="France"><region name="Occitanie (région administrative)"><name sortKey="Delwaulle, Celine" sort="Delwaulle, Celine" uniqKey="Delwaulle C" first="Céline" last="Delwaulle">Céline Delwaulle</name>
</region>
<name sortKey="Bosse, Emilie" sort="Bosse, Emilie" uniqKey="Bosse E" first="Emilie" last="Bosse">Emilie Bosse</name>
<name sortKey="Houzelot, Jean Leon" sort="Houzelot, Jean Leon" uniqKey="Houzelot J" first="Jean-Léon" last="Houzelot">Jean-Léon Houzelot</name>
<name sortKey="Magnaldo, Alastair" sort="Magnaldo, Alastair" uniqKey="Magnaldo A" first="Alastair" last="Magnaldo">Alastair Magnaldo</name>
<name sortKey="Rodier, Benjamin" sort="Rodier, Benjamin" uniqKey="Rodier B" first="Benjamin" last="Rodier">Benjamin Rodier</name>
<name sortKey="Salvatores, Andrea" sort="Salvatores, Andrea" uniqKey="Salvatores A" first="Andrea" last="Salvatores">Andrea Salvatores</name>
<name sortKey="Schaer, Eric" sort="Schaer, Eric" uniqKey="Schaer E" first="Eric" last="Schaer">Eric Schaer</name>
</country>
</tree>
</affiliations>
</record>

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Development of a new method for investigating the mechanisms of solid particle dissolution in nitric acid media: Millifluidic study using fluorescent indicators

Development of a new method for investigating the mechanisms of solid particle dissolution in nitric acid media: Millifluidic study using fluorescent indicators

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