Application of adsorptive stripping voltammetry to trace measurements of molybdenum in plant materials
Identifieur interne : 000812 ( Istex/Corpus ); précédent : 000811; suivant : 000813Application of adsorptive stripping voltammetry to trace measurements of molybdenum in plant materials
Auteurs : Mustafa Karakaplan ; Günter HenzeSource :
- Electroanalysis [ 1040-0397 ] ; 1993-08.
English descriptors
Abstract
A procedure is presented for quantifying molybdenum in dry ashed plant samples. The determination is made by adsorptive stripping voltammetry in the differential pulse mode (DPAdSV). It is based on the adsorptive accumulation of the Mo(VI)‐chloranilic acid complex on the surface of a hanging mercury drop, followed by the reduction of the adsorbed complex. Optimal conditions are stirred acidified supporting electrolyte solution (of pH 2–3), containing 10−3 mol/L chloranilic acid and an accumulation potential of −0.20 V (vs. Ag/AgCl, 3 mol/L KCl). The height of the cathodic stripping peak around −0.60 V depends linearly on the molybdenum concentration and accumulation time (over the ranges 0–12 ng/ml and 0–300 seconds, respectively). For an accumulation period of 5 minutes, the detection limit is 0.02 ng/ml. Possible interferences by other trace metals are investigated. The proposed procedure has been applied to the determination of molybdenum traces in a variety of plants with good accuracy and precision. The results are in good agreement with those obtained by atomic absorption spectrometry.
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DOI: 10.1002/elan.1140050717
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ISTEX:2B31C58C7422FCA11883F198E4D148D72AAA74B4Le document en format XML
<record><TEI wicri:istexFullTextTei="biblStruct"><teiHeader><fileDesc><titleStmt><title xml:lang="en">Application of adsorptive stripping voltammetry to trace measurements of molybdenum in plant materials</title><author><name sortKey="Karakaplan, Mustafa" sort="Karakaplan, Mustafa" uniqKey="Karakaplan M" first="Mustafa" last="Karakaplan">Mustafa Karakaplan</name><affiliation><mods:affiliation>Fachbereich Chemie der Universität Kaiserslautern und Abteilung für Anorganische und Analytische Chemie der Universität Trier, Postfach 3625, W‐5500 Trier, Federal Republic of Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, Gunter" sort="Henze, Gunter" uniqKey="Henze G" first="Günter" last="Henze">Günter Henze</name><affiliation><mods:affiliation>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</mods:affiliation></affiliation><affiliation><mods:affiliation>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:2B31C58C7422FCA11883F198E4D148D72AAA74B4</idno><date when="1993" year="1993">1993</date><idno type="doi">10.1002/elan.1140050717</idno><idno type="url">https://api.istex.fr/document/2B31C58C7422FCA11883F198E4D148D72AAA74B4/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">000812</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000812</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main" xml:lang="en">Application of adsorptive stripping voltammetry to trace measurements of molybdenum in plant materials</title><author><name sortKey="Karakaplan, Mustafa" sort="Karakaplan, Mustafa" uniqKey="Karakaplan M" first="Mustafa" last="Karakaplan">Mustafa Karakaplan</name><affiliation><mods:affiliation>Fachbereich Chemie der Universität Kaiserslautern und Abteilung für Anorganische und Analytische Chemie der Universität Trier, Postfach 3625, W‐5500 Trier, Federal Republic of Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, Gunter" sort="Henze, Gunter" uniqKey="Henze G" first="Günter" last="Henze">Günter Henze</name><affiliation><mods:affiliation>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</mods:affiliation></affiliation><affiliation><mods:affiliation>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Electroanalysis</title><title level="j" type="abbrev">Electroanalysis</title><idno type="ISSN">1040-0397</idno><idno type="eISSN">1521-4109</idno><imprint><publisher>VCH Verlagsgesellschaft mbH</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="1993-08">1993-08</date><biblScope unit="volume">5</biblScope><biblScope unit="issue">7</biblScope><biblScope unit="page" from="623">623</biblScope><biblScope unit="page" to="625">625</biblScope></imprint><idno type="ISSN">1040-0397</idno></series><idno type="istex">2B31C58C7422FCA11883F198E4D148D72AAA74B4</idno><idno type="DOI">10.1002/elan.1140050717</idno><idno type="ArticleID">ELAN1140050717</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1040-0397</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Adsorptive stripping voltammetry</term><term>Molybdenum</term><term>Plant materials</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A procedure is presented for quantifying molybdenum in dry ashed plant samples. The determination is made by adsorptive stripping voltammetry in the differential pulse mode (DPAdSV). It is based on the adsorptive accumulation of the Mo(VI)‐chloranilic acid complex on the surface of a hanging mercury drop, followed by the reduction of the adsorbed complex. Optimal conditions are stirred acidified supporting electrolyte solution (of pH 2–3), containing 10−3 mol/L chloranilic acid and an accumulation potential of −0.20 V (vs. Ag/AgCl, 3 mol/L KCl). The height of the cathodic stripping peak around −0.60 V depends linearly on the molybdenum concentration and accumulation time (over the ranges 0–12 ng/ml and 0–300 seconds, respectively). For an accumulation period of 5 minutes, the detection limit is 0.02 ng/ml. Possible interferences by other trace metals are investigated. The proposed procedure has been applied to the determination of molybdenum traces in a variety of plants with good accuracy and precision. The results are in good agreement with those obtained by atomic absorption spectrometry.</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Mustafa Karakaplan</name><affiliations><json:string>Fachbereich Chemie der Universität Kaiserslautern und Abteilung für Anorganische und Analytische Chemie der Universität Trier, Postfach 3625, W‐5500 Trier, Federal Republic of Germany</json:string></affiliations></json:item><json:item><name>GÜNter Henze</name><affiliations><json:string>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</json:string><json:string>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>Molybdenum</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Plant materials</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Adsorptive stripping voltammetry</value></json:item></subject><articleId><json:string>ELAN1140050717</json:string></articleId><language><json:string>eng</json:string></language><originalGenre><json:string>shortCommunication</json:string></originalGenre><abstract>A procedure is presented for quantifying molybdenum in dry ashed plant samples. The determination is made by adsorptive stripping voltammetry in the differential pulse mode (DPAdSV). It is based on the adsorptive accumulation of the Mo(VI)‐chloranilic acid complex on the surface of a hanging mercury drop, followed by the reduction of the adsorbed complex. Optimal conditions are stirred acidified supporting electrolyte solution (of pH 2–3), containing 10−3 mol/L chloranilic acid and an accumulation potential of −0.20 V (vs. Ag/AgCl, 3 mol/L KCl). The height of the cathodic stripping peak around −0.60 V depends linearly on the molybdenum concentration and accumulation time (over the ranges 0–12 ng/ml and 0–300 seconds, respectively). For an accumulation period of 5 minutes, the detection limit is 0.02 ng/ml. Possible interferences by other trace metals are investigated. The proposed procedure has been applied to the determination of molybdenum traces in a variety of plants with good accuracy and precision. 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affiliationRef="#af1"><personName><givenNames>Mustafa</givenNames><familyName>Karakaplan</familyName></personName></creator><creator xml:id="au2" creatorRole="author" affiliationRef="#af2" corresponding="yes"><personName><givenNames>GÜNter</givenNames><familyName>Henze</familyName></personName></creator></creators><affiliationGroup><affiliation xml:id="af1" countryCode="DE" type="organization"><unparsedAffiliation>Fachbereich Chemie der Universität Kaiserslautern und Abteilung für Anorganische und Analytische Chemie der Universität Trier, Postfach 3625, W‐5500 Trier, Federal Republic of Germany</unparsedAffiliation></affiliation><affiliation xml:id="af2" countryCode="TR" type="organization"><unparsedAffiliation>Inönü Üniversitesi, Fen‐Edebiyat Fakültesi, Kimya Bölümü, TR‐44069 Malatya, Turkey</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1">Molybdenum</keyword><keyword xml:id="kwd2">Plant materials</keyword><keyword xml:id="kwd3">Adsorptive stripping voltammetry</keyword></keywordGroup><abstractGroup><abstract type="main" xml:lang="en"><title type="main">Abstract</title><p>A procedure is presented for quantifying molybdenum in dry ashed plant samples. The determination is made by adsorptive stripping voltammetry in the differential pulse mode (DPAdSV). It is based on the adsorptive accumulation of the Mo(VI)‐chloranilic acid complex on the surface of a hanging mercury drop, followed by the reduction of the adsorbed complex. Optimal conditions are stirred acidified supporting electrolyte solution (of pH 2–3), containing 10<sup>−3</sup> mol/L chloranilic acid and an accumulation potential of −0.20 V (vs. Ag/AgCl, 3 mol/L KCl). The height of the cathodic stripping peak around −0.60 V depends linearly on the molybdenum concentration and accumulation time (over the ranges 0–12 ng/ml and 0–300 seconds, respectively). For an accumulation period of 5 minutes, the detection limit is 0.02 ng/ml. Possible interferences by other trace metals are investigated. The proposed procedure has been applied to the determination of molybdenum traces in a variety of plants with good accuracy and precision. 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The determination is made by adsorptive stripping voltammetry in the differential pulse mode (DPAdSV). It is based on the adsorptive accumulation of the Mo(VI)‐chloranilic acid complex on the surface of a hanging mercury drop, followed by the reduction of the adsorbed complex. Optimal conditions are stirred acidified supporting electrolyte solution (of pH 2–3), containing 10−3 mol/L chloranilic acid and an accumulation potential of −0.20 V (vs. Ag/AgCl, 3 mol/L KCl). The height of the cathodic stripping peak around −0.60 V depends linearly on the molybdenum concentration and accumulation time (over the ranges 0–12 ng/ml and 0–300 seconds, respectively). For an accumulation period of 5 minutes, the detection limit is 0.02 ng/ml. Possible interferences by other trace metals are investigated. The proposed procedure has been applied to the determination of molybdenum traces in a variety of plants with good accuracy and precision. The results are in good agreement with those obtained by atomic absorption spectrometry.</abstract><subject lang="en"><genre>keywords</genre><topic>Molybdenum</topic><topic>Plant materials</topic><topic>Adsorptive stripping voltammetry</topic></subject><relatedItem type="host"><titleInfo><title>Electroanalysis</title></titleInfo><titleInfo type="abbreviated"><title>Electroanalysis</title></titleInfo><genre type="journal">journal</genre><subject><genre>article-category</genre><topic>Short Communication</topic></subject><identifier type="ISSN">1040-0397</identifier><identifier type="eISSN">1521-4109</identifier><identifier type="DOI">10.1002/(ISSN)1521-4109</identifier><identifier type="PublisherID">ELAN</identifier><part><date>1993</date><detail type="volume"><caption>vol.</caption><number>5</number></detail><detail type="issue"><caption>no.</caption><number>7</number></detail><extent unit="pages"><start>623</start><end>625</end><total>3</total></extent></part></relatedItem><identifier type="istex">2B31C58C7422FCA11883F198E4D148D72AAA74B4</identifier><identifier type="DOI">10.1002/elan.1140050717</identifier><identifier type="ArticleID">ELAN1140050717</identifier><accessCondition type="use and reproduction" contentType="copyright">Copyright © 1993 VCH Publishers, Inc.</accessCondition><recordInfo><recordContentSource>WILEY</recordContentSource><recordOrigin>VCH Verlagsgesellschaft mbH</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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