Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs
Identifieur interne : 000E49 ( Istex/Corpus ); précédent : 000E48; suivant : 000E50Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs
Auteurs : Md. Moniruzzaman ; C. K. DasSource :
- Macromolecular Symposia [ 1022-1360 ] ; 2010-12.
English descriptors
Abstract
Summary: Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO3 through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO3 surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO3 is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO3 composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO3 composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. Maximum power density was found to be 5147.70 W/kg in the same composite at a scan rate of 200 mv/s.
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DOI: 10.1002/masy.201000032
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Das</name><affiliation><mods:affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:0521EC0EBDA72FA27FEBC9ABDBA59FE95DAB3B0C</idno><date when="2010" year="2010">2010</date><idno type="doi">10.1002/masy.201000032</idno><idno type="url">https://api.istex.fr/document/0521EC0EBDA72FA27FEBC9ABDBA59FE95DAB3B0C/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">000E49</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main" xml:lang="en">Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs</title><author><name sortKey="Moniruzzaman, Md" sort="Moniruzzaman, Md" uniqKey="Moniruzzaman M" first="Md." last="Moniruzzaman">Md. Moniruzzaman</name><affiliation><mods:affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</mods:affiliation></affiliation></author><author><name sortKey="Das, C K" sort="Das, C K" uniqKey="Das C" first="C. K." last="Das">C. K. Das</name><affiliation><mods:affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Macromolecular Symposia</title><title level="j" type="abbrev">Macromol. Symp.</title><idno type="ISSN">1022-1360</idno><idno type="eISSN">1521-3900</idno><imprint><publisher>WILEY‐VCH Verlag</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="2010-12">2010-12</date><biblScope unit="volume">298</biblScope><biblScope unit="issue">1</biblScope><biblScope unit="page" from="34">34</biblScope><biblScope unit="page" to="42">42</biblScope></imprint><idno type="ISSN">1022-1360</idno></series><idno type="istex">0521EC0EBDA72FA27FEBC9ABDBA59FE95DAB3B0C</idno><idno type="DOI">10.1002/masy.201000032</idno><idno type="ArticleID">MASY201000032</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1022-1360</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>MWCNTs</term><term>in‐situ polymerization</term><term>nanocomposites</term><term>polyaniline</term><term>supercapacitor</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Summary: Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO3 through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO3 surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO3 is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO3 composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO3 composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. Maximum power density was found to be 5147.70 W/kg in the same composite at a scan rate of 200 mv/s.</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Md. Moniruzzaman</name><affiliations><json:string>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</json:string></affiliations></json:item><json:item><name>C. K. Das</name><affiliations><json:string>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>in‐situ polymerization</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>MWCNTs</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>nanocomposites</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>polyaniline</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>supercapacitor</value></json:item></subject><language><json:string>eng</json:string></language><abstract>Summary: Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO3 through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO3 surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO3 is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO3 composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO3 composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. 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K.</forename><surname>Das</surname></persName><note type="correspondence"><p>Correspondence: Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India.</p></note><affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</affiliation></author></analytic><monogr><title level="j">Macromolecular Symposia</title><title level="j" type="abbrev">Macromol. Symp.</title><idno type="pISSN">1022-1360</idno><idno type="eISSN">1521-3900</idno><idno type="DOI">10.1002/(ISSN)1521-3900</idno><imprint><publisher>WILEY‐VCH Verlag</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="2010-12"></date><biblScope unit="volume">298</biblScope><biblScope unit="issue">1</biblScope><biblScope unit="page" from="34">34</biblScope><biblScope unit="page" to="42">42</biblScope></imprint></monogr><idno type="istex">0521EC0EBDA72FA27FEBC9ABDBA59FE95DAB3B0C</idno><idno type="DOI">10.1002/masy.201000032</idno><idno type="ArticleID">MASY201000032</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>2010</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>Summary: Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO3 through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO3 surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO3 is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO3 composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO3 composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. 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KGaA, Weinheim</copyright><eventGroup><event type="xmlConverted" agent="Converter:JWSART34_TO_WML3G version:2.4.2 mode:FullText mathml2tex" date="2011-01-07"></event><event type="firstOnline" date="2011-01-07"></event><event type="publishedOnlineFinalForm" date="2011-01-07"></event><event type="xmlConverted" agent="Converter:WILEY_ML3G_TO_WILEY_ML3GV2 version:3.8.8" date="2014-02-02"></event><event type="xmlConverted" agent="Converter:WML3G_To_WML3G version:4.1.7 mode:FullText,remove_FC" date="2014-10-31"></event></eventGroup><numberingGroup><numbering type="pageFirst">34</numbering><numbering type="pageLast">42</numbering></numberingGroup><correspondenceTo>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India.</correspondenceTo><linkGroup><link type="toTypesetVersion" href="file:MASY.MASY201000032.pdf"></link></linkGroup></publicationMeta><contentMeta><countGroup><count type="figureTotal" number="6"></count><count type="tableTotal" number="4"></count><count type="referenceTotal" number="26"></count><count type="wordTotal" number="3549"></count></countGroup><titleGroup><title type="main" xml:lang="en">Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs</title></titleGroup><creators><creator xml:id="au1" creatorRole="author" affiliationRef="#af1"><personName><givenNames>Md.</givenNames><familyName>Moniruzzaman</familyName></personName></creator><creator xml:id="au2" creatorRole="author" affiliationRef="#af1" corresponding="yes"><personName><givenNames>C. K.</givenNames><familyName>Das</familyName></personName><contactDetails><email>monir1enstn@gmail.com</email></contactDetails></creator></creators><affiliationGroup><affiliation xml:id="af1" countryCode="IN" type="organization"><unparsedAffiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1">in‐situ polymerization</keyword><keyword xml:id="kwd2">MWCNTs</keyword><keyword xml:id="kwd3">nanocomposites</keyword><keyword xml:id="kwd4">polyaniline</keyword><keyword xml:id="kwd5">supercapacitor</keyword></keywordGroup><abstractGroup><abstract type="main" xml:lang="en"><title type="main">Abstract</title><p><b>Summary:</b> Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO<sub>3</sub> through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO<sub>3</sub> surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO<sub>3</sub> is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO<sub>3</sub> composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO<sub>3</sub> composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. Maximum power density was found to be 5147.70 W/kg in the same composite at a scan rate of 200 mv/s.</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Preparation and Characterization of In‐Situ Polymerized Nanocomposites Based on Polyaniline in Presence of MWCNTs</title></titleInfo><name type="personal"><namePart type="given">Md.</namePart><namePart type="family">Moniruzzaman</namePart><affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">C. K.</namePart><namePart type="family">Das</namePart><affiliation>Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India</affiliation><description>Correspondence: Materials Science Centre, Indian Institute of Technology, Kharagpur‐721302, India.</description><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article">article</genre><originInfo><publisher>WILEY‐VCH Verlag</publisher><place><placeTerm type="text">Weinheim</placeTerm></place><dateIssued encoding="w3cdtf">2010-12</dateIssued><copyrightDate encoding="w3cdtf">2010</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">6</extent><extent unit="tables">4</extent><extent unit="references">26</extent><extent unit="words">3549</extent></physicalDescription><abstract lang="en">Summary: Polyaniline (PANI) composites were prepared with both unmodified and amine modified MWCNTs with and without BaTiO3 through in‐situ oxidative polymerization. Uniform coating of PANI on the MWCNTs and BaTiO3 surfaces was found which was evident from the Field Emission Scanning Electron Microscopic (FESEM) and High Resolution Transmission Electron Microscopic (HRTEM) images. The structure of pure and amine modified MWCNTs was identified by Fourier Transform Infrared Spectroscopy (FTIR). The thermal stability of the amine modified composite with BaTiO3 is higher than that of the unmodified composite because of the better affinity between modified MWCNTs and polymer matrix and due to the higher stability of barium titanate itself. The capacitance of amine modified MWCNTs and BaTiO3 composites was less than that of the pure MWCNTs composites but the thermal stability increased in amine modified MWCNTs and BaTiO3 composites with respect to the pure MWCNTs composites. The maximum capacitance and energy density values were found in MWCNT/PANI composites which were equal to 523.20 F/g and 142.83 Wh/kg respectively at a scan rate of 10mv/s. Maximum power density was found to be 5147.70 W/kg in the same composite at a scan rate of 200 mv/s.</abstract><subject lang="en"><genre>Keywords</genre><topic>in‐situ polymerization</topic><topic>MWCNTs</topic><topic>nanocomposites</topic><topic>polyaniline</topic><topic>supercapacitor</topic></subject><relatedItem type="host"><titleInfo><title>Macromolecular Symposia</title></titleInfo><titleInfo type="abbreviated"><title>Macromol. 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