Stepwise Synthesis and Crystal Structure of Tricarbonyl[pentakis(methylthio)cyclopentadienyl]‐manganese [{C5(SMe)5}Mn(CO)3]
Identifieur interne : 001285 ( Istex/Corpus ); précédent : 001284; suivant : 001286Stepwise Synthesis and Crystal Structure of Tricarbonyl[pentakis(methylthio)cyclopentadienyl]‐manganese [{C5(SMe)5}Mn(CO)3]
Auteurs : Karlheinz Sünkel ; Doris MotzSource :
- Angewandte Chemie International Edition in English [ 0570-0833 ] ; 1988-07.
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Abstract
Functionalized cyclopentadienyl ligands, with, e.g. one to five methylthio and four to zero chloro substituents are very promising species. Starting from [(C5Cl4Br)Mn(CO)3] it has now been possible to synthesize all members of the series 1 which contain this ligand. The donor properties of the ligand increase with increasing number of MeS groups.
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DOI: 10.1002/anie.198809391
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ISTEX:8B3ED9E732B339565FAEBB367F76A05A8C4BB510Le document en format XML
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Starting from [(C5Cl4Br)Mn(CO)3] it has now been possible to synthesize all members of the series 1 which contain this ligand. 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Starting from [(C<sub>5</sub>Cl<sub>4</sub>Br)Mn(CO)<sub>3</sub>] it has now been possible to synthesize all members of the series <b>1</b> which contain this ligand. The donor properties of the ligand increase with increasing number of MeS groups. <blockFixed type="graphic"><mediaResourceGroup><mediaResource alt="image" copyright="VCH Verlagsgesellschaft mbH" href="urn:x-wiley:05700833:media:ANIE198809391:ust001"></mediaResource><mediaResource alt="thumbnail image" rendition="webLoRes" mimeType="image/gif" href=""></mediaResource><mediaResource alt="original image" rendition="webOriginal" mimeType="image/gif" href=""></mediaResource><mediaResource alt="magnified image" rendition="webHiRes" mimeType="image/gif" href=""></mediaResource></mediaResourceGroup></blockFixed></p></abstract></abstractGroup></contentMeta><noteGroup><note xml:id="fn1"><p>Complexation Chemistry of Perhalogenated Cyclopentadienes and Alkynes, Part 2. We thank Prof. Dr. <i>W. Beck</i> for his interest in and support of this work.—Part 1: [1].</p></note></noteGroup></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Stepwise Synthesis and Crystal Structure of Tricarbonyl[pentakis(methylthio)cyclopentadienyl]‐manganese [{C5(SMe)5}Mn(CO)3]</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Stepwise Synthesis and Crystal Structure of Tricarbonyl[pentakis(methylthio)cyclopentadienyl]‐manganese [{C5(SMe)5}Mn(CO)3]</title></titleInfo><name type="personal"><namePart type="termsOfAddress">Dr.</namePart><namePart type="given">Karlheinz</namePart><namePart type="family">Sünkel</namePart><affiliation>Institut für anorganische Chemie der Universität, Meiserstrasse 1, D‐8000 München 2 (FRG)</affiliation><affiliation>Correspondence address: Institut für anorganische Chemie der Universität, Meiserstrasse 1, D‐8000 München 2 (FRG)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Doris</namePart><namePart type="family">Motz</namePart><affiliation>Institut für anorganische Chemie der Universität, Meiserstrasse 1, D‐8000 München 2 (FRG)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="brief-communication" displayLabel="shortCommunication" authority="ISTEX" authorityURI="https://content-type.data.istex.fr" valueURI="https://content-type.data.istex.fr/ark:/67375/XTP-S9SX2MFS-0">brief-communication</genre><originInfo><publisher>Hüthig & Wepf Verlag</publisher><place><placeTerm type="text">Zug</placeTerm></place><dateIssued encoding="w3cdtf">1988-07</dateIssued><dateCaptured encoding="w3cdtf">1988-02-11</dateCaptured><copyrightDate encoding="w3cdtf">1988</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><extent unit="figures">1</extent><extent unit="tables">0</extent><extent unit="references">12</extent></physicalDescription><abstract>Functionalized cyclopentadienyl ligands, with, e.g. one to five methylthio and four to zero chloro substituents are very promising species. Starting from [(C5Cl4Br)Mn(CO)3] it has now been possible to synthesize all members of the series 1 which contain this ligand. The donor properties of the ligand increase with increasing number of MeS groups.</abstract><note type="content">*Complexation Chemistry of Perhalogenated Cyclopentadienes and Alkynes, Part 2. We thank Prof. Dr. W. Beck for his interest in and support of this work.—Part 1: [1].</note><relatedItem type="host"><titleInfo><title>Angewandte Chemie International Edition in English</title></titleInfo><titleInfo type="abbreviated"><title>Angew. Chem. Int. Ed. 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