Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection
Identifieur interne : 000850 ( Istex/Corpus ); précédent : 000849; suivant : 000851Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection
Auteurs : H.-P. Nirmaier ; E. Fischer ; A. Meyer ; G. HenzeSource :
- Journal of Chromatography A [ 0021-9673 ] ; 1996.
Abstract
The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).
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DOI: 10.1016/0021-9673(95)01143-9
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Fischer</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Meyer, A" sort="Meyer, A" uniqKey="Meyer A" first="A." last="Meyer">A. Meyer</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, G" sort="Henze, G" uniqKey="Henze G" first="G." last="Henze">G. Henze</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0</idno><date when="1996" year="1996">1996</date><idno type="doi">10.1016/0021-9673(95)01143-9</idno><idno type="url">https://api.istex.fr/document/2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">000850</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000850</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a">Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title><author><name sortKey="Nirmaier, H P" sort="Nirmaier, H P" uniqKey="Nirmaier H" first="H.-P." last="Nirmaier">H.-P. Nirmaier</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Fischer, E" sort="Fischer, E" uniqKey="Fischer E" first="E." last="Fischer">E. Fischer</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Meyer, A" sort="Meyer, A" uniqKey="Meyer A" first="A." last="Meyer">A. Meyer</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, G" sort="Henze, G" uniqKey="Henze G" first="G." last="Henze">G. Henze</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Journal of Chromatography A</title><title level="j" type="abbrev">CHROMA</title><idno type="ISSN">0021-9673</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1996">1996</date><biblScope unit="volume">730</biblScope><biblScope unit="issue">1–2</biblScope><biblScope unit="page" from="169">169</biblScope><biblScope unit="page" to="175">175</biblScope></imprint><idno type="ISSN">0021-9673</idno></series><idno type="istex">2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0</idno><idno type="DOI">10.1016/0021-9673(95)01143-9</idno><idno type="PII">0021-9673(95)01143-9</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0021-9673</idno></seriesStmt></fileDesc><profileDesc><textClass></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).</div></front></TEI><istex><corpusName>elsevier</corpusName><author><json:item><name>H.-P. Nirmaier</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</json:string></affiliations></json:item><json:item><name>E. Fischer</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</json:string></affiliations></json:item><json:item><name>A. Meyer</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</json:string></affiliations></json:item><json:item><name>G. Henze</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>Miscellaneous applications</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Environmental analysis</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Water analysis</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Solid-phase extraction</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Detectors, LC</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Polynuclear aromatic hydrocarbons</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Trichloroacetic acid</value></json:item></subject><language><json:string>eng</json:string></language><originalGenre><json:string>Full-length article</json:string></originalGenre><abstract>The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).</abstract><qualityIndicators><score>3.451</score><pdfVersion>1.2</pdfVersion><pdfPageSize>576 x 720 pts</pdfPageSize><refBibsNative>true</refBibsNative><keywordCount>7</keywordCount><abstractCharCount>840</abstractCharCount><pdfWordCount>2011</pdfWordCount><pdfCharCount>15992</pdfCharCount><pdfPageCount>7</pdfPageCount><abstractWordCount>120</abstractWordCount></qualityIndicators><title>Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title><pii><json:string>0021-9673(95)01143-9</json:string></pii><refBibs><json:item><host><volume>1</volume><pages><first>747</first></pages><author></author><title>J. Environ. Path. 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Chem.</title></host></json:item><json:item><host><author></author><title>Statistische Methoden in der Wasseranalytik</title></host></json:item></refBibs><genre><json:string>research-article</json:string></genre><host><volume>730</volume><pii><json:string>S0021-9673(00)X0010-6</json:string></pii><pages><last>175</last><first>169</first></pages><conference><json:item><name>19th International Symposium on Column Liquid Chromatography, Innsbruck 19950528 19950602</name></json:item></conference><issn><json:string>0021-9673</json:string></issn><issue>1–2</issue><genre><json:string>journal</json:string></genre><language><json:string>unknown</json:string></language><title>Journal of Chromatography A</title><publicationDate>1996</publicationDate></host><categories><wos><json:string>science</json:string><json:string>chemistry, analytical</json:string><json:string>biochemical research methods</json:string></wos><scienceMetrix><json:string>natural sciences</json:string><json:string>chemistry</json:string><json:string>analytical chemistry</json:string></scienceMetrix></categories><publicationDate>1996</publicationDate><copyrightDate>1996</copyrightDate><doi><json:string>10.1016/0021-9673(95)01143-9</json:string></doi><id>2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0</id><score>0.6792904</score><fulltext><json:item><extension>pdf</extension><original>true</original><mimetype>application/pdf</mimetype><uri>https://api.istex.fr/document/2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0/fulltext/pdf</uri></json:item><json:item><extension>zip</extension><original>false</original><mimetype>application/zip</mimetype><uri>https://api.istex.fr/document/2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0/fulltext/zip</uri></json:item><istex:fulltextTEI uri="https://api.istex.fr/document/2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0/fulltext/tei"><teiHeader><fileDesc><titleStmt><title level="a">Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>ELSEVIER</publisher><availability><p>ELSEVIER</p></availability><date>1996</date></publicationStmt><sourceDesc><biblStruct type="inbook"><analytic><title level="a">Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title><author xml:id="author-1"><persName><forename type="first">H.-P.</forename><surname>Nirmaier</surname></persName><note type="correspondence"><p>Corresponding author.</p></note><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation></author><author xml:id="author-2"><persName><forename type="first">E.</forename><surname>Fischer</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation></author><author xml:id="author-3"><persName><forename type="first">A.</forename><surname>Meyer</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation></author><author xml:id="author-4"><persName><forename type="first">G.</forename><surname>Henze</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation></author></analytic><monogr><title level="j">Journal of Chromatography A</title><title level="j" type="abbrev">CHROMA</title><idno type="pISSN">0021-9673</idno><idno type="PII">S0021-9673(00)X0010-6</idno><meeting><addName>19th International Symposium on Column Liquid Chromatography, Innsbruck</addName><date>19950528</date><date>19950602</date></meeting><imprint><publisher>ELSEVIER</publisher><date type="published" when="1996"></date><biblScope unit="volume">730</biblScope><biblScope unit="issue">1–2</biblScope><biblScope unit="page" from="169">169</biblScope><biblScope unit="page" to="175">175</biblScope></imprint></monogr><idno type="istex">2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0</idno><idno type="DOI">10.1016/0021-9673(95)01143-9</idno><idno type="PII">0021-9673(95)01143-9</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1996</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).</p></abstract><textClass><keywords scheme="keyword"><list><head>article-category</head><item><term>Miscellaneous applications</term></item></list></keywords></textClass><textClass><keywords scheme="keyword"><list><head>Keywords</head><item><term>Environmental analysis</term></item><item><term>Water analysis</term></item><item><term>Solid-phase extraction</term></item><item><term>Detectors, LC</term></item><item><term>Polynuclear aromatic hydrocarbons</term></item><item><term>Trichloroacetic acid</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="1996">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><extension>txt</extension><original>false</original><mimetype>text/plain</mimetype><uri>https://api.istex.fr/document/2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Elsevier, elements deleted: tail"><istex:xmlDeclaration>version="1.0" encoding="utf-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//ES//DTD journal article DTD version 4.5.2//EN//XML" URI="art452.dtd" name="istex:docType"></istex:docType><istex:document><converted-article version="4.5.2" docsubtype="fla"><item-info><jid>CHROMA</jid><aid>95011439</aid><ce:pii>0021-9673(95)01143-9</ce:pii><ce:doi>10.1016/0021-9673(95)01143-9</ce:doi><ce:copyright type="unknown" year="1996"></ce:copyright><ce:doctopics><ce:doctopic><ce:text>Miscellaneous applications</ce:text></ce:doctopic></ce:doctopics></item-info><head><ce:title>Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</ce:title><ce:author-group><ce:author><ce:given-name>H.-P.</ce:given-name><ce:surname>Nirmaier</ce:surname><ce:cross-ref refid="COR1"><ce:sup>∗</ce:sup></ce:cross-ref></ce:author><ce:author><ce:given-name>E.</ce:given-name><ce:surname>Fischer</ce:surname></ce:author><ce:author><ce:given-name>A.</ce:given-name><ce:surname>Meyer</ce:surname></ce:author><ce:author><ce:given-name>G.</ce:given-name><ce:surname>Henze</ce:surname></ce:author><ce:affiliation><ce:textfn>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</ce:textfn></ce:affiliation><ce:correspondence id="COR1"><ce:label>∗</ce:label><ce:text>Corresponding author.</ce:text></ce:correspondence></ce:author-group><ce:abstract><ce:section-title>Abstract</ce:section-title><ce:abstract-sec><ce:simple-para>The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).</ce:simple-para></ce:abstract-sec></ce:abstract><ce:keywords><ce:section-title>Keywords</ce:section-title><ce:keyword><ce:text>Environmental analysis</ce:text></ce:keyword><ce:keyword><ce:text>Water analysis</ce:text></ce:keyword><ce:keyword><ce:text>Solid-phase extraction</ce:text></ce:keyword><ce:keyword><ce:text>Detectors, LC</ce:text></ce:keyword><ce:keyword><ce:text>Polynuclear aromatic hydrocarbons</ce:text></ce:keyword><ce:keyword><ce:text>Trichloroacetic acid</ce:text></ce:keyword></ce:keywords></head></converted-article></istex:document></istex:metadataXml><mods version="3.6"><titleInfo><title>Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title></titleInfo><titleInfo type="alternative" contentType="CDATA"><title>Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection</title></titleInfo><name type="personal"><namePart type="given">H.-P.</namePart><namePart type="family">Nirmaier</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation><description>Corresponding author.</description><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">E.</namePart><namePart type="family">Fischer</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">A.</namePart><namePart type="family">Meyer</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">G.</namePart><namePart type="family">Henze</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, und Abteilung Anorganische and Analytische Chemie, Universität Trier, Posyach 3825, D-54228 Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="Full-length article"></genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">1996</dateIssued><copyrightDate encoding="w3cdtf">1996</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm><languageTerm type="code" authority="rfc3066">en</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">The determination of polycyclic aromatic hydrocarbons (PAHs) using high-performance liquid chromatography (HPLC) with UV and fluorescence detection has been well established. Although most of the PAHs can be detected by these methods, some environmentally important polyaromatic compounds, such as acenaphthylene, do not show fluorescence and can only be determined by UV detection at higher concentrations. A sensitive and selective determination of acenaphthylene, acenaphthene and the six PAHs listed in the TVO, the German drinking water standard, is also possible by amperometric detection following HPLC separation. The method was applied to the determination of PAHs in different water samples after solid-phase extraction (SPE). The efficiency of the amperometric determination was found to be superior to UV detection (λ = 300 nm).</abstract><subject><genre>article-category</genre><topic>Miscellaneous applications</topic></subject><subject><genre>Keywords</genre><topic>Environmental analysis</topic><topic>Water analysis</topic><topic>Solid-phase extraction</topic><topic>Detectors, LC</topic><topic>Polynuclear aromatic hydrocarbons</topic><topic>Trichloroacetic acid</topic></subject><relatedItem type="host"><titleInfo><title>Journal of Chromatography A</title></titleInfo><titleInfo type="abbreviated"><title>CHROMA</title></titleInfo><name type="conference"><namePart>19th International Symposium on Column Liquid Chromatography, Innsbruck</namePart><namePart type="date">19950528</namePart><namePart type="date">19950602</namePart></name><genre type="journal">journal</genre><originInfo><dateIssued encoding="w3cdtf">19960412</dateIssued></originInfo><identifier type="ISSN">0021-9673</identifier><identifier type="PII">S0021-9673(00)X0010-6</identifier><part><date>19960412</date><detail type="issue"><title>19th International Symposium on Column Liquid Chromatography, Innsbruck</title></detail><detail type="volume"><number>730</number><caption>vol.</caption></detail><detail type="issue"><number>1–2</number><caption>no.</caption></detail><extent unit="issue pages"><start>1</start><end>403</end></extent><extent unit="pages"><start>169</start><end>175</end></extent></part></relatedItem><identifier type="istex">2259A5F07AD37EB3DF0A27A863775EEF09ED1DA0</identifier><identifier type="DOI">10.1016/0021-9673(95)01143-9</identifier><identifier type="PII">0021-9673(95)01143-9</identifier><recordInfo><recordContentSource>ELSEVIER</recordContentSource></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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|texte= Determination of polycyclic aromatic hydrocarbons in water samples using high-performance liquid chromatography with amperometric detection
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