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Determination of zinc, cadmium, lead and copper in soils and sewage sludges by microprocessor-controlled voltammetry in comparison with atomic absorption spectrometry

Identifieur interne : 000818 ( Istex/Corpus ); précédent : 000817; suivant : 000819

Determination of zinc, cadmium, lead and copper in soils and sewage sludges by microprocessor-controlled voltammetry in comparison with atomic absorption spectrometry

Auteurs : Axel Meyer ; Ulrike De La Chevallerie-Haaf ; Günter Henze

Source :

RBID : ISTEX:83773E903C38D35EADA6DB4882B5E740322760F1

Abstract

Summary: Information on the heavy metal contents in soils and sewage sludges is of strong ecological interest. For control of the maximum allowed concentrations photometric and atomic absorption spectrometric methods have been developed for the determination of the single elements; sample digestion is carried out using hydrochloric acid and nitric acid. Differential pulse polarography and differential pulse anodic stripping voltammetry allow the simultaneous determination of different heavy metals in one digestion solution according to their electrochemical behaviour. This possibility is given, for instance, for zinc, cadmium, lead and copper. The adequate procedure was tested with a microprocessor-controlled polarograph. Flame atomic absorption spectrometry was used as reference method.

Url:
DOI: 10.1007/BF00468969

Links to Exploration step

ISTEX:83773E903C38D35EADA6DB4882B5E740322760F1

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<Heading>Summary</Heading>
<Para>Information on the heavy metal contents in soils and sewage sludges is of strong ecological interest. For control of the maximum allowed concentrations photometric and atomic absorption spectrometric methods have been developed for the determination of the single elements; sample digestion is carried out using hydrochloric acid and nitric acid.</Para>
<Para>Differential pulse polarography and differential pulse anodic stripping voltammetry allow the simultaneous determination of different heavy metals in one digestion solution according to their electrochemical behaviour. This possibility is given, for instance, for zinc, cadmium, lead and copper. The adequate procedure was tested with a microprocessor-controlled polarograph. Flame atomic absorption spectrometry was used as reference method.</Para>
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<title>Determination of zinc, cadmium, lead and copper in soils and sewage sludges by microprocessor-controlled voltammetry in comparison with atomic absorption spectrometry</title>
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<title>Determination of zinc, cadmium, lead and copper in soils and sewage sludges by microprocessor-controlled voltammetry in comparison with atomic absorption spectrometry</title>
</titleInfo>
<titleInfo lang="de">
<title>Bestimmung von Zink, Cadmium, Blei und Kupfer in Böden und Klärschlämmen durch mikroprozessorgesteuerte Voltammetrie im Vergleich mit der Atomabsorptionsspektrometrie</title>
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<title>Bestimmung von Zink, Cadmium, Blei und Kupfer in Böden und Klärschlämmen durch mikroprozessorgesteuerte Voltammetrie im Vergleich mit der Atomabsorptionsspektrometrie</title>
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<name type="personal">
<namePart type="given">Axel</namePart>
<namePart type="family">Meyer</namePart>
<affiliation>Department of Inorganic and Analytical Chemistry, University of Trier, P. O. Box 3825, D-5500, Trier, Federal Republic of Germany</affiliation>
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<name type="personal">
<namePart type="given">Ulrike</namePart>
<namePart type="family">de la Chevallerie-Haaf</namePart>
<affiliation>Department of Inorganic and Analytical Chemistry, University of Trier, P. O. Box 3825, D-5500, Trier, Federal Republic of Germany</affiliation>
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<namePart type="given">Günter</namePart>
<namePart type="family">Henze</namePart>
<affiliation>Department of Inorganic and Analytical Chemistry, University of Trier, P. O. Box 3825, D-5500, Trier, Federal Republic of Germany</affiliation>
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<dateCreated encoding="w3cdtf">1987-05-02</dateCreated>
<dateIssued encoding="w3cdtf">1987-01-01</dateIssued>
<copyrightDate encoding="w3cdtf">1987</copyrightDate>
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<abstract lang="en">Summary: Information on the heavy metal contents in soils and sewage sludges is of strong ecological interest. For control of the maximum allowed concentrations photometric and atomic absorption spectrometric methods have been developed for the determination of the single elements; sample digestion is carried out using hydrochloric acid and nitric acid. Differential pulse polarography and differential pulse anodic stripping voltammetry allow the simultaneous determination of different heavy metals in one digestion solution according to their electrochemical behaviour. This possibility is given, for instance, for zinc, cadmium, lead and copper. The adequate procedure was tested with a microprocessor-controlled polarograph. Flame atomic absorption spectrometry was used as reference method.</abstract>
<note>Original Papers/Environmental Analysis</note>
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<title>Z. Anal. Chem.</title>
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<dateIssued encoding="w3cdtf">1987-01-01</dateIssued>
<copyrightDate encoding="w3cdtf">1987</copyrightDate>
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<subject>
<genre>Chemistry</genre>
<topic>Analytical Chemistry</topic>
<topic>Food Science</topic>
<topic>Inorganic Chemistry</topic>
<topic>Physical Chemistry</topic>
<topic>Monitoring/Environmental Analysis/Environmental Ecotoxicology</topic>
</subject>
<identifier type="ISSN">0016-1152</identifier>
<identifier type="eISSN">1618-2650</identifier>
<identifier type="JournalID">216</identifier>
<identifier type="IssueArticleCount">27</identifier>
<identifier type="VolumeIssueCount">8</identifier>
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<date>1987</date>
<detail type="volume">
<number>328</number>
<caption>vol.</caption>
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<detail type="issue">
<number>7</number>
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<start>565</start>
<end>568</end>
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