[Determination of carbendazim residue in orange and soil using high performance liquid chromatography].
Identifieur interne : 000959 ( PubMed/Curation ); précédent : 000958; suivant : 000960[Determination of carbendazim residue in orange and soil using high performance liquid chromatography].
Auteurs : Jing Shen [République populaire de Chine] ; Jun Liu ; Jian LiuSource :
- Se pu = Chinese journal of chromatography [ 1000-8713 ] ; 2009.
English descriptors
- KwdEn :
- MESH :
- chemical , analysis : Benzimidazoles, Carbamates, Pesticide Residues, Soil, Soil Pollutants.
- analysis : Food Contamination.
- chemistry : Citrus sinensis.
- methods : Chromatography, High Pressure Liquid, Solid Phase Extraction.
- Sensitivity and Specificity.
Abstract
An analytical method of high performance liquid chromatography (HPLC) was established for determining carbendazim residue in orange and soil. The residue was extracted with alkaline acetonitrile, cleaned-up by NH2 solid-phase extraction (SPE), separated on a Luna C18 column (250 mm x 4.6 mm, 5 microm) using 10 mmol/L ammonium acetate solution (A) and acetonitrile (B) as the mobile phases with the gradient elution (0-->15 min, 20% B; 15-->25 min, 80% B; 25-->35 min, 20% B) at a flow rate of 1.0 mL/min, and detected at 275 nm. The method showed a linear relationship between peak area and concentration at the range of 0.02 - 5.0 mg/L for carbendazim. The average recoveries of the method ranged from 89.2% to 102% with the relative standard deviations of 1.8% - 9.1% at spiked level of 0.05 - 0.5 mg/kg. The limit of detection was 0.05 mg/kg in sarcocarp and soil, and that was 0.1 mg/kg in pericarp and whole orange. The method is characterized by simplicity, higher sensitivity and accuracy.
PubMed: 19803135
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<author><name sortKey="Shen, Jing" sort="Shen, Jing" uniqKey="Shen J" first="Jing" last="Shen">Jing Shen</name>
<affiliation wicri:level="1"><nlm:affiliation>Agricultural Testing & Information Center, Hubei Academy of Agriculture Science, Wuhan 430064, China. myshenjing@126.com</nlm:affiliation>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea>Agricultural Testing & Information Center, Hubei Academy of Agriculture Science, Wuhan 430064</wicri:regionArea>
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<author><name sortKey="Liu, Jun" sort="Liu, Jun" uniqKey="Liu J" first="Jun" last="Liu">Jun Liu</name>
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<author><name sortKey="Liu, Jian" sort="Liu, Jian" uniqKey="Liu J" first="Jian" last="Liu">Jian Liu</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en">[Determination of carbendazim residue in orange and soil using high performance liquid chromatography].</title>
<author><name sortKey="Shen, Jing" sort="Shen, Jing" uniqKey="Shen J" first="Jing" last="Shen">Jing Shen</name>
<affiliation wicri:level="1"><nlm:affiliation>Agricultural Testing & Information Center, Hubei Academy of Agriculture Science, Wuhan 430064, China. myshenjing@126.com</nlm:affiliation>
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<author><name sortKey="Liu, Jun" sort="Liu, Jun" uniqKey="Liu J" first="Jun" last="Liu">Jun Liu</name>
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<author><name sortKey="Liu, Jian" sort="Liu, Jian" uniqKey="Liu J" first="Jian" last="Liu">Jian Liu</name>
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<series><title level="j">Se pu = Chinese journal of chromatography</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Benzimidazoles (analysis)</term>
<term>Carbamates (analysis)</term>
<term>Chromatography, High Pressure Liquid (methods)</term>
<term>Citrus sinensis (chemistry)</term>
<term>Food Contamination (analysis)</term>
<term>Pesticide Residues (analysis)</term>
<term>Sensitivity and Specificity</term>
<term>Soil (analysis)</term>
<term>Soil Pollutants (analysis)</term>
<term>Solid Phase Extraction (methods)</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Benzimidazoles</term>
<term>Carbamates</term>
<term>Pesticide Residues</term>
<term>Soil</term>
<term>Soil Pollutants</term>
</keywords>
<keywords scheme="MESH" qualifier="analysis" xml:lang="en"><term>Food Contamination</term>
</keywords>
<keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Citrus sinensis</term>
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<keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Chromatography, High Pressure Liquid</term>
<term>Solid Phase Extraction</term>
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<front><div type="abstract" xml:lang="en">An analytical method of high performance liquid chromatography (HPLC) was established for determining carbendazim residue in orange and soil. The residue was extracted with alkaline acetonitrile, cleaned-up by NH2 solid-phase extraction (SPE), separated on a Luna C18 column (250 mm x 4.6 mm, 5 microm) using 10 mmol/L ammonium acetate solution (A) and acetonitrile (B) as the mobile phases with the gradient elution (0-->15 min, 20% B; 15-->25 min, 80% B; 25-->35 min, 20% B) at a flow rate of 1.0 mL/min, and detected at 275 nm. The method showed a linear relationship between peak area and concentration at the range of 0.02 - 5.0 mg/L for carbendazim. The average recoveries of the method ranged from 89.2% to 102% with the relative standard deviations of 1.8% - 9.1% at spiked level of 0.05 - 0.5 mg/kg. The limit of detection was 0.05 mg/kg in sarcocarp and soil, and that was 0.1 mg/kg in pericarp and whole orange. The method is characterized by simplicity, higher sensitivity and accuracy.</div>
</front>
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<Issue>3</Issue>
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<ArticleTitle>[Determination of carbendazim residue in orange and soil using high performance liquid chromatography].</ArticleTitle>
<Pagination><MedlinePgn>308-12</MedlinePgn>
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<Abstract><AbstractText>An analytical method of high performance liquid chromatography (HPLC) was established for determining carbendazim residue in orange and soil. The residue was extracted with alkaline acetonitrile, cleaned-up by NH2 solid-phase extraction (SPE), separated on a Luna C18 column (250 mm x 4.6 mm, 5 microm) using 10 mmol/L ammonium acetate solution (A) and acetonitrile (B) as the mobile phases with the gradient elution (0-->15 min, 20% B; 15-->25 min, 80% B; 25-->35 min, 20% B) at a flow rate of 1.0 mL/min, and detected at 275 nm. The method showed a linear relationship between peak area and concentration at the range of 0.02 - 5.0 mg/L for carbendazim. The average recoveries of the method ranged from 89.2% to 102% with the relative standard deviations of 1.8% - 9.1% at spiked level of 0.05 - 0.5 mg/kg. The limit of detection was 0.05 mg/kg in sarcocarp and soil, and that was 0.1 mg/kg in pericarp and whole orange. The method is characterized by simplicity, higher sensitivity and accuracy.</AbstractText>
</Abstract>
<AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Shen</LastName>
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<Chemical><RegistryNumber>H75J14AA89</RegistryNumber>
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