Essential oil composition of Citrus medica L. Cv. Diamante (Diamante citron) determined after using different extraction methods
Identifieur interne : 001277 ( Istex/Corpus ); précédent : 001276; suivant : 001278Essential oil composition of Citrus medica L. Cv. Diamante (Diamante citron) determined after using different extraction methods
Auteurs : Bartolo Gabriele ; Alessia Fazio ; Paola Dugo ; Rosaria Costa ; Luigi MondelloSource :
- Journal of Separation Science [ 1615-9306 ] ; 2009-01.
English descriptors
Abstract
In this paper, we report the qualitative and quantitative composition of the volatile and the oxygenated heterocyclic fraction of citron (Citrus medica L. cv. Diamante (Diamante citron)). The fruits selected for the extraction were of three types: green citron of little size, green citron of big size, and yellow citron after 1 month from the harvest. The essential oils were extracted using three different methods. The nine samples of oil thus obtained were analyzed by high resolution GC (HRGC)‐flame ionization detection (FID), HRGC‐MS, and RP‐HPLC. They differ only in the quantitative composition, while the qualitative profile was the same. The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. Oxypeucedanin was the main component of the oxygenated heterocyclic fraction in the extracts of green fruits, while citropten was the major oxygenated compound in the oil obtained from yellow citron.
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DOI: 10.1002/jssc.200800404
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ISTEX:321AED8DE08F91345A5CAE0B225667C6DF21431CLe document en format XML
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The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. Oxypeucedanin was the main component of the oxygenated heterocyclic fraction in the extracts of green fruits, while citropten was the major oxygenated compound in the oil obtained from yellow citron.</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Bartolo Gabriele</name><affiliations><json:string>E-mail: b.gabriele@unical.it</json:string><json:string>Dipartimento di Scienze Farmaceutiche, Università della Calabria, Cosenza, Italy. 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They differ only in the quantitative composition, while the qualitative profile was the same. The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. 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The fruits selected for the extraction were of three types: green citron of little size, green citron of big size, and yellow citron after 1 month from the harvest. The essential oils were extracted using three different methods. The nine samples of oil thus obtained were analyzed by high resolution GC (HRGC)‐flame ionization detection (FID), HRGC‐MS, and RP‐HPLC. They differ only in the quantitative composition, while the qualitative profile was the same. The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. Oxypeucedanin was the main component of the oxygenated heterocyclic fraction in the extracts of green fruits, while citropten was the major oxygenated compound in the oil obtained from yellow citron.</p></abstract><textClass xml:lang="en"><keywords scheme="keyword"><list><head>Keywords</head><item><term>Citrus medica L. cv. 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Diamante (Diamante citron) determined after using different extraction methods</title></titleGroup><creators><creator xml:id="au1" creatorRole="author"><personName><givenNames>Bartolo</givenNames><familyName>Gabriele</familyName></personName><contactDetails><email>b.gabriele@unical.it</email></contactDetails></creator><creator xml:id="au2" creatorRole="author" affiliationRef="#a1"><personName><givenNames>Alessia</givenNames><familyName>Fazio</familyName></personName></creator><creator xml:id="au3" creatorRole="author" affiliationRef="#a2"><personName><givenNames>Paola</givenNames><familyName>Dugo</familyName></personName></creator><creator xml:id="au4" creatorRole="author" affiliationRef="#a3"><personName><givenNames>Rosaria</givenNames><familyName>Costa</familyName></personName></creator><creator xml:id="au5" creatorRole="author" affiliationRef="#a3"><personName><givenNames>Luigi</givenNames><familyName>Mondello</familyName></personName></creator></creators><affiliationGroup><affiliation xml:id="a1" countryCode="IT" type="organization"><unparsedAffiliation>Dipartimento di Scienze Farmaceutiche, Università della Calabria, Cosenza, Italy. Fax: +39‐0984‐492044</unparsedAffiliation></affiliation><affiliation xml:id="a2" countryCode="IT" type="organization"><unparsedAffiliation>Dipartimento di Scienze degli Alimenti e dell'Ambiente, Università di Messina, Messina, Italy</unparsedAffiliation></affiliation><affiliation xml:id="a3" countryCode="IT" type="organization"><unparsedAffiliation>Dipartimento Farmaco‐Chimico, Università di Messina, Messina, Italy</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1"><i>Citrus medica </i>L. cv. Diamante (Diamante citron)</keyword><keyword xml:id="kwd2">HRGC‐FID</keyword><keyword xml:id="kwd3">HRGC‐MS</keyword><keyword xml:id="kwd4">RP‐HPLC</keyword></keywordGroup><abstractGroup><abstract type="main" xml:lang="en"><title type="main">Abstract</title><p>In this paper, we report the qualitative and quantitative composition of the volatile and the oxygenated heterocyclic fraction of citron (<i>Citrus medica</i> L. cv. Diamante (Diamante citron)). The fruits selected for the extraction were of three types: green citron of little size, green citron of big size, and yellow citron after 1 month from the harvest. The essential oils were extracted using three different methods. The nine samples of oil thus obtained were analyzed by high resolution GC (HRGC)‐flame ionization detection (FID), HRGC‐MS, and RP‐HPLC. They differ only in the quantitative composition, while the qualitative profile was the same. The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. Oxypeucedanin was the main component of the oxygenated heterocyclic fraction in the extracts of green fruits, while citropten was the major oxygenated compound in the oil obtained from yellow citron.</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Essential oil composition of Citrus medica L. Cv. Diamante (Diamante citron) determined after using different extraction methods</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Essential oil composition of</title></titleInfo><name type="personal"><namePart type="given">Bartolo</namePart><namePart type="family">Gabriele</namePart><affiliation>E-mail: b.gabriele@unical.it</affiliation><affiliation>Dipartimento di Scienze Farmaceutiche, Università della Calabria, Cosenza, Italy. Fax: +39‐0984‐492044</affiliation><affiliation>Dipartimento di Scienze degli Alimenti e dell'Ambiente, Università di Messina, Messina, Italy</affiliation><affiliation>Dipartimento Farmaco‐Chimico, Università di Messina, Messina, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Alessia</namePart><namePart type="family">Fazio</namePart><affiliation>Dipartimento di Scienze Farmaceutiche, Università della Calabria, Cosenza, Italy. Fax: +39‐0984‐492044</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Paola</namePart><namePart type="family">Dugo</namePart><affiliation>Dipartimento di Scienze degli Alimenti e dell'Ambiente, Università di Messina, Messina, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Rosaria</namePart><namePart type="family">Costa</namePart><affiliation>Dipartimento Farmaco‐Chimico, Università di Messina, Messina, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Luigi</namePart><namePart type="family">Mondello</namePart><affiliation>Dipartimento Farmaco‐Chimico, Università di Messina, Messina, Italy</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article">article</genre><originInfo><publisher>WILEY‐VCH Verlag</publisher><place><placeTerm type="text">Weinheim</placeTerm></place><dateIssued encoding="w3cdtf">2009-01</dateIssued><dateCaptured encoding="w3cdtf">2008-07-18</dateCaptured><copyrightDate encoding="w3cdtf">2009</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">4</extent><extent unit="tables">4</extent><extent unit="references">22</extent></physicalDescription><abstract lang="en">In this paper, we report the qualitative and quantitative composition of the volatile and the oxygenated heterocyclic fraction of citron (Citrus medica L. cv. Diamante (Diamante citron)). The fruits selected for the extraction were of three types: green citron of little size, green citron of big size, and yellow citron after 1 month from the harvest. The essential oils were extracted using three different methods. The nine samples of oil thus obtained were analyzed by high resolution GC (HRGC)‐flame ionization detection (FID), HRGC‐MS, and RP‐HPLC. They differ only in the quantitative composition, while the qualitative profile was the same. The volatile fraction of every sample of oil is characterized by a high content of limonene, γ‐terpinene, and monoterpene aldehydes and a lower content of α‐ and β‐pinene and myrcene, sesquiterpenes, and aliphatic aldehydes. Enantioselective (Es)‐GC analysis of the extracts allowed the determination of the enantiomeric distribution of five terpenoid compounds; a prevalence of four dextrorotatory isomers was observed. Oxypeucedanin was the main component of the oxygenated heterocyclic fraction in the extracts of green fruits, while citropten was the major oxygenated compound in the oil obtained from yellow citron.</abstract><subject lang="en"><genre>Keywords</genre><topic>Citrus medica L. cv. Diamante (Diamante citron)</topic><topic>HRGC‐FID</topic><topic>HRGC‐MS</topic><topic>RP‐HPLC</topic></subject><relatedItem type="host"><titleInfo><title>Journal of Separation Science</title></titleInfo><titleInfo type="abbreviated"><title>J. Sep. Science</title></titleInfo><subject><genre>article category</genre><topic>Gas Chromatography</topic></subject><identifier type="ISSN">1615-9306</identifier><identifier type="eISSN">1615-9314</identifier><identifier type="DOI">10.1002/(ISSN)1615-9314</identifier><identifier type="PublisherID">JSSC</identifier><part><date>2009</date><detail type="volume"><caption>vol.</caption><number>32</number></detail><detail type="issue"><caption>no.</caption><number>1</number></detail><extent unit="pages"><start>99</start><end>108</end><total>10</total></extent></part></relatedItem><relatedItem type="preceding"><titleInfo><title>Journal of High Resolution Chromatography</title></titleInfo><identifier type="ISSN">0935-6304</identifier><part><date point="end">2000</date><detail type="volume"><caption>last vol.</caption><number>23</number></detail><detail type="issue"><caption>last no.</caption><number>12</number></detail></part></relatedItem><identifier type="istex">321AED8DE08F91345A5CAE0B225667C6DF21431C</identifier><identifier type="DOI">10.1002/jssc.200800404</identifier><identifier type="ArticleID">JSSC200800404</identifier><accessCondition type="use and reproduction" contentType="copyright">Copyright © 2009 WILEY‐VCH Verlag GmbH & Co. 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