Kinetics of Secondary Reactions Affecting the Organosolv Lignin Structure.
Identifieur interne : 000297 ( Main/Exploration ); précédent : 000296; suivant : 000298Kinetics of Secondary Reactions Affecting the Organosolv Lignin Structure.
Auteurs : James R. Meyer [États-Unis] ; Huiyong Li [États-Unis] ; Jialiang Zhang [États-Unis] ; Marcus B. Foston [États-Unis]Source :
- ChemSusChem [ 1864-564X ] ; 2020.
Abstract
Many valorization approaches for lignin rely on its organic solvent (organosolv) extraction. However, the severity of the extraction conditions required to obtain high lignin extraction generally results in low-quality lignin for downstream processing. To better understand the secondary reaction pathways and kinetics related to molecular alterations that result from organosolv extraction under extreme conditions, extractions were conducted at temperatures of 150, 180, and 210 °C. Lignin was collected at residence times between 0.25 and 18 h and analyzed by NMR techniques to quantify the concentrations of key chemical moieties that appear or disappear upon reactions of lignin molecules during and after their fractionation from biomass. The kinetics of chemical moiety evolution was modeled as processes in-series. In these models, pseudo first-order kinetics were used to describe the change in concentration of chemical moieties on extracted lignin as a function of residence time.
DOI: 10.1002/cssc.202000942
PubMed: 32413243
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Meyer</name><affiliation wicri:level="4"><nlm:affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130</wicri:regionArea><orgName type="university">Université Washington de Saint-Louis</orgName><placeName><settlement type="city">Saint-Louis (Missouri)</settlement><region type="state">Missouri (État)</region></placeName></affiliation></author><author><name sortKey="Li, Huiyong" sort="Li, Huiyong" uniqKey="Li H" first="Huiyong" last="Li">Huiyong Li</name><affiliation wicri:level="4"><nlm:affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130</wicri:regionArea><orgName type="university">Université Washington de Saint-Louis</orgName><placeName><settlement type="city">Saint-Louis (Missouri)</settlement><region type="state">Missouri (État)</region></placeName></affiliation></author><author><name sortKey="Zhang, Jialiang" sort="Zhang, Jialiang" uniqKey="Zhang J" first="Jialiang" last="Zhang">Jialiang Zhang</name><affiliation wicri:level="4"><nlm:affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130</wicri:regionArea><orgName type="university">Université Washington de Saint-Louis</orgName><placeName><settlement type="city">Saint-Louis (Missouri)</settlement><region type="state">Missouri (État)</region></placeName></affiliation></author><author><name sortKey="Foston, Marcus B" sort="Foston, Marcus B" uniqKey="Foston M" first="Marcus B" last="Foston">Marcus B. Foston</name><affiliation wicri:level="4"><nlm:affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130</wicri:regionArea><orgName type="university">Université Washington de Saint-Louis</orgName><placeName><settlement type="city">Saint-Louis (Missouri)</settlement><region type="state">Missouri (État)</region></placeName></affiliation></author></analytic><series><title level="j">ChemSusChem</title><idno type="eISSN">1864-564X</idno><imprint><date when="2020" type="published">2020</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Many valorization approaches for lignin rely on its organic solvent (organosolv) extraction. However, the severity of the extraction conditions required to obtain high lignin extraction generally results in low-quality lignin for downstream processing. To better understand the secondary reaction pathways and kinetics related to molecular alterations that result from organosolv extraction under extreme conditions, extractions were conducted at temperatures of 150, 180, and 210 °C. Lignin was collected at residence times between 0.25 and 18 h and analyzed by NMR techniques to quantify the concentrations of key chemical moieties that appear or disappear upon reactions of lignin molecules during and after their fractionation from biomass. The kinetics of chemical moiety evolution was modeled as processes in-series. In these models, pseudo first-order kinetics were used to describe the change in concentration of chemical moieties on extracted lignin as a function of residence time.</div></front></TEI><pubmed><MedlineCitation Status="Publisher" Owner="NLM"><PMID Version="1">32413243</PMID><DateRevised><Year>2020</Year><Month>06</Month><Day>15</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1864-564X</ISSN><JournalIssue CitedMedium="Internet"><PubDate><Year>2020</Year><Month>May</Month><Day>15</Day></PubDate></JournalIssue><Title>ChemSusChem</Title><ISOAbbreviation>ChemSusChem</ISOAbbreviation></Journal><ArticleTitle>Kinetics of Secondary Reactions Affecting the Organosolv Lignin Structure.</ArticleTitle><ELocationID EIdType="doi" ValidYN="Y">10.1002/cssc.202000942</ELocationID><Abstract><AbstractText>Many valorization approaches for lignin rely on its organic solvent (organosolv) extraction. However, the severity of the extraction conditions required to obtain high lignin extraction generally results in low-quality lignin for downstream processing. To better understand the secondary reaction pathways and kinetics related to molecular alterations that result from organosolv extraction under extreme conditions, extractions were conducted at temperatures of 150, 180, and 210 °C. Lignin was collected at residence times between 0.25 and 18 h and analyzed by NMR techniques to quantify the concentrations of key chemical moieties that appear or disappear upon reactions of lignin molecules during and after their fractionation from biomass. The kinetics of chemical moiety evolution was modeled as processes in-series. In these models, pseudo first-order kinetics were used to describe the change in concentration of chemical moieties on extracted lignin as a function of residence time.</AbstractText><CopyrightInformation>© 2020 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Meyer</LastName><ForeName>James R</ForeName><Initials>JR</Initials><AffiliationInfo><Affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Li</LastName><ForeName>Huiyong</ForeName><Initials>H</Initials><AffiliationInfo><Affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zhang</LastName><ForeName>Jialiang</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Foston</LastName><ForeName>Marcus B</ForeName><Initials>MB</Initials><Identifier Source="ORCID">http://orcid.org/0000-0002-4227-0362</Identifier><AffiliationInfo><Affiliation>Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, 1 Brookings Dr, St. Louis, MO, 63130, USA.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><GrantList CompleteYN="Y"><Grant><GrantID>15-48571</GrantID><Agency>Division of Civil, Mechanical and Manufacturing Innovation</Agency><Country></Country></Grant></GrantList><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2020</Year><Month>05</Month><Day>15</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>ChemSusChem</MedlineTA><NlmUniqueID>101319536</NlmUniqueID><ISSNLinking>1864-5631</ISSNLinking></MedlineJournalInfo><CitationSubset>IM</CitationSubset><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">NMR spectroscopy</Keyword><Keyword MajorTopicYN="N">hybrid poplar</Keyword><Keyword MajorTopicYN="N">kinetics</Keyword><Keyword MajorTopicYN="N">lignin</Keyword><Keyword MajorTopicYN="N">organosolv extraction</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2020</Year><Month>04</Month><Day>10</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2020</Year><Month>05</Month><Day>14</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2020</Year><Month>5</Month><Day>16</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2020</Year><Month>5</Month><Day>16</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2020</Year><Month>5</Month><Day>16</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>aheadofprint</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">32413243</ArticleId><ArticleId IdType="doi">10.1002/cssc.202000942</ArticleId></ArticleIdList><ReferenceList><Reference><Citation> </Citation></Reference><Reference><Citation>E. de Jong, A. 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Food Chem. 2004, 52, 1850-1860.</Citation></Reference></ReferenceList></PubmedData></pubmed><affiliations><list><country><li>États-Unis</li></country><region><li>Missouri (État)</li></region><settlement><li>Saint-Louis (Missouri)</li></settlement><orgName><li>Université Washington de Saint-Louis</li></orgName></list><tree><country name="États-Unis"><region name="Missouri (État)"><name sortKey="Meyer, James R" sort="Meyer, James R" uniqKey="Meyer J" first="James R" last="Meyer">James R. Meyer</name></region><name sortKey="Foston, Marcus B" sort="Foston, Marcus B" uniqKey="Foston M" first="Marcus B" last="Foston">Marcus B. Foston</name><name sortKey="Li, Huiyong" sort="Li, Huiyong" uniqKey="Li H" first="Huiyong" last="Li">Huiyong Li</name><name sortKey="Zhang, Jialiang" sort="Zhang, Jialiang" uniqKey="Zhang J" first="Jialiang" last="Zhang">Jialiang Zhang</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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