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Crystallization and precipitation engineering — VII. The modelling of sodium perborate tetrahydrate crystallization from solution

Identifieur interne : 001242 ( Istex/Corpus ); précédent : 001241; suivant : 001243

Crystallization and precipitation engineering — VII. The modelling of sodium perborate tetrahydrate crystallization from solution

Auteurs : René David ; Jean-Michel Bossoutrot

Source :

RBID : ISTEX:E2EDF5B28909CB1DD4B1DF5C6D5DE5BACDF34B19

English descriptors

Abstract

Abstract: The crystallization of sodium perborate tetrahydrate (SPT) was carried out in a batch crystallizer with and without seeding. SPT concentration and CSD were monitored as functions of time, and the final crystals visualized by SEM micrography. Experimental evidence for primary and secondary nucleation, crystal growth and crystal agglomeration was observed. Thus, a simulation model including these processes is presented. From the experimental data, seven parameters of the model were fitted by optimization in two different steps.

Url:
DOI: 10.1016/0009-2509(96)00276-X

Links to Exploration step

ISTEX:E2EDF5B28909CB1DD4B1DF5C6D5DE5BACDF34B19

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<affiliation>Elf-Atochem, Centre de Recherche Rhône-Alpes, BP 63, 69493 Pierre-Bénite Cedex, France</affiliation>
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<abstract lang="en">Abstract: The crystallization of sodium perborate tetrahydrate (SPT) was carried out in a batch crystallizer with and without seeding. SPT concentration and CSD were monitored as functions of time, and the final crystals visualized by SEM micrography. Experimental evidence for primary and secondary nucleation, crystal growth and crystal agglomeration was observed. Thus, a simulation model including these processes is presented. From the experimental data, seven parameters of the model were fitted by optimization in two different steps.</abstract>
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<genre>Keywords</genre>
<topic>Crystallization</topic>
<topic>sodium perborate tetrahydrate</topic>
<topic>agglomeration</topic>
<topic>growth</topic>
<topic>nucleation</topic>
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<dateIssued encoding="w3cdtf">199611</dateIssued>
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<identifier type="ISSN">0009-2509</identifier>
<identifier type="PII">S0009-2509(00)X0055-3</identifier>
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<number>51</number>
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<identifier type="DOI">10.1016/0009-2509(96)00276-X</identifier>
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