Liquid-Chromatographie von Alkoholen auf mikrokristalliner Cellulose
Identifieur interne : 003605 ( Main/Exploration ); précédent : 003604; suivant : 003606Liquid-Chromatographie von Alkoholen auf mikrokristalliner Cellulose
Auteurs : Egon Stahl [Allemagne] ; Ernst Laub [Allemagne] ; Richard Woller [Allemagne]Source :
- Fresenius' Zeitschrift für analytische Chemie [ 0016-1152 ] ; 1975-01-01.
Abstract
Abstract: In “liquid chromatography” (LC), a stationary phase of microcrystalline cellulose is suitable for the separation of polyhydric alcohols such as glycerine, ethylene glycol, propane diol and butane diol when using a solvent mixture of ethyl acetate and n-propanol, saturated with approx. 15% of water. When using benzene as solvent, the monohydric alcohols C1-C5 can also be separated on the same column. Differential refractometers and micro adsorption detectors are suitable for detection.
Url:
DOI: 10.1007/BF00429369
Affiliations:
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Anal. Chem.</title><idno type="ISSN">0016-1152</idno><idno type="eISSN">1618-2650</idno><imprint><publisher>Springer-Verlag</publisher><pubPlace>Berlin/Heidelberg</pubPlace><date type="published" when="1975-01-01">1975-01-01</date><biblScope unit="volume">275</biblScope><biblScope unit="issue">4</biblScope><biblScope unit="page" from="257">257</biblScope><biblScope unit="page" to="260">260</biblScope></imprint><idno type="ISSN">0016-1152</idno></series><idno type="istex">B925952814E5DDC381DED3EE42B8B2F969E8C4D1</idno><idno type="DOI">10.1007/BF00429369</idno><idno type="ArticleID">BF00429369</idno><idno type="ArticleID">Art1</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0016-1152</idno></seriesStmt></fileDesc><profileDesc><textClass></textClass><langUsage><language ident="de">de</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: In “liquid chromatography” (LC), a stationary phase of microcrystalline cellulose is suitable for the separation of polyhydric alcohols such as glycerine, ethylene glycol, propane diol and butane diol when using a solvent mixture of ethyl acetate and n-propanol, saturated with approx. 15% of water. When using benzene as solvent, the monohydric alcohols C1-C5 can also be separated on the same column. 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