Voltammetric determination of Ioxynil and 2-methyl-3-nitroaniline using C18 modified carbon paste electrodes
Identifieur interne : 002C15 ( Main/Merge ); précédent : 002C14; suivant : 002C16Voltammetric determination of Ioxynil and 2-methyl-3-nitroaniline using C18 modified carbon paste electrodes
Auteurs : Christine Faller [Allemagne] ; Axel Meyer [Allemagne] ; Günter Henze [Allemagne]Source :
- Fresenius' Journal of Analytical Chemistry [ 0937-0633 ] ; 1996-09-01.
Abstract
Abstract: The stripping voltammetric behaviour of Ioxynil and 2-methyl-3-nitroaniline has been studied by means of a C18 modified carbon paste electrode. The analytes are preconcentrated under open-circuit conditions (Ioxynil at pH 3.9; 2-methyl-3-nitroaniline at pH 10). For the determination of Ioxynil and 2-methyl-3-nitroaniline 0.01 mol/l HCl and 1 mol/l KOH, respectively, have been used as supporting electrolyte. Under optimized conditions detection limits up to 0.1 μg/ml Ioxynil and 0.3 μg/ml 2-methyl-3-nitroaniline have been obtained. The methods have been applied to the determination of Ioxynil and 2-methyl-3-nitroaniline in drinking water.
Url:
DOI: 10.1007/s0021663560279
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<front><div type="abstract" xml:lang="en">Abstract: The stripping voltammetric behaviour of Ioxynil and 2-methyl-3-nitroaniline has been studied by means of a C18 modified carbon paste electrode. The analytes are preconcentrated under open-circuit conditions (Ioxynil at pH 3.9; 2-methyl-3-nitroaniline at pH 10). For the determination of Ioxynil and 2-methyl-3-nitroaniline 0.01 mol/l HCl and 1 mol/l KOH, respectively, have been used as supporting electrolyte. Under optimized conditions detection limits up to 0.1 μg/ml Ioxynil and 0.3 μg/ml 2-methyl-3-nitroaniline have been obtained. The methods have been applied to the determination of Ioxynil and 2-methyl-3-nitroaniline in drinking water.</div>
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