Impact of the design and the materials of rectangular microchannel reactors on the photocatalytic decomposition of organic pollutant
Identifieur interne : 000897 ( Main/Exploration ); précédent : 000896; suivant : 000898Impact of the design and the materials of rectangular microchannel reactors on the photocatalytic decomposition of organic pollutant
Auteurs : Guillaume Charles [France] ; Thibault Roques-Carmes [France] ; Nidhal Becheikh [France] ; Laurent Falk [France] ; Serge Corbel [France]Source :
- Green Processing and Synthesis [ 2191-9542 ] ; 2012-08-01.
Descripteurs français
English descriptors
- KwdEn :
- Acat, Acid concentration, Acid solution, Adsorption, Catal, Catalyst, Catalyst surface, Channel height, Channel length, Channel width, Chem, Chemical engineering, Cnrs, Contaminant concentration, Continuous flow operation, Corbel, Cout, Dark adsorption, Degradation, Degradation ratio, Different dimensions, Ecole nationale, Engineering degree, Entire catalyst surface, Experimental conditions, Experimental data, Flow rate, Flow rates, Geometrical, Geometrical characteristics, Geometrical dimensions, Guillaume charles, Inlet, Inlet concentration, Laboratoire, Largest channel width, Laurent falk, Light intensity, Light irradiation, Lorraine, Mass transfer limitation, Microchannel, Microchannel dimensions, Microchannel length, Microchannel reactor, Microchannel reactors, Microchannel size, Microreactors, Nancy cedex, Optimal design, Permanent regime, Photocatalyst, Photocatalytic, Photocatalytic activity, Photocatalytic degradation, Photocatalytic efficiency, Photocatalytic experiment, Photocatalytic performances, Photocatalytic process, Photocatalytic reaction, Photocatalytic reactions, Plateau value, Pollutant, Polycarbonate, Polymeric, Proportionality factor, Reactor, Reactor dimensions, Rectangular, Residence time, Salicylic, Salicylic acid, Salicylic acid concentration, Specific catalyst surface area, Stereolithography, Tio2, Tio2 film, Titanium dioxide, Total catalyst surface, Volume unit.
- Teeft :
- Acat, Acid concentration, Acid solution, Adsorption, Catal, Catalyst, Catalyst surface, Channel height, Channel length, Channel width, Chem, Chemical engineering, Cnrs, Contaminant concentration, Continuous flow operation, Corbel, Cout, Dark adsorption, Degradation, Degradation ratio, Different dimensions, Ecole nationale, Engineering degree, Entire catalyst surface, Experimental conditions, Experimental data, Flow rate, Flow rates, Geometrical, Geometrical characteristics, Geometrical dimensions, Guillaume charles, Inlet, Inlet concentration, Laboratoire, Largest channel width, Laurent falk, Light intensity, Light irradiation, Lorraine, Mass transfer limitation, Microchannel, Microchannel dimensions, Microchannel length, Microchannel reactor, Microchannel reactors, Microchannel size, Microreactors, Nancy cedex, Optimal design, Permanent regime, Photocatalyst, Photocatalytic, Photocatalytic activity, Photocatalytic degradation, Photocatalytic efficiency, Photocatalytic experiment, Photocatalytic performances, Photocatalytic process, Photocatalytic reaction, Photocatalytic reactions, Plateau value, Pollutant, Polycarbonate, Polymeric, Proportionality factor, Reactor, Reactor dimensions, Rectangular, Residence time, Salicylic, Salicylic acid, Salicylic acid concentration, Specific catalyst surface area, Stereolithography, Tio2, Tio2 film, Titanium dioxide, Total catalyst surface, Volume unit.
Abstract
The objective of this article is to find the optimal design of rectangular microchannel reactors, in terms of reactor dimensions and materials, in order to increase the photocatalytic activity. Microchannel reactors with immobilized titanium dioxide (TiO2) as photocatalyst have been designed, fabricated, and tested. The photocatalytic degradation of salicylic acid is investigated as a function of microchannel size, materials that constitute the reactor, contaminant concentration and flow rate. All the reactors exhibit the same behavior. Higher degradation is observed for low pollutant concentrations and flow rates. The nature of the constituent element of the reactor has practically no influence on the photocatalytic process. The degradation performance is affected by the microchannel dimensions. The reactor with the largest channel width and length, and the lowest channel height displays the highest photocatalytic activity. For an optimal design of the rectangular microchannel reactors a relation between the degradation ratio X and the dimensions of the microchannel is reported. A linear relationship between X and wL/h2 (L: length, w: width, h: height of the channel) is found experimentally. The product wL emphasizes the uniform irradiance over the entire catalyst surface and confirms that the bottom of the channel covered with TiO2 is photoactivated. The term in 1/h2 is necessary to take into account the mass transfer limitation.
Url:
DOI: 10.1515/gps-2012-0022
Affiliations:
- France
- Grand Est, Lorraine (région)
- Nancy
- Centre national de la recherche scientifique, Laboratoire réactions et génie des procédés, Université de Lorraine
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Le document en format XML
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xml:lang="en"><term>Acat</term><term>Acid concentration</term><term>Acid solution</term><term>Adsorption</term><term>Catal</term><term>Catalyst</term><term>Catalyst surface</term><term>Channel height</term><term>Channel length</term><term>Channel width</term><term>Chem</term><term>Chemical engineering</term><term>Cnrs</term><term>Contaminant concentration</term><term>Continuous flow operation</term><term>Corbel</term><term>Cout</term><term>Dark adsorption</term><term>Degradation</term><term>Degradation ratio</term><term>Different dimensions</term><term>Ecole nationale</term><term>Engineering degree</term><term>Entire catalyst surface</term><term>Experimental conditions</term><term>Experimental data</term><term>Flow rate</term><term>Flow rates</term><term>Geometrical</term><term>Geometrical characteristics</term><term>Geometrical dimensions</term><term>Guillaume charles</term><term>Inlet</term><term>Inlet concentration</term><term>Laboratoire</term><term>Largest channel width</term><term>Laurent falk</term><term>Light intensity</term><term>Light irradiation</term><term>Lorraine</term><term>Mass transfer limitation</term><term>Microchannel</term><term>Microchannel dimensions</term><term>Microchannel length</term><term>Microchannel reactor</term><term>Microchannel reactors</term><term>Microchannel size</term><term>Microreactors</term><term>Nancy cedex</term><term>Optimal design</term><term>Permanent regime</term><term>Photocatalyst</term><term>Photocatalytic</term><term>Photocatalytic activity</term><term>Photocatalytic degradation</term><term>Photocatalytic efficiency</term><term>Photocatalytic experiment</term><term>Photocatalytic performances</term><term>Photocatalytic process</term><term>Photocatalytic reaction</term><term>Photocatalytic reactions</term><term>Plateau value</term><term>Pollutant</term><term>Polycarbonate</term><term>Polymeric</term><term>Proportionality factor</term><term>Reactor</term><term>Reactor dimensions</term><term>Rectangular</term><term>Residence time</term><term>Salicylic</term><term>Salicylic acid</term><term>Salicylic acid concentration</term><term>Specific catalyst surface area</term><term>Stereolithography</term><term>Tio2</term><term>Tio2 film</term><term>Titanium dioxide</term><term>Total catalyst surface</term><term>Volume unit</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Acat</term><term>Acid concentration</term><term>Acid solution</term><term>Adsorption</term><term>Catal</term><term>Catalyst</term><term>Catalyst surface</term><term>Channel height</term><term>Channel length</term><term>Channel width</term><term>Chem</term><term>Chemical engineering</term><term>Cnrs</term><term>Contaminant concentration</term><term>Continuous flow operation</term><term>Corbel</term><term>Cout</term><term>Dark adsorption</term><term>Degradation</term><term>Degradation ratio</term><term>Different dimensions</term><term>Ecole nationale</term><term>Engineering degree</term><term>Entire catalyst surface</term><term>Experimental conditions</term><term>Experimental data</term><term>Flow rate</term><term>Flow rates</term><term>Geometrical</term><term>Geometrical characteristics</term><term>Geometrical dimensions</term><term>Guillaume charles</term><term>Inlet</term><term>Inlet concentration</term><term>Laboratoire</term><term>Largest channel width</term><term>Laurent falk</term><term>Light intensity</term><term>Light irradiation</term><term>Lorraine</term><term>Mass transfer limitation</term><term>Microchannel</term><term>Microchannel dimensions</term><term>Microchannel length</term><term>Microchannel reactor</term><term>Microchannel reactors</term><term>Microchannel size</term><term>Microreactors</term><term>Nancy cedex</term><term>Optimal design</term><term>Permanent regime</term><term>Photocatalyst</term><term>Photocatalytic</term><term>Photocatalytic activity</term><term>Photocatalytic degradation</term><term>Photocatalytic efficiency</term><term>Photocatalytic experiment</term><term>Photocatalytic performances</term><term>Photocatalytic process</term><term>Photocatalytic reaction</term><term>Photocatalytic reactions</term><term>Plateau value</term><term>Pollutant</term><term>Polycarbonate</term><term>Polymeric</term><term>Proportionality factor</term><term>Reactor</term><term>Reactor dimensions</term><term>Rectangular</term><term>Residence time</term><term>Salicylic</term><term>Salicylic acid</term><term>Salicylic acid concentration</term><term>Specific catalyst surface area</term><term>Stereolithography</term><term>Tio2</term><term>Tio2 film</term><term>Titanium dioxide</term><term>Total catalyst surface</term><term>Volume unit</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Lorraine</term><term>Polluant</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The objective of this article is to find the optimal design of rectangular microchannel reactors, in terms of reactor dimensions and materials, in order to increase the photocatalytic activity. Microchannel reactors with immobilized titanium dioxide (TiO2) as photocatalyst have been designed, fabricated, and tested. The photocatalytic degradation of salicylic acid is investigated as a function of microchannel size, materials that constitute the reactor, contaminant concentration and flow rate. All the reactors exhibit the same behavior. Higher degradation is observed for low pollutant concentrations and flow rates. The nature of the constituent element of the reactor has practically no influence on the photocatalytic process. The degradation performance is affected by the microchannel dimensions. The reactor with the largest channel width and length, and the lowest channel height displays the highest photocatalytic activity. For an optimal design of the rectangular microchannel reactors a relation between the degradation ratio X and the dimensions of the microchannel is reported. A linear relationship between X and wL/h2 (L: length, w: width, h: height of the channel) is found experimentally. The product wL emphasizes the uniform irradiance over the entire catalyst surface and confirms that the bottom of the channel covered with TiO2 is photoactivated. The term in 1/h2 is necessary to take into account the mass transfer limitation.</div></front></TEI><affiliations><list><country><li>France</li></country><region><li>Grand Est</li><li>Lorraine (région)</li></region><settlement><li>Nancy</li></settlement><orgName><li>Centre national de la recherche scientifique</li><li>Laboratoire réactions et génie des procédés</li><li>Université de Lorraine</li></orgName></list><tree><country name="France"><region name="Grand Est"><name sortKey="Charles, Guillaume" sort="Charles, Guillaume" uniqKey="Charles G" first="Guillaume" last="Charles">Guillaume Charles</name></region><name sortKey="Becheikh, Nidhal" sort="Becheikh, Nidhal" uniqKey="Becheikh N" first="Nidhal" last="Becheikh">Nidhal Becheikh</name><name sortKey="Becheikh, Nidhal" sort="Becheikh, Nidhal" uniqKey="Becheikh N" first="Nidhal" last="Becheikh">Nidhal Becheikh</name><name sortKey="Charles, Guillaume" sort="Charles, Guillaume" uniqKey="Charles G" first="Guillaume" last="Charles">Guillaume Charles</name><name sortKey="Corbel, Serge" sort="Corbel, Serge" uniqKey="Corbel S" first="Serge" last="Corbel">Serge Corbel</name><name sortKey="Corbel, Serge" sort="Corbel, Serge" uniqKey="Corbel S" first="Serge" last="Corbel">Serge Corbel</name><name sortKey="Falk, Laurent" sort="Falk, Laurent" uniqKey="Falk L" first="Laurent" last="Falk">Laurent Falk</name><name sortKey="Falk, Laurent" sort="Falk, Laurent" uniqKey="Falk L" first="Laurent" last="Falk">Laurent Falk</name><name sortKey="Roques Carmes, Thibault" sort="Roques Carmes, Thibault" uniqKey="Roques Carmes T" first="Thibault" last="Roques-Carmes">Thibault Roques-Carmes</name><name sortKey="Roques Carmes, Thibault" sort="Roques Carmes, Thibault" uniqKey="Roques Carmes T" first="Thibault" last="Roques-Carmes">Thibault Roques-Carmes</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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