Isolation of xanthyletin, an inhibitor of ants' symbiotic fungus, by high-speed counter-current chromatography.
Identifieur interne : 000955 ( PubMed/Corpus ); précédent : 000954; suivant : 000956Isolation of xanthyletin, an inhibitor of ants' symbiotic fungus, by high-speed counter-current chromatography.
Auteurs : Cristiane De Melo Cazal ; Vanessa De Cássia Domingues ; Jaqueline Raquel Batalhão ; Odair Corrêa Bueno ; Edson Rodrigues Filho ; Maria Fátima G Fernandes Da Silva ; Paulo Cezar Vieira ; João Batista FernandesSource :
- Journal of chromatography. A [ 1873-3778 ] ; 2009.
English descriptors
- KwdEn :
- Animals, Antifungal Agents (chemistry), Antifungal Agents (isolation & purification), Ants (microbiology), Basidiomycota, Citrus (chemistry), Citrus sinensis (chemistry), Coumarins (chemistry), Coumarins (isolation & purification), Countercurrent Distribution (methods), Plant Extracts (chemistry), Plant Roots (chemistry), Solvents (chemistry), Symbiosis.
- MESH :
- chemical , chemistry : Antifungal Agents, Coumarins, Plant Extracts, Solvents.
- chemical , isolation & purification : Antifungal Agents, Coumarins.
- chemistry : Citrus, Citrus sinensis, Plant Roots.
- methods : Countercurrent Distribution.
- microbiology : Ants.
- Animals, Basidiomycota, Symbiosis.
Abstract
Xanthyletin, an inhibitor of symbiotic fungus (Leucoagaricus gongylophorus) of leaf-cutting ant (Atta sexdens rubropilosa), as well as suberosin, seselin and xanthoxyletin were isolated from Citrus sinensis grafted on Citrus limonia. A two-phase solvent system composed of hexane/ethanol/acetonitrile/water (10:8:1:1, v/v) was used for the high-speed counter-current chromatographic isolation of xanthyletin with high yield and over 99% purity as determined by liquid and gas chromatography with mass spectrometry detection. Identifications were performed by UV spectra, IR spectra, (1)H NMR and (13)C NMR.
DOI: 10.1016/j.chroma.2009.02.066
PubMed: 19296958
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pubmed:19296958Le document en format XML
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A</title><idno type="eISSN">1873-3778</idno><imprint><date when="2009" type="published">2009</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Animals</term><term>Antifungal Agents (chemistry)</term><term>Antifungal Agents (isolation & purification)</term><term>Ants (microbiology)</term><term>Basidiomycota</term><term>Citrus (chemistry)</term><term>Citrus sinensis (chemistry)</term><term>Coumarins (chemistry)</term><term>Coumarins (isolation & purification)</term><term>Countercurrent Distribution (methods)</term><term>Plant Extracts (chemistry)</term><term>Plant Roots (chemistry)</term><term>Solvents (chemistry)</term><term>Symbiosis</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Antifungal Agents</term><term>Coumarins</term><term>Plant Extracts</term><term>Solvents</term></keywords><keywords scheme="MESH" type="chemical" qualifier="isolation & purification" xml:lang="en"><term>Antifungal Agents</term><term>Coumarins</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Citrus</term><term>Citrus sinensis</term><term>Plant Roots</term></keywords><keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Countercurrent Distribution</term></keywords><keywords scheme="MESH" qualifier="microbiology" xml:lang="en"><term>Ants</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Animals</term><term>Basidiomycota</term><term>Symbiosis</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Xanthyletin, an inhibitor of symbiotic fungus (Leucoagaricus gongylophorus) of leaf-cutting ant (Atta sexdens rubropilosa), as well as suberosin, seselin and xanthoxyletin were isolated from Citrus sinensis grafted on Citrus limonia. A two-phase solvent system composed of hexane/ethanol/acetonitrile/water (10:8:1:1, v/v) was used for the high-speed counter-current chromatographic isolation of xanthyletin with high yield and over 99% purity as determined by liquid and gas chromatography with mass spectrometry detection. Identifications were performed by UV spectra, IR spectra, (1)H NMR and (13)C NMR.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">19296958</PMID><DateCreated><Year>2009</Year><Month>4</Month><Day>20</Day></DateCreated><DateCompleted><Year>2009</Year><Month>07</Month><Day>15</Day></DateCompleted><DateRevised><Year>2012</Year><Month>11</Month><Day>15</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1873-3778</ISSN><JournalIssue CitedMedium="Internet"><Volume>1216</Volume><Issue>19</Issue><PubDate><Year>2009</Year><Month>May</Month><Day>8</Day></PubDate></JournalIssue><Title>Journal of chromatography. A</Title><ISOAbbreviation>J Chromatogr A</ISOAbbreviation></Journal><ArticleTitle>Isolation of xanthyletin, an inhibitor of ants' symbiotic fungus, by high-speed counter-current chromatography.</ArticleTitle><Pagination><MedlinePgn>4307-12</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.chroma.2009.02.066</ELocationID><Abstract><AbstractText>Xanthyletin, an inhibitor of symbiotic fungus (Leucoagaricus gongylophorus) of leaf-cutting ant (Atta sexdens rubropilosa), as well as suberosin, seselin and xanthoxyletin were isolated from Citrus sinensis grafted on Citrus limonia. A two-phase solvent system composed of hexane/ethanol/acetonitrile/water (10:8:1:1, v/v) was used for the high-speed counter-current chromatographic isolation of xanthyletin with high yield and over 99% purity as determined by liquid and gas chromatography with mass spectrometry detection. Identifications were performed by UV spectra, IR spectra, (1)H NMR and (13)C NMR.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Cazal</LastName><ForeName>Cristiane de Melo</ForeName><Initials>Cde M</Initials><AffiliationInfo><Affiliation>Universidade Federal de São Carlos, Departamento de Química, SP, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Domingues</LastName><ForeName>Vanessa de Cássia</ForeName><Initials>Vde C</Initials></Author><Author ValidYN="Y"><LastName>Batalhão</LastName><ForeName>Jaqueline Raquel</ForeName><Initials>JR</Initials></Author><Author ValidYN="Y"><LastName>Bueno</LastName><ForeName>Odair Corrêa</ForeName><Initials>OC</Initials></Author><Author ValidYN="Y"><LastName>Filho</LastName><ForeName>Edson Rodrigues</ForeName><Initials>ER</Initials></Author><Author ValidYN="Y"><LastName>da Silva</LastName><ForeName>Maria Fátima G Fernandes</ForeName><Initials>MF</Initials></Author><Author ValidYN="Y"><LastName>Vieira</LastName><ForeName>Paulo Cezar</ForeName><Initials>PC</Initials></Author><Author ValidYN="Y"><LastName>Fernandes</LastName><ForeName>João Batista</ForeName><Initials>JB</Initials></Author></AuthorList><Language>ENG</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D013485">Research Support, Non-U.S. Gov't</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2009</Year><Month>Mar</Month><Day>03</Day></ArticleDate></Article><MedlineJournalInfo><Country>Netherlands</Country><MedlineTA>J Chromatogr A</MedlineTA><NlmUniqueID>9318488</NlmUniqueID><ISSNLinking>0021-9673</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D000935">Antifungal Agents</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance 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MajorTopicYN="N">Plant Extracts</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D018517" MajorTopicYN="N">Plant Roots</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D012997" MajorTopicYN="N">Solvents</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D013559" MajorTopicYN="N">Symbiosis</DescriptorName></MeshHeading></MeshHeadingList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2008</Year><Month>8</Month><Day>31</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2009</Year><Month>1</Month><Day>18</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2009</Year><Month>2</Month><Day>5</Day></PubMedPubDate><PubMedPubDate 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