Crystallization and precipitation engineering — VII. The modelling of sodium perborate tetrahydrate crystallization from solution
Identifieur interne : 001242 ( Istex/Corpus ); précédent : 001241; suivant : 001243Crystallization and precipitation engineering — VII. The modelling of sodium perborate tetrahydrate crystallization from solution
Auteurs : René David ; Jean-Michel BossoutrotSource :
- Chemical Engineering Science [ 0009-2509 ] ; 1996.
English descriptors
- KwdEn :
- Agglomeration, Aqueous solutions, Average class size, Average size, Average sizes, Batch crystallizer, Chem, Chianese, Crystal growth, Crystal size, Crystal size distribution, Crystallization, Crystallization process, Desupersaturation, Desupersaturation curve, Desupersaturation curves, Dimensionless, Draft tube, Elementary agglomeration rate, Elsevier science, Experimental evidence, First moments, Growth rate, Hydrogen peroxide, Initial concentration, Initial concentrations, Kinetic model, Liquid phase, Model desupersaturation curves, Model experiment, Nucleation, Objective function, Perborate, Peroxide, Precipitation, Precipitation engineering, Primary nucleation, Primary nucleation parameter, Reactant, Same mass, Second half, Secondary nucleation, Shape factor, Smaller crystals, Sodium metaborate, Sodium perborate, Sodium perborate tetrahydrate, Solid volume fraction, Stoichiometric coefficient, Suspension volume, Temperature sensor, Thermostatic bath, Volume fraction, agglomeration, growth, nucleation, sodium perborate tetrahydrate.
- Teeft :
- Agglomeration, Aqueous solutions, Average class size, Average size, Average sizes, Batch crystallizer, Chem, Chianese, Crystal growth, Crystal size, Crystal size distribution, Crystallization, Crystallization process, Desupersaturation, Desupersaturation curve, Desupersaturation curves, Dimensionless, Draft tube, Elementary agglomeration rate, Elsevier science, Experimental evidence, First moments, Growth rate, Hydrogen peroxide, Initial concentration, Initial concentrations, Kinetic model, Liquid phase, Model desupersaturation curves, Model experiment, Nucleation, Objective function, Perborate, Peroxide, Precipitation, Precipitation engineering, Primary nucleation, Primary nucleation parameter, Reactant, Same mass, Second half, Secondary nucleation, Shape factor, Smaller crystals, Sodium metaborate, Sodium perborate, Sodium perborate tetrahydrate, Solid volume fraction, Stoichiometric coefficient, Suspension volume, Temperature sensor, Thermostatic bath, Volume fraction.
Abstract
Abstract: The crystallization of sodium perborate tetrahydrate (SPT) was carried out in a batch crystallizer with and without seeding. SPT concentration and CSD were monitored as functions of time, and the final crystals visualized by SEM micrography. Experimental evidence for primary and secondary nucleation, crystal growth and crystal agglomeration was observed. Thus, a simulation model including these processes is presented. From the experimental data, seven parameters of the model were fitted by optimization in two different steps.
Url:
DOI: 10.1016/0009-2509(96)00276-X
Links to Exploration step
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<ce:abstract-sec><ce:simple-para view="all" id="simple-para.0010">The crystallization of sodium perborate tetrahydrate (SPT) was carried out in a batch crystallizer with and without seeding. SPT concentration and CSD were monitored as functions of time, and the final crystals visualized by SEM micrography. Experimental evidence for primary and secondary nucleation, crystal growth and crystal agglomeration was observed. Thus, a simulation model including these processes is presented. From the experimental data, seven parameters of the model were fitted by optimization in two different steps.</ce:simple-para>
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<name type="personal"><namePart type="given">Jean-Michel</namePart>
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<affiliation>Elf-Atochem, Centre de Recherche Rhône-Alpes, BP 63, 69493 Pierre-Bénite Cedex, France</affiliation>
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<dateIssued encoding="w3cdtf">1996</dateIssued>
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<language><languageTerm type="code" authority="iso639-2b">eng</languageTerm>
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<abstract lang="en">Abstract: The crystallization of sodium perborate tetrahydrate (SPT) was carried out in a batch crystallizer with and without seeding. SPT concentration and CSD were monitored as functions of time, and the final crystals visualized by SEM micrography. Experimental evidence for primary and secondary nucleation, crystal growth and crystal agglomeration was observed. Thus, a simulation model including these processes is presented. From the experimental data, seven parameters of the model were fitted by optimization in two different steps.</abstract>
<subject lang="en"><genre>Keywords</genre>
<topic>Crystallization</topic>
<topic>sodium perborate tetrahydrate</topic>
<topic>agglomeration</topic>
<topic>growth</topic>
<topic>nucleation</topic>
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<relatedItem type="host"><titleInfo><title>Chemical Engineering Science</title>
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<dateIssued encoding="w3cdtf">199611</dateIssued>
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<identifier type="ISSN">0009-2509</identifier>
<identifier type="PII">S0009-2509(00)X0055-3</identifier>
<part><date>199611</date>
<detail type="volume"><number>51</number>
<caption>vol.</caption>
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<detail type="issue"><number>21</number>
<caption>no.</caption>
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<extent unit="issue-pages"><start>4749</start>
<end>4947</end>
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<extent unit="pages"><start>4939</start>
<end>4947</end>
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<identifier type="DOI">10.1016/0009-2509(96)00276-X</identifier>
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<identifier type="ArticleID">9600276X</identifier>
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