Validated HPTLC methods for the determination of salicin in Salix sp. and of harpagoside in Harpagophytum [corrected] procumbens.
Identifieur interne : 001878 ( Main/Exploration ); précédent : 001877; suivant : 001879Validated HPTLC methods for the determination of salicin in Salix sp. and of harpagoside in Harpagophytum [corrected] procumbens.
Auteurs : Steffen Wagner [Allemagne] ; Abraham Ure A ; Eike Reich ; Irmgard MerfortSource :
- Journal of pharmaceutical and biomedical analysis [ 0731-7085 ] ; 2008.
Descripteurs français
- KwdFr :
- Alcools benzyliques (analyse), Chromatographie en phase liquide à haute performance (méthodes), Chromatographie en phase liquide à haute performance (économie), Facteurs temps (MeSH), Glucosides (MeSH), Harpagophytum (composition chimique), Hétérosides (analyse), Pyrannes (analyse), Racines de plante (composition chimique), Reproductibilité des résultats (MeSH), Salix (composition chimique), Sensibilité et spécificité (MeSH), Structure moléculaire (MeSH).
- MESH :
- analyse : Alcools benzyliques, Hétérosides, Pyrannes.
- composition chimique : Harpagophytum, Racines de plante, Salix.
- méthodes : Chromatographie en phase liquide à haute performance.
- économie : Chromatographie en phase liquide à haute performance.
- Facteurs temps, Glucosides, Reproductibilité des résultats, Sensibilité et spécificité, Structure moléculaire.
English descriptors
- KwdEn :
- Benzyl Alcohols (analysis), Chromatography, High Pressure Liquid (economics), Chromatography, High Pressure Liquid (methods), Glucosides (MeSH), Glycosides (analysis), Harpagophytum (chemistry), Molecular Structure (MeSH), Plant Roots (chemistry), Pyrans (analysis), Reproducibility of Results (MeSH), Salix (chemistry), Sensitivity and Specificity (MeSH), Time Factors (MeSH).
- MESH :
- chemical , analysis : Benzyl Alcohols, Glycosides, Pyrans.
- chemistry : Harpagophytum, Plant Roots, Salix.
- economics : Chromatography, High Pressure Liquid.
- methods : Chromatography, High Pressure Liquid.
- chemical : Glucosides, Molecular Structure, Reproducibility of Results, Sensitivity and Specificity, Time Factors.
Abstract
Preparations of Harpagophytum procumbens and of Salix species are successfully used for the treatment of degenerative rheumatism and painful arthrosis. For the quality control of both drugs, rapid methods of quantification are desirable. Here we report the development of two HPTLC methods enabling the determination of harpagoside in Harpagophyti radix and of salicin in Salicis cortex. We focused on a standardized methodology and thorough validation including two laboratories. The methods allow the analyses of up to 16 samples in parallel demonstrating the proposed methods as very rapid and cost efficient.
DOI: 10.1016/j.jpba.2008.05.030
PubMed: 18602786
Affiliations:
Links toward previous steps (curation, corpus...)
Le document en format XML
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<author><name sortKey="Reich, Eike" sort="Reich, Eike" uniqKey="Reich E" first="Eike" last="Reich">Eike Reich</name>
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<term>Glucosides (MeSH)</term>
<term>Glycosides (analysis)</term>
<term>Harpagophytum (chemistry)</term>
<term>Molecular Structure (MeSH)</term>
<term>Plant Roots (chemistry)</term>
<term>Pyrans (analysis)</term>
<term>Reproducibility of Results (MeSH)</term>
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<term>Facteurs temps (MeSH)</term>
<term>Glucosides (MeSH)</term>
<term>Harpagophytum (composition chimique)</term>
<term>Hétérosides (analyse)</term>
<term>Pyrannes (analyse)</term>
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<term>Reproductibilité des résultats (MeSH)</term>
<term>Salix (composition chimique)</term>
<term>Sensibilité et spécificité (MeSH)</term>
<term>Structure moléculaire (MeSH)</term>
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<term>Reproducibility of Results</term>
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<term>Time Factors</term>
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<front><div type="abstract" xml:lang="en">Preparations of Harpagophytum procumbens and of Salix species are successfully used for the treatment of degenerative rheumatism and painful arthrosis. For the quality control of both drugs, rapid methods of quantification are desirable. Here we report the development of two HPTLC methods enabling the determination of harpagoside in Harpagophyti radix and of salicin in Salicis cortex. We focused on a standardized methodology and thorough validation including two laboratories. The methods allow the analyses of up to 16 samples in parallel demonstrating the proposed methods as very rapid and cost efficient.</div>
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<Abstract><AbstractText>Preparations of Harpagophytum procumbens and of Salix species are successfully used for the treatment of degenerative rheumatism and painful arthrosis. For the quality control of both drugs, rapid methods of quantification are desirable. Here we report the development of two HPTLC methods enabling the determination of harpagoside in Harpagophyti radix and of salicin in Salicis cortex. We focused on a standardized methodology and thorough validation including two laboratories. The methods allow the analyses of up to 16 samples in parallel demonstrating the proposed methods as very rapid and cost efficient.</AbstractText>
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