LrgpV1, Istex, Corpus, bibRecord, 001792

Studies on the steroidal components of domestic plants—XXI

Identifieur interne : 001792 ( Istex/Corpus ); précédent : 001791; suivant : 001793

Studies on the steroidal components of domestic plants—XXI

Auteurs : Tokuo Kubota ; Ken'Ichi Takeda

Source :

Tetrahedron [ 0040-4020 ] ; 1960.

RBID : ISTEX:56F0F00FF19B80D62C8A7F9EE1289403B79C0533

English descriptors

KwdEn :
- Acetonide formation, Allylic, Allylic rearrangement, Analytical values, Anhydrokogagcnin, Anhydrokogagcnin triacctatc, Anhydrokogagcnin triacetate, Authentic sample, Benzene, Chloroform, Chrm, Cthcr, Dioxide, Domestic plants, Double bond, Empirical formula, Ether, Further clution, Hydroxyl, Hydroxyl band, Isomer, Kogagcnin, Lithium aluminium hydride, Manganese, Manganese dioxide, Manganese dioxide oxidation, Methanol, Mlxturc, Neutral product, Pcrbcnzoic acid, Primary product, Pure umplc, Small amount, Thionyl chloride, Ulth, Ulth cthcr, Wcrc, Xvllla.
Teeft :
- Acetonide formation, Allylic, Allylic rearrangement, Analytical values, Anhydrokogagcnin, Anhydrokogagcnin triacctatc, Anhydrokogagcnin triacetate, Authentic sample, Benzene, Chloroform, Chrm, Cthcr, Dioxide, Domestic plants, Double bond, Empirical formula, Ether, Further clution, Hydroxyl, Hydroxyl band, Isomer, Kogagcnin, Lithium aluminium hydride, Manganese, Manganese dioxide, Manganese dioxide oxidation, Methanol, Mlxturc, Neutral product, Pcrbcnzoic acid, Primary product, Pure umplc, Small amount, Thionyl chloride, Ulth, Ulth cthcr, Wcrc, Xvllla.

Abstract

Abstract: In an earlier paper2 of this series, we assigned the position of the double bond in anhydrokogagenin, a dehydration product of kogagenin, at C-5 and 6 tentatively. This has now been confirmed to be located at C-4 and 5 from the results of the epoxide formation, manganese dioxide oxidation and the glycol fission reaction. It has been found that the reaction of anhydrokogagenin with acetone containing a small amount of p-toluenesulphonic acid gives an allylic rearrangement product together with the normal acetonide.

Url:

https://api.istex.fr/document/56F0F00FF19B80D62C8A7F9EE1289403B79C0533/fulltext/pdf

DOI: 10.1016/0040-4020(60)85001-6

Links to Exploration step

ISTEX:56F0F00FF19B80D62C8A7F9EE1289403B79C0533

Le document en format XML

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<front><div type="abstract" xml:lang="en">Abstract: In an earlier paper2 of this series, we assigned the position of the double bond in anhydrokogagenin, a dehydration product of kogagenin, at C-5 and 6 tentatively. This has now been confirmed to be located at C-4 and 5 from the results of the epoxide formation, manganese dioxide oxidation and the glycol fission reaction. It has been found that the reaction of anhydrokogagenin with acetone containing a small amount of p-toluenesulphonic acid gives an allylic rearrangement product together with the normal acetonide.</div>
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   |texte=   Studies on the steroidal components of domestic plants—XXI
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	Serveur d'exploration sur le LRGP
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Studies on the steroidal components of domestic plants—XXI

Studies on the steroidal components of domestic plants—XXI

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