Pyrolysis of Biomass Impregnated With Ammonium Dihydrogen Phosphate for Polygeneration of Phenol and Supercapacitor Electrode Material.
Identifieur interne : 000165 ( Main/Exploration ); précédent : 000164; suivant : 000166Pyrolysis of Biomass Impregnated With Ammonium Dihydrogen Phosphate for Polygeneration of Phenol and Supercapacitor Electrode Material.
Auteurs : Kai Li [République populaire de Chine] ; Bo Wang [République populaire de Chine] ; Dana Bolatibieke [République populaire de Chine] ; Dong-Hong Nan [République populaire de Chine] ; Qiang Lu [République populaire de Chine]Source :
- Frontiers in chemistry [ 2296-2646 ] ; 2020.
Abstract
A new method was proposed for polygeneration of phenol and supercapacitor electrode material from pyrolysis of biomass impregnated with ammonium dihydrogen phosphate (NH4H2PO4). The pyrolysis experiments were executed to demonstrate the product distributions under different NH4H2PO4-to-poplar (PA-to-PL) ratios and pyrolysis temperatures in a lab-scale device. The results revealed that the phenol yield attained its optimal value of 4.57 wt% with a satisfactory selectivity of 20.09% at 500°C under PA-to-PL ratio of 0.6. The pyrolytic solid product obtained at this condition was then subjected to high temperature activation directly without additional activators to prepare N and P co-doped activated carbon (NPAC) as supercapacitor. The physicochemical analysis of NPAC showed that the N and P contents in NPAC reached 3.75 and 3.65 wt%, respectively. The electrochemical experiments executed in a three-electrode system indicated that the NPAC exhibited promising electrochemical performance with a satisfactory capacitance of 181.3 F g-1 at 1 A g-1.
DOI: 10.3389/fchem.2020.00436
PubMed: 32509737
PubMed Central: PMC7248177
Affiliations:
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Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Bolatibieke, Dana" sort="Bolatibieke, Dana" uniqKey="Bolatibieke D" first="Dana" last="Bolatibieke">Dana Bolatibieke</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Nan, Dong Hong" sort="Nan, Dong Hong" uniqKey="Nan D" first="Dong-Hong" last="Nan">Dong-Hong Nan</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Lu, Qiang" sort="Lu, Qiang" uniqKey="Lu Q" first="Qiang" last="Lu">Qiang Lu</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country 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Ammonium Dihydrogen Phosphate for Polygeneration of Phenol and Supercapacitor Electrode Material.</title><author><name sortKey="Li, Kai" sort="Li, Kai" uniqKey="Li K" first="Kai" last="Li">Kai Li</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Wang, Bo" sort="Wang, Bo" uniqKey="Wang B" first="Bo" last="Wang">Bo Wang</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Bolatibieke, Dana" sort="Bolatibieke, Dana" uniqKey="Bolatibieke D" first="Dana" last="Bolatibieke">Dana Bolatibieke</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Nan, Dong Hong" sort="Nan, Dong Hong" uniqKey="Nan D" first="Dong-Hong" last="Nan">Dong-Hong Nan</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author><author><name sortKey="Lu, Qiang" sort="Lu, Qiang" uniqKey="Lu Q" first="Qiang" last="Lu">Qiang Lu</name><affiliation wicri:level="3"><nlm:affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing</wicri:regionArea><placeName><settlement type="city">Pékin</settlement></placeName></affiliation></author></analytic><series><title level="j">Frontiers in chemistry</title><idno type="ISSN">2296-2646</idno><imprint><date when="2020" type="published">2020</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A new method was proposed for polygeneration of phenol and supercapacitor electrode material from pyrolysis of biomass impregnated with ammonium dihydrogen phosphate (NH<sub>4</sub>H<sub>2</sub>PO<sub>4</sub>). The pyrolysis experiments were executed to demonstrate the product distributions under different NH<sub>4</sub>H<sub>2</sub>PO<sub>4</sub>-to-poplar (PA-to-PL) ratios and pyrolysis temperatures in a lab-scale device. The results revealed that the phenol yield attained its optimal value of 4.57 wt% with a satisfactory selectivity of 20.09% at 500°C under PA-to-PL ratio of 0.6. The pyrolytic solid product obtained at this condition was then subjected to high temperature activation directly without additional activators to prepare N and P co-doped activated carbon (NPAC) as supercapacitor. The physicochemical analysis of NPAC showed that the N and P contents in NPAC reached 3.75 and 3.65 wt%, respectively. The electrochemical experiments executed in a three-electrode system indicated that the NPAC exhibited promising electrochemical performance with a satisfactory capacitance of 181.3 F g<sup>-1</sup> at 1 A g<sup>-1</sup>.</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">32509737</PMID><DateRevised><Year>2020</Year><Month>09</Month><Day>28</Day></DateRevised><Article PubModel="Electronic-eCollection"><Journal><ISSN IssnType="Print">2296-2646</ISSN><JournalIssue CitedMedium="Print"><Volume>8</Volume><PubDate><Year>2020</Year></PubDate></JournalIssue><Title>Frontiers in chemistry</Title><ISOAbbreviation>Front Chem</ISOAbbreviation></Journal><ArticleTitle>Pyrolysis of Biomass Impregnated With Ammonium Dihydrogen Phosphate for Polygeneration of Phenol and Supercapacitor Electrode Material.</ArticleTitle><Pagination><MedlinePgn>436</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.3389/fchem.2020.00436</ELocationID><Abstract><AbstractText>A new method was proposed for polygeneration of phenol and supercapacitor electrode material from pyrolysis of biomass impregnated with ammonium dihydrogen phosphate (NH<sub>4</sub>H<sub>2</sub>PO<sub>4</sub>). The pyrolysis experiments were executed to demonstrate the product distributions under different NH<sub>4</sub>H<sub>2</sub>PO<sub>4</sub>-to-poplar (PA-to-PL) ratios and pyrolysis temperatures in a lab-scale device. The results revealed that the phenol yield attained its optimal value of 4.57 wt% with a satisfactory selectivity of 20.09% at 500°C under PA-to-PL ratio of 0.6. The pyrolytic solid product obtained at this condition was then subjected to high temperature activation directly without additional activators to prepare N and P co-doped activated carbon (NPAC) as supercapacitor. The physicochemical analysis of NPAC showed that the N and P contents in NPAC reached 3.75 and 3.65 wt%, respectively. The electrochemical experiments executed in a three-electrode system indicated that the NPAC exhibited promising electrochemical performance with a satisfactory capacitance of 181.3 F g<sup>-1</sup> at 1 A g<sup>-1</sup>.</AbstractText><CopyrightInformation>Copyright © 2020 Li, Wang, Bolatibieke, Nan and Lu.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Li</LastName><ForeName>Kai</ForeName><Initials>K</Initials><AffiliationInfo><Affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Bo</ForeName><Initials>B</Initials><AffiliationInfo><Affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Bolatibieke</LastName><ForeName>Dana</ForeName><Initials>D</Initials><AffiliationInfo><Affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Nan</LastName><ForeName>Dong-Hong</ForeName><Initials>DH</Initials><AffiliationInfo><Affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Lu</LastName><ForeName>Qiang</ForeName><Initials>Q</Initials><AffiliationInfo><Affiliation>National Engineering Laboratory for Biomass Power Generation Equipment, North China Electric Power University, Beijing, China.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2020</Year><Month>05</Month><Day>19</Day></ArticleDate></Article><MedlineJournalInfo><Country>Switzerland</Country><MedlineTA>Front Chem</MedlineTA><NlmUniqueID>101627988</NlmUniqueID><ISSNLinking>2296-2646</ISSNLinking></MedlineJournalInfo><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">NH4H2PO4</Keyword><Keyword MajorTopicYN="N">biomass</Keyword><Keyword MajorTopicYN="N">phenol</Keyword><Keyword MajorTopicYN="N">pyrolysis</Keyword><Keyword MajorTopicYN="N">supercapacitor</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2020</Year><Month>03</Month><Day>20</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2020</Year><Month>04</Month><Day>27</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2020</Year><Month>6</Month><Day>9</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate 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