Electropolymerized nanoporous polymeric SPME coatings: preparation and characterization by small angle X-ray scattering and scanning electron microscopy
Identifieur interne : 000047 ( Pmc/Curation ); précédent : 000046; suivant : 000048Electropolymerized nanoporous polymeric SPME coatings: preparation and characterization by small angle X-ray scattering and scanning electron microscopy
Auteurs : Boguslaw Buszewski [Pologne] ; Pawel Olszowy [Pologne] ; Stanislaw Pikus [Pologne] ; Maciej Kozak [Pologne]Source :
- Monatshefte Fur Chemie [ 0026-9247 ] ; 2014.
Abstract
Polymeric polypyrrole and polythiophene solid phase microextraction (SPME) coatings were prepared using electropolymerization with a linear sweep voltammetry technique. Physicochemical properties were measured using different methods, in particular small angle X-ray scattering and scanning electron microscopy. By using innovative approaches for pore size measurement, we were able to calculate a maximum of the pore size range from 80 to 90 nm. Additionally, film thicknesses measured from 90 to 150 μm. Using scanning electron microscopy, we describe the characteristics of polymer growth on the support surface.
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DOI: 10.1007/s00706-013-1115-3
PubMed: 26166891
PubMed Central: 4494846
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Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun</wicri:regionArea></affiliation></author><author><name sortKey="Pikus, Stanislaw" sort="Pikus, Stanislaw" uniqKey="Pikus S" first="Stanislaw" last="Pikus">Stanislaw Pikus</name><affiliation wicri:level="1"><nlm:aff id="Aff2">Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin</wicri:regionArea></affiliation></author><author><name sortKey="Kozak, Maciej" sort="Kozak, Maciej" uniqKey="Kozak M" first="Maciej" last="Kozak">Maciej Kozak</name><affiliation wicri:level="1"><nlm:aff id="Aff3">Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan</wicri:regionArea></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">26166891</idno><idno type="pmc">4494846</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4494846</idno><idno type="RBID">PMC:4494846</idno><idno type="doi">10.1007/s00706-013-1115-3</idno><date when="2014">2014</date><idno type="wicri:Area/Pmc/Corpus">000047</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000047</idno><idno type="wicri:Area/Pmc/Curation">000047</idno><idno type="wicri:explorRef" 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Olszowy</name><affiliation wicri:level="1"><nlm:aff id="Aff1">Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun</wicri:regionArea></affiliation></author><author><name sortKey="Pikus, Stanislaw" sort="Pikus, Stanislaw" uniqKey="Pikus S" first="Stanislaw" last="Pikus">Stanislaw Pikus</name><affiliation wicri:level="1"><nlm:aff id="Aff2">Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin</wicri:regionArea></affiliation></author><author><name sortKey="Kozak, Maciej" sort="Kozak, Maciej" uniqKey="Kozak M" first="Maciej" last="Kozak">Maciej Kozak</name><affiliation wicri:level="1"><nlm:aff id="Aff3">Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan</wicri:regionArea></affiliation></author></analytic><series><title level="j">Monatshefte Fur Chemie</title><idno type="ISSN">0026-9247</idno><idno type="eISSN">1434-4475</idno><imprint><date when="2014">2014</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><sec><title>Abstract</title><p>Polymeric polypyrrole and polythiophene solid phase microextraction (SPME) coatings were prepared using electropolymerization with a linear sweep voltammetry technique. Physicochemical properties were measured using different methods, in particular small angle X-ray scattering and scanning electron microscopy. By using innovative approaches for pore size measurement, we were able to calculate a maximum of the pore size range from 80 to 90 nm. Additionally, film thicknesses measured from 90 to 150 μm. 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<front><journal-meta><journal-id journal-id-type="nlm-ta">Monatsh Chem</journal-id><journal-id journal-id-type="iso-abbrev">Monatsh. Chem</journal-id><journal-title-group><journal-title>Monatshefte Fur Chemie</journal-title></journal-title-group><issn pub-type="ppub">0026-9247</issn><issn pub-type="epub">1434-4475</issn><publisher><publisher-name>Springer Vienna</publisher-name><publisher-loc>Vienna</publisher-loc></publisher></journal-meta><article-meta><article-id pub-id-type="pmid">26166891</article-id><article-id pub-id-type="pmc">4494846</article-id><article-id pub-id-type="publisher-id">1115</article-id><article-id pub-id-type="doi">10.1007/s00706-013-1115-3</article-id><article-categories><subj-group subj-group-type="heading"><subject>Original Paper</subject></subj-group></article-categories><title-group><article-title>Electropolymerized nanoporous polymeric SPME coatings: preparation and characterization by small angle X-ray scattering and scanning electron microscopy</article-title></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name><surname>Buszewski</surname><given-names>Boguslaw</given-names></name><address><email>bbusz@chem.umk.pl</email></address><xref ref-type="aff" rid="Aff1"></xref></contrib><contrib contrib-type="author"><name><surname>Olszowy</surname><given-names>Pawel</given-names></name><xref ref-type="aff" rid="Aff1"></xref></contrib><contrib contrib-type="author"><name><surname>Pikus</surname><given-names>Stanislaw</given-names></name><xref ref-type="aff" rid="Aff2"></xref></contrib><contrib contrib-type="author"><name><surname>Kozak</surname><given-names>Maciej</given-names></name><xref ref-type="aff" rid="Aff3"></xref></contrib><aff id="Aff1"><label></label>Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun, Poland</aff><aff id="Aff2"><label></label>Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin, Poland</aff><aff id="Aff3"><label></label>Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan, Poland</aff></contrib-group><pub-date pub-type="epub"><day>24</day><month>1</month><year>2014</year></pub-date><pub-date pub-type="pmc-release"><day>24</day><month>1</month><year>2014</year></pub-date><pub-date pub-type="ppub"><year>2014</year></pub-date><volume>145</volume><issue>3</issue><fpage>527</fpage><lpage>531</lpage><history><date date-type="received"><day>4</day><month>9</month><year>2013</year></date><date date-type="accepted"><day>26</day><month>10</month><year>2013</year></date></history><permissions><copyright-statement>© The Author(s) 2014</copyright-statement><license license-type="OpenAccess"><license-p><bold>Open Access</bold>This article is distributed under the terms of the Creative Commons Attribution License which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited.</license-p></license></permissions><abstract id="Abs1"><sec><title>Abstract</title><p>Polymeric polypyrrole and polythiophene solid phase microextraction (SPME) coatings were prepared using electropolymerization with a linear sweep voltammetry technique. Physicochemical properties were measured using different methods, in particular small angle X-ray scattering and scanning electron microscopy. By using innovative approaches for pore size measurement, we were able to calculate a maximum of the pore size range from 80 to 90 nm. Additionally, film thicknesses measured from 90 to 150 μm. Using scanning electron microscopy, we describe the characteristics of polymer growth on the support surface.</p></sec><sec><title>Graphical abstract</title><p><graphic position="anchor" xlink:href="706_2013_1115_Figa_HTML" id="MO1"></graphic></p></sec></abstract><kwd-group xml:lang="en"><title>Keywords</title><kwd>Polymerization</kwd><kwd>Extraction</kwd><kwd>X-ray scattering</kwd><kwd>Porosity measurements</kwd><kwd>Electron microscopy</kwd></kwd-group><custom-meta-group><custom-meta><meta-name>issue-copyright-statement</meta-name><meta-value>© Springer-Verlag Wien 2014</meta-value></custom-meta></custom-meta-group></article-meta></front></pmc></record>Pour manipuler ce document sous Unix (Dilib)
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