Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent
Identifieur interne : 000974 ( Istex/Corpus ); précédent : 000973; suivant : 000975Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent
Auteurs : Sylvia Sander ; Günter HenzeSource :
- Fresenius' Journal of Analytical Chemistry [ 0937-0633 ] ; 1994-08-01.
Abstract
Abstract: Uranium (VI) can be determined by adsorptive voltammetric techniques, as its chloranilic acid complex, over a wide concentration range. Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.
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DOI: 10.1007/BF00323474
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ISTEX:7F372AB8F9051371A929416A7FD5D9EC1DA2EF28Le document en format XML
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Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.</div></front></TEI><istex><corpusName>springer</corpusName><author><json:item><name>Sylvia Sander</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</json:string></affiliations></json:item><json:item><name>Günter Henze</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</json:string></affiliations></json:item></author><articleId><json:string>BF00323474</json:string><json:string>Art19</json:string></articleId><language><json:string>eng</json:string></language><originalGenre><json:string>OriginalPaper</json:string></originalGenre><abstract>Abstract: Uranium (VI) can be determined by adsorptive voltammetric techniques, as its chloranilic acid complex, over a wide concentration range. Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.</abstract><qualityIndicators><score>3.948</score><pdfVersion>1.3</pdfVersion><pdfPageSize>598 x 785 pts</pdfPageSize><refBibsNative>false</refBibsNative><keywordCount>0</keywordCount><abstractCharCount>796</abstractCharCount><pdfWordCount>2520</pdfWordCount><pdfCharCount>15612</pdfCharCount><pdfPageCount>5</pdfPageCount><abstractWordCount>119</abstractWordCount></qualityIndicators><title>Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent</title><refBibs><json:item><host><author><json:item><name>G Henze</name></json:item><json:item><name>R Neeb</name></json:item></author><title>Elektrochemische Analytik</title><publicationDate>1986</publicationDate></host></json:item><json:item><host><author><json:item><name>R Neeb</name></json:item></author><title>Inverse Polarographie und 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Page</name></json:item><json:item><name>G Van Loon</name></json:item></author><host><volume>65</volume><pages><first>1139</first></pages><author></author><title>Can J Chem</title><publicationDate>1987</publicationDate></host><publicationDate>1987</publicationDate></json:item><json:item><author><json:item><name>M Karakaplan</name></json:item><json:item><name>G Henze</name></json:item></author><host><volume>352</volume><pages><first>186</first></pages><author></author><title>Fresenius J Anal Chem</title><publicationDate>1992</publicationDate></host><publicationDate>1992</publicationDate></json:item><json:item><host><author><json:item><name>S Sander</name></json:item></author><publicationDate>1992</publicationDate></host></json:item></refBibs><genre><json:string>research-article</json:string></genre><host><volume>349</volume><pages><last>658</last><first>654</first></pages><issn><json:string>0937-0633</json:string></issn><issue>8-9</issue><subject><json:item><value>Analytical 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reagent</title><respStmt><resp>Références bibliographiques récupérées via GROBID</resp><name resp="ISTEX-API">ISTEX-API (INIST-CNRS)</name></respStmt><respStmt><resp>Références bibliographiques récupérées via GROBID</resp><name resp="ISTEX-API">ISTEX-API (INIST-CNRS)</name></respStmt></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>Springer-Verlag</publisher><pubPlace>Berlin/Heidelberg</pubPlace><availability><p>Springer-Verlag, 1994</p></availability><date>1993-07-31</date></publicationStmt><notesStmt><note>Lectures And Posters</note></notesStmt><sourceDesc><biblStruct type="inbook"><analytic><title level="a" type="main" xml:lang="en">Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent</title><author xml:id="author-1"><persName><forename type="first">Sylvia</forename><surname>Sander</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</affiliation></author><author xml:id="author-2" corresp="yes"><persName><forename type="first">Günter</forename><surname>Henze</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</affiliation></author></analytic><monogr><title level="j">Fresenius' Journal of Analytical Chemistry</title><title level="j" type="abbrev">Fresenius J Anal Chem</title><idno type="journal-ID">216</idno><idno type="pISSN">0937-0633</idno><idno type="eISSN">1432-1130</idno><idno type="issue-article-count">29</idno><idno type="volume-issue-count">12</idno><imprint><publisher>Springer-Verlag</publisher><pubPlace>Berlin/Heidelberg</pubPlace><date type="published" when="1994-08-01"></date><biblScope unit="volume">349</biblScope><biblScope unit="issue">8-9</biblScope><biblScope unit="page" from="654">654</biblScope><biblScope unit="page" to="658">658</biblScope></imprint></monogr><idno type="istex">7F372AB8F9051371A929416A7FD5D9EC1DA2EF28</idno><idno type="DOI">10.1007/BF00323474</idno><idno type="ArticleID">BF00323474</idno><idno type="ArticleID">Art19</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1993-07-31</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>Abstract: Uranium (VI) can be determined by adsorptive voltammetric techniques, as its chloranilic acid complex, over a wide concentration range. Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.</p></abstract><textClass><keywords scheme="Journal Subject"><list><head>Chemistry</head><item><term>Analytical Chemistry</term></item><item><term>Food Science</term></item><item><term>Inorganic Chemistry</term></item><item><term>Physical Chemistry</term></item><item><term>Monitoring/Environmental Analysis/Environmental Ecotoxicology</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="1993-07-31">Created</change><change when="1994-08-01">Published</change><change xml:id="refBibs-istex" who="#ISTEX-API" when="2016-11-22">References added</change><change xml:id="refBibs-istex" who="#ISTEX-API" when="2017-01-20">References 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II-III</DateString><Year>1994</Year><Month>8</Month></CoverDate></IssueHistory><IssueCopyright><CopyrightHolderName>Springer-Verlag</CopyrightHolderName><CopyrightYear>1994</CopyrightYear></IssueCopyright></IssueInfo><Article ID="Art19"><ArticleInfo Language="En" ArticleType="OriginalPaper" NumberingStyle="Unnumbered" TocLevels="0" ContainsESM="No"><ArticleID>BF00323474</ArticleID><ArticleDOI>10.1007/BF00323474</ArticleDOI><ArticleSequenceNumber>19</ArticleSequenceNumber><ArticleTitle Language="En">Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent</ArticleTitle><ArticleCategory>Lectures And Posters</ArticleCategory><ArticleFirstPage>654</ArticleFirstPage><ArticleLastPage>658</ArticleLastPage><ArticleHistory><RegistrationDate><Year>2004</Year><Month>8</Month><Day>27</Day></RegistrationDate><Received><Year>1993</Year><Month>7</Month><Day>31</Day></Received></ArticleHistory><ArticleCopyright><CopyrightHolderName>Springer-Verlag</CopyrightHolderName><CopyrightYear>1994</CopyrightYear></ArticleCopyright><ArticleGrants Type="Regular"><MetadataGrant Grant="OpenAccess"></MetadataGrant><AbstractGrant Grant="OpenAccess"></AbstractGrant><BodyPDFGrant Grant="Restricted"></BodyPDFGrant><BodyHTMLGrant Grant="Restricted"></BodyHTMLGrant><BibliographyGrant Grant="Restricted"></BibliographyGrant><ESMGrant Grant="Restricted"></ESMGrant></ArticleGrants><ArticleContext><JournalID>216</JournalID><VolumeIDStart>349</VolumeIDStart><VolumeIDEnd>349</VolumeIDEnd><IssueIDStart>8</IssueIDStart><IssueIDEnd>9</IssueIDEnd></ArticleContext></ArticleInfo><ArticleHeader><AuthorGroup><Author AffiliationIDS="Aff1"><AuthorName DisplayOrder="Western"><GivenName>Sylvia</GivenName><FamilyName>Sander</FamilyName></AuthorName></Author><Author AffiliationIDS="Aff1" CorrespondingAffiliationID="Aff1"><AuthorName DisplayOrder="Western"><GivenName>Günter</GivenName><FamilyName>Henze</FamilyName></AuthorName></Author><Affiliation ID="Aff1"><OrgDivision>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie</OrgDivision><OrgName>Universität Trier</OrgName><OrgAddress><Postbox>Postfach 3825</Postbox><Postcode>D-54228</Postcode><City>Trier</City><Country>Germany</Country></OrgAddress></Affiliation></AuthorGroup><Abstract ID="Abs1" Language="En"><Heading>Abstract</Heading><Para>Uranium (VI) can be determined by adsorptive voltammetric techniques, as its chloranilic acid complex, over a wide concentration range. Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.</Para></Abstract><ArticleNote Type="Dedication"><SimplePara>Dedicated to Professor R. Geyer on the occasion of his 80th birthday</SimplePara></ArticleNote></ArticleHeader><NoBody></NoBody></Article></Issue></Volume></Journal></Publisher></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Adsorption voltammetric techniques for the determination of uranium(VI) with 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone as complex forming reagent</title></titleInfo><name type="personal"><namePart type="given">Sylvia</namePart><namePart type="family">Sander</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal" displayLabel="corresp"><namePart type="given">Günter</namePart><namePart type="family">Henze</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54228, Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="OriginalPaper"></genre><originInfo><publisher>Springer-Verlag</publisher><place><placeTerm type="text">Berlin/Heidelberg</placeTerm></place><dateCreated encoding="w3cdtf">1993-07-31</dateCreated><dateIssued encoding="w3cdtf">1994-08-01</dateIssued><copyrightDate encoding="w3cdtf">1994</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">Abstract: Uranium (VI) can be determined by adsorptive voltammetric techniques, as its chloranilic acid complex, over a wide concentration range. Differential pulse polarography is useful for quantification of uranium between 0.1 and 1.5 mg/l; for the range from 10 to 500 μg/l differential pulse voltammetry and for ultra-trace analysis between 0.024 and 40 μg/l adsorptive stripping voltammetry are preferred. The standard deviation for the 3σ-detection limit of 24 ng/l uranium was found to be 8%. In the trace analysis of metals in aquatic environmental systems by adsorptive stripping voltammetry it is normally necessary to decompose polluted water samples by UV irradiation or microwave digestion. The advantage of the developed method is the fact that no sample pretreatment is necessary.</abstract><note>Lectures And Posters</note><relatedItem type="host"><titleInfo><title>Fresenius' Journal of Analytical Chemistry</title></titleInfo><titleInfo type="abbreviated"><title>Fresenius J Anal Chem</title></titleInfo><genre type="journal" displayLabel="Archive Journal"></genre><originInfo><dateIssued encoding="w3cdtf">1994-08-01</dateIssued><copyrightDate encoding="w3cdtf">1994</copyrightDate></originInfo><subject><genre>Chemistry</genre><topic>Analytical Chemistry</topic><topic>Food Science</topic><topic>Inorganic Chemistry</topic><topic>Physical Chemistry</topic><topic>Monitoring/Environmental Analysis/Environmental Ecotoxicology</topic></subject><identifier type="ISSN">0937-0633</identifier><identifier type="eISSN">1432-1130</identifier><identifier type="JournalID">216</identifier><identifier type="IssueArticleCount">29</identifier><identifier type="VolumeIssueCount">12</identifier><part><date>1994</date><detail type="volume"><number>349</number><caption>vol.</caption></detail><detail type="issue"><number>8-9</number><caption>no.</caption></detail><extent unit="pages"><start>654</start><end>658</end></extent></part><recordInfo><recordOrigin>Springer-Verlag, 1994</recordOrigin></recordInfo></relatedItem><identifier type="istex">7F372AB8F9051371A929416A7FD5D9EC1DA2EF28</identifier><identifier type="DOI">10.1007/BF00323474</identifier><identifier type="ArticleID">BF00323474</identifier><identifier type="ArticleID">Art19</identifier><accessCondition type="use and reproduction" contentType="copyright">Springer-Verlag, 1994</accessCondition><recordInfo><recordContentSource>SPRINGER</recordContentSource><recordOrigin>Springer-Verlag, 1994</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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