Barrier Film of Etherified Hemicellulose from Single-Step Synthesis.
Identifieur interne : 000548 ( Main/Exploration ); précédent : 000547; suivant : 000549Barrier Film of Etherified Hemicellulose from Single-Step Synthesis.
Auteurs : Hui Shao [République populaire de Chine] ; Yuelong Zhao [République populaire de Chine] ; Hui Sun [République populaire de Chine] ; Biao Yang [République populaire de Chine] ; Baomin Fan [République populaire de Chine] ; Huijuan Zhang [République populaire de Chine] ; Yunxuan Weng [République populaire de Chine]Source :
- Polymers [ 2073-4360 ] ; 2020.
Abstract
Hemicellulose with good biodegradability and low oxygen permeability shows great potential in food packaging. However, its strong hydrophilicity leads to its poor moisture resistance, which hinders its wider application. In this paper, a near-hydrophobic hemicellulose was obtained by using single-step synthesis from poplar powder via etherification modification with epoxy chloropropane. This proposed approach has the advantage of avoiding the destruction of hemicellulose structure by secondary alkali-hydrolysis, which was what usually occurred in traditional etherification procedures. The feasibility of using epoxy chloropropane as an alkylation reagent to etherify hemicellulose was confirmed, and the reaction mechanism was elucidated. Contact angle test, thermogravimetric analysis, oxygen transmittance test, and infrared spectrum analysis showed that the barrier property and thermal stability of etherified hemicellulose films have been significantly improved. At an epoxy chloropropane/wood powder ratio (volume/weight) of 2/3 (mL/g), the epoxy hemicellulose films contained the most epoxy groups and displayed the best performance, i.e., tensile strength of 14.6 MPa, surface contact angle of 71.7° and oxygen transmission coefficient of 1.9 (cm3·µm)/(m2·d·kPa), showing great promise as barrier film in food-packaging.
DOI: 10.3390/polym12102199
PubMed: 32992935
PubMed Central: PMC7599748
Affiliations:
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type="wicri:Area/Main/Exploration">000087</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en">Barrier Film of Etherified Hemicellulose from Single-Step Synthesis.</title><author><name sortKey="Shao, Hui" sort="Shao, Hui" uniqKey="Shao H" first="Hui" last="Shao">Hui Shao</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Zhao, Yuelong" sort="Zhao, Yuelong" uniqKey="Zhao Y" first="Yuelong" last="Zhao">Yuelong Zhao</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Sun, Hui" sort="Sun, Hui" uniqKey="Sun H" first="Hui" last="Sun">Hui Sun</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation><affiliation wicri:level="1"><nlm:affiliation>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Yang, Biao" sort="Yang, Biao" uniqKey="Yang B" first="Biao" last="Yang">Biao Yang</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Fan, Baomin" sort="Fan, Baomin" uniqKey="Fan B" first="Baomin" last="Fan">Baomin Fan</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Zhang, Huijuan" sort="Zhang, Huijuan" uniqKey="Zhang H" first="Huijuan" last="Zhang">Huijuan Zhang</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Weng, Yunxuan" sort="Weng, Yunxuan" uniqKey="Weng Y" first="Yunxuan" last="Weng">Yunxuan Weng</name><affiliation wicri:level="1"><nlm:affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation><affiliation wicri:level="1"><nlm:affiliation>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author></analytic><series><title level="j">Polymers</title><idno type="eISSN">2073-4360</idno><imprint><date when="2020" type="published">2020</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Hemicellulose with good biodegradability and low oxygen permeability shows great potential in food packaging. However, its strong hydrophilicity leads to its poor moisture resistance, which hinders its wider application. In this paper, a near-hydrophobic hemicellulose was obtained by using single-step synthesis from poplar powder via etherification modification with epoxy chloropropane. This proposed approach has the advantage of avoiding the destruction of hemicellulose structure by secondary alkali-hydrolysis, which was what usually occurred in traditional etherification procedures. The feasibility of using epoxy chloropropane as an alkylation reagent to etherify hemicellulose was confirmed, and the reaction mechanism was elucidated. Contact angle test, thermogravimetric analysis, oxygen transmittance test, and infrared spectrum analysis showed that the barrier property and thermal stability of etherified hemicellulose films have been significantly improved. At an epoxy chloropropane/wood powder ratio (volume/weight) of 2/3 (mL/g), the epoxy hemicellulose films contained the most epoxy groups and displayed the best performance, i.e., tensile strength of 14.6 MPa, surface contact angle of 71.7° and oxygen transmission coefficient of 1.9 (cm<sup>3</sup>·µm)/(m<sup>2</sup>·d·kPa), showing great promise as barrier film in food-packaging.</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">32992935</PMID><DateRevised><Year>2020</Year><Month>11</Month><Day>03</Day></DateRevised><Article PubModel="Electronic"><Journal><ISSN IssnType="Electronic">2073-4360</ISSN><JournalIssue CitedMedium="Internet"><Volume>12</Volume><Issue>10</Issue><PubDate><Year>2020</Year><Month>Sep</Month><Day>25</Day></PubDate></JournalIssue><Title>Polymers</Title><ISOAbbreviation>Polymers (Basel)</ISOAbbreviation></Journal><ArticleTitle>Barrier Film of Etherified Hemicellulose from Single-Step Synthesis.</ArticleTitle><ELocationID EIdType="pii" ValidYN="Y">E2199</ELocationID><ELocationID EIdType="doi" ValidYN="Y">10.3390/polym12102199</ELocationID><Abstract><AbstractText>Hemicellulose with good biodegradability and low oxygen permeability shows great potential in food packaging. However, its strong hydrophilicity leads to its poor moisture resistance, which hinders its wider application. In this paper, a near-hydrophobic hemicellulose was obtained by using single-step synthesis from poplar powder via etherification modification with epoxy chloropropane. This proposed approach has the advantage of avoiding the destruction of hemicellulose structure by secondary alkali-hydrolysis, which was what usually occurred in traditional etherification procedures. The feasibility of using epoxy chloropropane as an alkylation reagent to etherify hemicellulose was confirmed, and the reaction mechanism was elucidated. Contact angle test, thermogravimetric analysis, oxygen transmittance test, and infrared spectrum analysis showed that the barrier property and thermal stability of etherified hemicellulose films have been significantly improved. At an epoxy chloropropane/wood powder ratio (volume/weight) of 2/3 (mL/g), the epoxy hemicellulose films contained the most epoxy groups and displayed the best performance, i.e., tensile strength of 14.6 MPa, surface contact angle of 71.7° and oxygen transmission coefficient of 1.9 (cm<sup>3</sup>·µm)/(m<sup>2</sup>·d·kPa), showing great promise as barrier film in food-packaging.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Shao</LastName><ForeName>Hui</ForeName><Initials>H</Initials><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zhao</LastName><ForeName>Yuelong</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Sun</LastName><ForeName>Hui</ForeName><Initials>H</Initials><Identifier Source="ORCID">0000-0003-4677-7299</Identifier><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Yang</LastName><ForeName>Biao</ForeName><Initials>B</Initials><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Fan</LastName><ForeName>Baomin</ForeName><Initials>B</Initials><Identifier Source="ORCID">0000-0002-0430-5712</Identifier><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zhang</LastName><ForeName>Huijuan</ForeName><Initials>H</Initials><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Weng</LastName><ForeName>Yunxuan</ForeName><Initials>Y</Initials><Identifier Source="ORCID">0000-0001-8492-0338</Identifier><AffiliationInfo><Affiliation>College of Chemistry and Materials Engineering, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing 100048, China.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><GrantList CompleteYN="Y"><Grant><GrantID>31570575, 21606005, 51473007</GrantID><Agency>National Natural Science Foundation of China</Agency><Country></Country></Grant><Grant><GrantID>2192016</GrantID><Agency>Natural Science Foundation of Beijing Municipality</Agency><Country></Country></Grant><Grant><GrantID>CIT&TCD201904042</GrantID><Agency>Support Project of High-level Teachers in Beijing Municipal Universities in the Period of 13th Five-year Plan</Agency><Country></Country></Grant><Grant><GrantID>LSL-1501</GrantID><Agency>the State Key Laboratory of Solid Lubrication of Lanzhou Institute of Chemical Physics</Agency><Country></Country></Grant></GrantList><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2020</Year><Month>09</Month><Day>25</Day></ArticleDate></Article><MedlineJournalInfo><Country>Switzerland</Country><MedlineTA>Polymers (Basel)</MedlineTA><NlmUniqueID>101545357</NlmUniqueID><ISSNLinking>2073-4360</ISSNLinking></MedlineJournalInfo><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">barrier film</Keyword><Keyword MajorTopicYN="N">epoxy chloropropane</Keyword><Keyword MajorTopicYN="N">etherification</Keyword><Keyword MajorTopicYN="N">hemicellulose</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2020</Year><Month>08</Month><Day>19</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2020</Year><Month>09</Month><Day>21</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2020</Year><Month>09</Month><Day>22</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2020</Year><Month>9</Month><Day>30</Day><Hour>1</Hour><Minute>2</Minute></PubMedPubDate><PubMedPubDate 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Sun</name><name sortKey="Weng, Yunxuan" sort="Weng, Yunxuan" uniqKey="Weng Y" first="Yunxuan" last="Weng">Yunxuan Weng</name><name sortKey="Weng, Yunxuan" sort="Weng, Yunxuan" uniqKey="Weng Y" first="Yunxuan" last="Weng">Yunxuan Weng</name><name sortKey="Yang, Biao" sort="Yang, Biao" uniqKey="Yang B" first="Biao" last="Yang">Biao Yang</name><name sortKey="Zhang, Huijuan" sort="Zhang, Huijuan" uniqKey="Zhang H" first="Huijuan" last="Zhang">Huijuan Zhang</name><name sortKey="Zhao, Yuelong" sort="Zhao, Yuelong" uniqKey="Zhao Y" first="Yuelong" last="Zhao">Yuelong Zhao</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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