A new protocol for the synthesis of α′,β′-unsaturated 1,3-diketones
Identifieur interne : 000611 ( Istex/Corpus ); précédent : 000610; suivant : 000612A new protocol for the synthesis of α′,β′-unsaturated 1,3-diketones
Auteurs : Renato Dalpozzo ; Antonio De Nino ; Emma Iantorno ; Giuseppe Bartoli ; Marcella Bosco ; Letizia SambriSource :
- Tetrahedron [ 0040-4020 ] ; 1997.
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Abstract
Abstract: Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and stereocontrol of the new double bond.
Url:
DOI: 10.1016/S0040-4020(96)01148-9
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ISTEX:F0CDEDF102188BA3FF7A583AF06729DBC7396CBDLe document en format XML
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Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Tetrahedron</title><title level="j" type="abbrev">TET</title><idno type="ISSN">0040-4020</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1997">1997</date><biblScope unit="volume">53</biblScope><biblScope unit="issue">7</biblScope><biblScope unit="page" from="2585">2585</biblScope><biblScope unit="page" to="2590">2590</biblScope></imprint><idno type="ISSN">0040-4020</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0040-4020</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Ammonium chloride</term><term>Apparent quintet</term><term>Carbonyl</term><term>Carbonyl compound</term><term>Carbonyl compounds</term><term>Double bond</term><term>Elsevier science</term><term>Enamino function</term><term>Equimolecular amount</term><term>Perkin trans</term><term>Product distribution</term><term>Reaction times</term><term>Solvent reaction time</term><term>Trans</term><term>Transition state</term><term>Vmax</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Ammonium chloride</term><term>Apparent quintet</term><term>Carbonyl</term><term>Carbonyl compound</term><term>Carbonyl compounds</term><term>Double bond</term><term>Elsevier science</term><term>Enamino function</term><term>Equimolecular amount</term><term>Perkin trans</term><term>Product distribution</term><term>Reaction times</term><term>Solvent reaction time</term><term>Trans</term><term>Transition state</term><term>Vmax</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and stereocontrol of the new double bond.</div></front></TEI><istex><corpusName>elsevier</corpusName><keywords><teeft><json:string>vmax</json:string><json:string>trans</json:string><json:string>carbonyl</json:string><json:string>carbonyl compound</json:string><json:string>product distribution</json:string><json:string>double bond</json:string><json:string>reaction times</json:string><json:string>carbonyl compounds</json:string><json:string>elsevier science</json:string><json:string>transition state</json:string><json:string>enamino function</json:string><json:string>ammonium chloride</json:string><json:string>equimolecular amount</json:string><json:string>solvent reaction time</json:string><json:string>apparent quintet</json:string><json:string>perkin trans</json:string></teeft></keywords><author><json:item><name>Renato Dalpozzo</name><affiliations><json:string>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</json:string><json:string>E-mail: dalpozzo@pobox.unical.it</json:string></affiliations></json:item><json:item><name>Antonio De Nino</name><affiliations><json:string>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</json:string></affiliations></json:item><json:item><name>Emma Iantorno</name><affiliations><json:string>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</json:string></affiliations></json:item><json:item><name>Giuseppe Bartoli</name><affiliations><json:string>Dipartimento di Chimica Organica ‘A. 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Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</affiliation></author><idno type="istex">F0CDEDF102188BA3FF7A583AF06729DBC7396CBD</idno><idno type="DOI">10.1016/S0040-4020(96)01148-9</idno><idno type="PII">S0040-4020(96)01148-9</idno></analytic><monogr><title level="j">Tetrahedron</title><title level="j" type="abbrev">TET</title><idno type="pISSN">0040-4020</idno><idno type="PII">S0040-4020(00)X0077-4</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1997"></date><biblScope unit="volume">53</biblScope><biblScope unit="issue">7</biblScope><biblScope unit="page" from="2585">2585</biblScope><biblScope unit="page" to="2590">2590</biblScope></imprint></monogr></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1997</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and stereocontrol of the new double bond.</p></abstract><abstract style="graphical"><p>Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and sterocontrol of the new formed double bond.gr1</p></abstract><textClass><keywords scheme="keyword"><list><head>article-category</head><item><term>Article</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="1996-12-11">Modified</change><change when="1997">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><extension>txt</extension><original>false</original><mimetype>text/plain</mimetype><uri>https://api.istex.fr/document/F0CDEDF102188BA3FF7A583AF06729DBC7396CBD/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Elsevier, elements deleted: tail"><istex:xmlDeclaration>version="1.0" encoding="utf-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//ES//DTD journal article DTD version 4.5.2//EN//XML" URI="art452.dtd" name="istex:docType"><istex:entity SYSTEM="gr1" NDATA="IMAGE" name="gr1"></istex:entity></istex:docType><istex:document><converted-article version="4.5.2" docsubtype="fla"><item-info><jid>TET</jid><aid>96011489</aid><ce:pii>S0040-4020(96)01148-9</ce:pii><ce:doi>10.1016/S0040-4020(96)01148-9</ce:doi><ce:copyright type="unknown" year="1997"></ce:copyright><ce:doctopics><ce:doctopic><ce:text>Article</ce:text></ce:doctopic></ce:doctopics></item-info><head><ce:title>A new protocol for the synthesis of α′,β′-unsaturated 1,3-diketones</ce:title><ce:author-group><ce:author><ce:given-name>Renato</ce:given-name><ce:surname>Dalpozzo</ce:surname><ce:ranking><ce:sup>∗</ce:sup></ce:ranking><ce:e-address>dalpozzo@pobox.unical.it</ce:e-address></ce:author><ce:author><ce:given-name>Antonio</ce:given-name><ce:surname>De Nino</ce:surname></ce:author><ce:author><ce:given-name>Emma</ce:given-name><ce:surname>Iantorno</ce:surname></ce:author><ce:affiliation><ce:textfn>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</ce:textfn></ce:affiliation></ce:author-group><ce:author-group><ce:author><ce:given-name>Giuseppe</ce:given-name><ce:surname>Bartoli</ce:surname></ce:author><ce:author><ce:given-name>Marcella</ce:given-name><ce:surname>Bosco</ce:surname></ce:author><ce:author><ce:given-name>Letizia</ce:given-name><ce:surname>Sambri</ce:surname></ce:author><ce:affiliation><ce:textfn>Dipartimento di Chimica Organica ‘A. Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</ce:textfn></ce:affiliation></ce:author-group><ce:date-received day="24" month="10" year="1996"></ce:date-received><ce:date-revised day="11" month="12" year="1996"></ce:date-revised><ce:date-accepted day="12" month="12" year="1996"></ce:date-accepted><ce:abstract><ce:section-title>Abstract</ce:section-title><ce:abstract-sec><ce:simple-para>Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and stereocontrol of the new double bond.</ce:simple-para></ce:abstract-sec></ce:abstract><ce:abstract class="graphical"><ce:abstract-sec><ce:simple-para>Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and sterocontrol of the new formed double bond.</ce:simple-para></ce:abstract-sec><ce:figure><ce:link locator="gr1"></ce:link></ce:figure></ce:abstract></head></converted-article></istex:document></istex:metadataXml><mods version="3.6"><titleInfo><title>A new protocol for the synthesis of α′,β′-unsaturated 1,3-diketones</title></titleInfo><titleInfo type="alternative" contentType="CDATA"><title>A new protocol for the synthesis of α′,β′-unsaturated 1,3-diketones</title></titleInfo><name type="personal"><namePart type="given">Renato</namePart><namePart type="family">Dalpozzo</namePart><affiliation>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</affiliation><affiliation>E-mail: dalpozzo@pobox.unical.it</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Antonio</namePart><namePart type="family">De Nino</namePart><affiliation>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Emma</namePart><namePart type="family">Iantorno</namePart><affiliation>Dipartimento di Chimica, Università della Calabria, I-87030 Arcavacata di Rende Cosenza, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Giuseppe</namePart><namePart type="family">Bartoli</namePart><affiliation>Dipartimento di Chimica Organica ‘A. Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Marcella</namePart><namePart type="family">Bosco</namePart><affiliation>Dipartimento di Chimica Organica ‘A. Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Letizia</namePart><namePart type="family">Sambri</namePart><affiliation>Dipartimento di Chimica Organica ‘A. Mangini’, viale Risorgimento 4, I-40136 Bologna, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="Full-length article" authority="ISTEX" authorityURI="https://content-type.data.istex.fr" valueURI="https://content-type.data.istex.fr/ark:/67375/XTP-1JC4F85T-7">research-article</genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">1997</dateIssued><dateModified encoding="w3cdtf">1996-12-11</dateModified><copyrightDate encoding="w3cdtf">1997</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm><languageTerm type="code" authority="rfc3066">en</languageTerm></language><abstract lang="en">Abstract: Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and stereocontrol of the new double bond.</abstract><abstract type="graphical">Dianions of α′-(trimethylsilyl)enaminones can be used as Peterson reagents in the reaction with aldehydes and ketones, to obtain α′,β′-unsaturated enaminones or 1,3-diketones with regio and sterocontrol of the new formed double bond.gr1 </abstract><subject><genre>article-category</genre><topic>Article</topic></subject><relatedItem type="host"><titleInfo><title>Tetrahedron</title></titleInfo><titleInfo type="abbreviated"><title>TET</title></titleInfo><genre type="journal" authority="ISTEX" authorityURI="https://publication-type.data.istex.fr" valueURI="https://publication-type.data.istex.fr/ark:/67375/JMC-0GLKJH51-B">journal</genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">19970217</dateIssued></originInfo><identifier type="ISSN">0040-4020</identifier><identifier type="PII">S0040-4020(00)X0077-4</identifier><part><date>19970217</date><detail type="volume"><number>53</number><caption>vol.</caption></detail><detail type="issue"><number>7</number><caption>no.</caption></detail><extent unit="issue-pages"><start>2323</start><end>2666</end></extent><extent unit="pages"><start>2585</start><end>2590</end></extent></part></relatedItem><identifier type="istex">F0CDEDF102188BA3FF7A583AF06729DBC7396CBD</identifier><identifier type="ark">ark:/67375/6H6-SMH2P28D-9</identifier><identifier type="DOI">10.1016/S0040-4020(96)01148-9</identifier><identifier type="PII">S0040-4020(96)01148-9</identifier><recordInfo><recordContentSource authority="ISTEX" authorityURI="https://loaded-corpus.data.istex.fr" valueURI="https://loaded-corpus.data.istex.fr/ark:/67375/XBH-HKKZVM7B-M">elsevier</recordContentSource></recordInfo></mods><json:item><extension>json</extension><original>false</original><mimetype>application/json</mimetype><uri>https://api.istex.fr/document/F0CDEDF102188BA3FF7A583AF06729DBC7396CBD/metadata/json</uri></json:item></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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