Synthesis of processible doped polyaniline‐polyacrylic acid composites
Identifieur interne : 001202 ( Istex/Corpus ); précédent : 001201; suivant : 001203Synthesis of processible doped polyaniline‐polyacrylic acid composites
Auteurs : Bhavana Gupta ; Rajiv PrakashSource :
- Journal of Applied Polymer Science [ 0021-8995 ] ; 2009-10-15.
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Abstract
Processible composites of emeraldine salt form of polyaniline (PANI) with polyacrylic acid (PAA) are synthesized and studied for their structural, electrical, mechanical, thermal, and electrochemical properties. The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as a = 5.93Å, b = 7.57Å, and c = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 M NaClO4‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009
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DOI: 10.1002/app.30554
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Appl. Polym. 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The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as a = 5.93Å, b = 7.57Å, and c = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 M NaClO4‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Bhavana Gupta</name><affiliations><json:string>School of Materials Science and Technology, Institute of Technology, Banaras Hindu University, Varanasi 221005, India</json:string></affiliations></json:item><json:item><name>Rajiv Prakash</name><affiliations><json:string>School of Materials Science and Technology, Institute of Technology, Banaras Hindu University, Varanasi 221005, India</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>conducting polymer</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>polyaniline</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>polyacrylic acid</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>polymer composite</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>electrochemical capacitor</value></json:item></subject><language><json:string>eng</json:string></language><abstract>Processible composites of emeraldine salt form of polyaniline (PANI) with polyacrylic acid (PAA) are synthesized and studied for their structural, electrical, mechanical, thermal, and electrochemical properties. The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as a = 5.93Å, b = 7.57Å, and c = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 M NaClO4‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. 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The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as a = 5.93Å, b = 7.57Å, and c = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 M NaClO4‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. 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The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as <i>a</i> = 5.93Å, <i>b</i> = 7.57Å, and <i>c</i> = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 <i>M</i> NaClO<sub>4</sub>‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Synthesis of processible doped polyaniline‐polyacrylic acid composites</title></titleInfo><titleInfo type="abbreviated" lang="en"><title>Synthesis of Polyaniline‐Polyacrylic Acid Composites</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Synthesis of processible doped polyaniline‐polyacrylic acid composites</title></titleInfo><name type="personal"><namePart type="given">Bhavana</namePart><namePart type="family">Gupta</namePart><affiliation>School of Materials Science and Technology, Institute of Technology, Banaras Hindu University, Varanasi 221005, India</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Rajiv</namePart><namePart type="family">Prakash</namePart><affiliation>School of Materials Science and Technology, Institute of Technology, Banaras Hindu University, Varanasi 221005, India</affiliation><description>Correspondence: School of Materials Science and Technology, Institute of Technology, Banaras Hindu University, Varanasi 221005, India===</description><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article">article</genre><originInfo><publisher>Wiley Subscription Services, Inc., A Wiley Company</publisher><place><placeTerm type="text">Hoboken</placeTerm></place><dateIssued encoding="w3cdtf">2009-10-15</dateIssued><dateCaptured encoding="w3cdtf">2008-07-24</dateCaptured><dateValid encoding="w3cdtf">2009-03-23</dateValid><copyrightDate encoding="w3cdtf">2009</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">12</extent><extent unit="tables">2</extent><extent unit="references">36</extent><extent unit="words">4768</extent></physicalDescription><abstract lang="en">Processible composites of emeraldine salt form of polyaniline (PANI) with polyacrylic acid (PAA) are synthesized and studied for their structural, electrical, mechanical, thermal, and electrochemical properties. The processible conducting composites of various weight percentage from 20 wt % to 90 wt % (of PANI) have been prepared by mixing the PANI and PAA under vigorous stirring and sonication conditions. Self‐standing films of electroactive homogeneous composites are obtained by solution casting method. A significant improvement in processibility, crystallinity, and thermal stability is observed in the composites; however, the electrical conductivity decreased remarkably as the percentage of PANI is decreased in the composites. The 60 wt % PANI‐PAA composite showed crystalline structural property with orthorhombic crystal system and cell parameters as a = 5.93Å, b = 7.57Å, and c = 10.11Å. The 60 wt % PANI‐PAA composite also showed better thermal stability and highest capacitance amongst all the composites and used as an active material for development of electrochemical capacitors (parallel plate assembly). The processible composites based electrochemical capacitors using 0.5 M NaClO4‐Acetonitril electrolyte showed super capacitance with ease in fabrication and cost effectiveness in comparison to other similar materials based capacitors. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</abstract><note type="funding">CSIR, New Delhi</note><subject lang="en"><genre>Keywords</genre><topic>conducting polymer</topic><topic>polyaniline</topic><topic>polyacrylic acid</topic><topic>polymer composite</topic><topic>electrochemical capacitor</topic></subject><relatedItem type="host"><titleInfo><title>Journal of Applied Polymer Science</title></titleInfo><titleInfo type="abbreviated"><title>J. Appl. Polym. 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