Full Utilization of Lignocellulose with Ionic Liquid Polyoxometalates in a One-Pot Three-Step Conversion.
Identifieur interne : 000705 ( Main/Curation ); précédent : 000704; suivant : 000706Full Utilization of Lignocellulose with Ionic Liquid Polyoxometalates in a One-Pot Three-Step Conversion.
Auteurs : Yiming Li [République populaire de Chine] ; Xueyan Zhang [République populaire de Chine] ; Zonghang Li [République populaire de Chine] ; Jiaying Song [République populaire de Chine] ; Xiaohong Wang [République populaire de Chine]Source :
- ChemSusChem [ 1864-564X ] ; 2019.
Abstract
The lignin-first concept is a new innovation for full utilization of lignocellulose into value-added chemicals. Ionic liquid (IL) polyoxometalates [MIMPS]2 H4 P2 Mo18 O62 [MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]2 H4 P2 Mo18 O62 achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.
DOI: 10.1002/cssc.201902503
PubMed: 31532070
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<front><div type="abstract" xml:lang="en">The lignin-first concept is a new innovation for full utilization of lignocellulose into value-added chemicals. Ionic liquid (IL) polyoxometalates [MIMPS]<sub>2</sub>
H<sub>4</sub>
P<sub>2</sub>
Mo<sub>18</sub>
O<sub>62</sub>
[MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]<sub>2</sub>
H<sub>4</sub>
P<sub>2</sub>
Mo<sub>18</sub>
O<sub>62</sub>
achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.</div>
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H<sub>4</sub>
P<sub>2</sub>
Mo<sub>18</sub>
O<sub>62</sub>
[MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]<sub>2</sub>
H<sub>4</sub>
P<sub>2</sub>
Mo<sub>18</sub>
O<sub>62</sub>
achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.</AbstractText>
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