LrgpV1, Main, Merge, bibRecord, 003318

Crystallization and precipitation engineering—IV. Kinetic model of adipic acid crystallization

Identifieur interne : 003318 ( Main/Merge ); précédent : 003317; suivant : 003319

Crystallization and precipitation engineering—IV. Kinetic model of adipic acid crystallization

Auteurs : René David [France] ; Jacques Villermaux [France] ; Philippe Marchal [France] ; Jean-Paul Klein [France]

Source :

Chemical Engineering Science [ 0009-2509 ] ; 1991.

RBID : ISTEX:8C7D34884A2D6736404E37B2C84C3A350318D8C4

English descriptors

Abstract

Abstract: A complete description of adipic crystallization from an aqueous solution is presented, including nucleation, growth and agglomeration. Crystallization is carried out in a semi-batch isothermal crystallizer fed by a hot solution of adipic acid. The conductivity of the solution is monitored and the CSD is sampled out as a function of time. As different kinetic processes control the successive steps of the crystallization, the kinetic model, which involves eight parameters, can be fitted by optimization of at most four parameters simultaneously. A good agreement is found between model predictions and experimental data. The model is shown to be valid to represent the crystallization of adipic acid in an MSMPR crystallizer.

Url:

https://api.istex.fr/document/8C7D34884A2D6736404E37B2C84C3A350318D8C4/fulltext/pdf

DOI: 10.1016/0009-2509(91)85105-7

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ISTEX:8C7D34884A2D6736404E37B2C84C3A350318D8C4

Le document en format XML

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<term>Aqueous solution</term>
<term>Average size</term>
<term>Chemical regime</term>
<term>Comparison betweenmodel</term>
<term>Conductometric</term>
<term>Conductometric curve</term>
<term>Continuous operation</term>
<term>Crystal growth</term>
<term>Crystal size distribution</term>
<term>Crystal size distributions</term>
<term>Crystallization</term>
<term>Crystallization process</term>
<term>Crystallizer</term>
<term>Diffusion layer</term>
<term>Efficient method</term>
<term>Experimental data</term>
<term>Feed concentration</term>
<term>Granulometric</term>
<term>Granulometric classes</term>
<term>Granulometric data</term>
<term>Growth rate</term>
<term>Kinetic parameters</term>
<term>Marchal</term>
<term>Msmpr</term>
<term>Msmpr crystallizer</term>
<term>Nucleation</term>
<term>Population balance</term>
<term>Precipitation</term>
<term>Primary nucleation</term>
<term>Pure water</term>
<term>Renb david</term>
<term>Rushton turbine</term>
<term>Secondary nucleation</term>
<term>Secondary nucleation rate</term>
<term>Size class</term>
<term>Solid concentration</term>
<term>Space time</term>
<term>Standard deviation</term>
<term>Steady state</term>
<term>Storage tank</term>
<term>Supersaturation</term>
<term>Total impurities</term>
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<keywords scheme="Teeft" xml:lang="en"><term>Adipic</term>
<term>Adipic acid</term>
<term>Agglomeration</term>
<term>Agglomeration rate</term>
<term>Aqueous solution</term>
<term>Average size</term>
<term>Chemical regime</term>
<term>Comparison betweenmodel</term>
<term>Conductometric</term>
<term>Conductometric curve</term>
<term>Continuous operation</term>
<term>Crystal growth</term>
<term>Crystal size distribution</term>
<term>Crystal size distributions</term>
<term>Crystallization</term>
<term>Crystallization process</term>
<term>Crystallizer</term>
<term>Diffusion layer</term>
<term>Efficient method</term>
<term>Experimental data</term>
<term>Feed concentration</term>
<term>Granulometric</term>
<term>Granulometric classes</term>
<term>Granulometric data</term>
<term>Growth rate</term>
<term>Kinetic parameters</term>
<term>Marchal</term>
<term>Msmpr</term>
<term>Msmpr crystallizer</term>
<term>Nucleation</term>
<term>Population balance</term>
<term>Precipitation</term>
<term>Primary nucleation</term>
<term>Pure water</term>
<term>Renb david</term>
<term>Rushton turbine</term>
<term>Secondary nucleation</term>
<term>Secondary nucleation rate</term>
<term>Size class</term>
<term>Solid concentration</term>
<term>Space time</term>
<term>Standard deviation</term>
<term>Steady state</term>
<term>Storage tank</term>
<term>Supersaturation</term>
<term>Total impurities</term>
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<front><div type="abstract" xml:lang="en">Abstract: A complete description of adipic crystallization from an aqueous solution is presented, including nucleation, growth and agglomeration. Crystallization is carried out in a semi-batch isothermal crystallizer fed by a hot solution of adipic acid. The conductivity of the solution is monitored and the CSD is sampled out as a function of time. As different kinetic processes control the successive steps of the crystallization, the kinetic model, which involves eight parameters, can be fitted by optimization of at most four parameters simultaneously. A good agreement is found between model predictions and experimental data. The model is shown to be valid to represent the crystallization of adipic acid in an MSMPR crystallizer.</div>
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Crystallization and precipitation engineering—IV. Kinetic model of adipic acid crystallization

Crystallization and precipitation engineering—IV. Kinetic model of adipic acid crystallization

Source :

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri