Optimization of a QuEChERS based method by means of central composite design for pesticide multiresidue determination in orange juice by UHPLC-MS/MS.
Identifieur interne : 001E06 ( Ncbi/Merge ); précédent : 001E05; suivant : 001E07Optimization of a QuEChERS based method by means of central composite design for pesticide multiresidue determination in orange juice by UHPLC-MS/MS.
Auteurs : Tiele M. Rizzetti [Brésil] ; Magali Kemmerich [Brésil] ; Manoel L. Martins [Brésil] ; Osmar D. Prestes [Brésil] ; Martha B. Adaime [Brésil] ; Renato Zanella [Brésil]Source :
- Food chemistry [ 0308-8146 ] ; 2016.
English descriptors
- KwdEn :
- MESH :
- chemical , analysis : Pesticide Residues.
- analysis : Beverages.
- chemistry : Citrus sinensis, Pesticide Residues.
- methods : Chromatography, High Pressure Liquid, Tandem Mass Spectrometry.
Abstract
In this study, different extraction procedures based on the QuEChERS method were compared for the multiresidue determination of pesticides in orange juice by ultra high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS). After choosing preliminary conditions, an experimental design was carried out with the variables C18, PSA, NaOH and CH3COONa to optimize the sample preparation step. The validation results of the validation were satisfactory, since the method presented recoveries between 70% and 118%, with RSD lower than 19% for spike levels between 10 and 100 μg L(-1). The method limit of detection (LOD) and limit of quantification (LOQ) ranged from 3.0 to 7.6 μg L(-1) and from 4.9 to 26 μg L(-1), respectively. The method developed was adequate for the determination of 74 pesticide residues in orange juice.
DOI: 10.1016/j.foodchem.2015.09.010
PubMed: 26593461
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Rizzetti</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author><author><name sortKey="Kemmerich, Magali" sort="Kemmerich, Magali" uniqKey="Kemmerich M" first="Magali" last="Kemmerich">Magali Kemmerich</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author><author><name sortKey="Martins, Manoel L" sort="Martins, Manoel L" uniqKey="Martins M" first="Manoel L" last="Martins">Manoel L. Martins</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author><author><name sortKey="Prestes, Osmar D" sort="Prestes, Osmar D" uniqKey="Prestes O" first="Osmar D" last="Prestes">Osmar D. Prestes</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author><author><name sortKey="Adaime, Martha B" sort="Adaime, Martha B" uniqKey="Adaime M" first="Martha B" last="Adaime">Martha B. Adaime</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author><author><name sortKey="Zanella, Renato" sort="Zanella, Renato" uniqKey="Zanella R" first="Renato" last="Zanella">Renato Zanella</name><affiliation wicri:level="2"><nlm:affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil. Electronic address: rzanella@base.ufsm.br.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS</wicri:regionArea><placeName><region type="state">Rio Grande do Sul</region></placeName></affiliation></author></analytic><series><title level="j">Food chemistry</title><idno type="ISSN">0308-8146</idno><imprint><date when="2016" type="published">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Beverages (analysis)</term><term>Chromatography, High Pressure Liquid (methods)</term><term>Citrus sinensis (chemistry)</term><term>Pesticide Residues (analysis)</term><term>Pesticide Residues (chemistry)</term><term>Tandem Mass Spectrometry (methods)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Pesticide Residues</term></keywords><keywords scheme="MESH" qualifier="analysis" xml:lang="en"><term>Beverages</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Citrus sinensis</term><term>Pesticide Residues</term></keywords><keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Chromatography, High Pressure Liquid</term><term>Tandem Mass Spectrometry</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">In this study, different extraction procedures based on the QuEChERS method were compared for the multiresidue determination of pesticides in orange juice by ultra high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS). After choosing preliminary conditions, an experimental design was carried out with the variables C18, PSA, NaOH and CH3COONa to optimize the sample preparation step. The validation results of the validation were satisfactory, since the method presented recoveries between 70% and 118%, with RSD lower than 19% for spike levels between 10 and 100 μg L(-1). The method limit of detection (LOD) and limit of quantification (LOQ) ranged from 3.0 to 7.6 μg L(-1) and from 4.9 to 26 μg L(-1), respectively. The method developed was adequate for the determination of 74 pesticide residues in orange juice.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">26593461</PMID><DateCreated><Year>2015</Year><Month>11</Month><Day>23</Day></DateCreated><DateCompleted><Year>2016</Year><Month>07</Month><Day>21</Day></DateCompleted><DateRevised><Year>2015</Year><Month>11</Month><Day>23</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Print">0308-8146</ISSN><JournalIssue CitedMedium="Internet"><Volume>196</Volume><PubDate><Year>2016</Year><Month>Apr</Month><Day>1</Day></PubDate></JournalIssue><Title>Food chemistry</Title><ISOAbbreviation>Food Chem</ISOAbbreviation></Journal><ArticleTitle>Optimization of a QuEChERS based method by means of central composite design for pesticide multiresidue determination in orange juice by UHPLC-MS/MS.</ArticleTitle><Pagination><MedlinePgn>25-33</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.foodchem.2015.09.010</ELocationID><ELocationID EIdType="pii" ValidYN="Y">S0308-8146(15)01353-9</ELocationID><Abstract><AbstractText>In this study, different extraction procedures based on the QuEChERS method were compared for the multiresidue determination of pesticides in orange juice by ultra high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS). After choosing preliminary conditions, an experimental design was carried out with the variables C18, PSA, NaOH and CH3COONa to optimize the sample preparation step. The validation results of the validation were satisfactory, since the method presented recoveries between 70% and 118%, with RSD lower than 19% for spike levels between 10 and 100 μg L(-1). The method limit of detection (LOD) and limit of quantification (LOQ) ranged from 3.0 to 7.6 μg L(-1) and from 4.9 to 26 μg L(-1), respectively. The method developed was adequate for the determination of 74 pesticide residues in orange juice.</AbstractText><CopyrightInformation>Copyright © 2015 Elsevier Ltd. All rights reserved.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Rizzetti</LastName><ForeName>Tiele M</ForeName><Initials>TM</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Kemmerich</LastName><ForeName>Magali</ForeName><Initials>M</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Martins</LastName><ForeName>Manoel L</ForeName><Initials>ML</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Prestes</LastName><ForeName>Osmar D</ForeName><Initials>OD</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Adaime</LastName><ForeName>Martha B</ForeName><Initials>MB</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zanella</LastName><ForeName>Renato</ForeName><Initials>R</Initials><AffiliationInfo><Affiliation>Laboratório de Análise de Resíduos de Pesticidas (LARP), Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria, RS, Brazil. Electronic address: rzanella@base.ufsm.br.</Affiliation></AffiliationInfo></Author></AuthorList><Language>ENG</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D013485">Research Support, Non-U.S. Gov't</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2015</Year><Month>Sep</Month><Day>08</Day></ArticleDate></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Food Chem</MedlineTA><NlmUniqueID>7702639</NlmUniqueID><ISSNLinking>0308-8146</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D010573">Pesticide Residues</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D001628" MajorTopicYN="N">Beverages</DescriptorName><QualifierName UI="Q000032" MajorTopicYN="Y">analysis</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D002851" MajorTopicYN="N">Chromatography, High Pressure Liquid</DescriptorName><QualifierName UI="Q000379" MajorTopicYN="Y">methods</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D032084" MajorTopicYN="N">Citrus sinensis</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D010573" MajorTopicYN="N">Pesticide Residues</DescriptorName><QualifierName UI="Q000032" MajorTopicYN="N">analysis</QualifierName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D053719" MajorTopicYN="N">Tandem Mass Spectrometry</DescriptorName><QualifierName UI="Q000379" MajorTopicYN="Y">methods</QualifierName></MeshHeading></MeshHeadingList><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Central composite design</Keyword><Keyword MajorTopicYN="N">Orange juice</Keyword><Keyword MajorTopicYN="N">Pesticides</Keyword><Keyword MajorTopicYN="N">QuEChERS</Keyword><Keyword MajorTopicYN="N">UHPLC–MS/MS</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2014</Year><Month>3</Month><Day>13</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2015</Year><Month>7</Month><Day>20</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2015</Year><Month>9</Month><Day>5</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2015</Year><Month>11</Month><Day>24</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2015</Year><Month>11</Month><Day>26</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2016</Year><Month>7</Month><Day>22</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">26593461</ArticleId><ArticleId IdType="pii">S0308-8146(15)01353-9</ArticleId><ArticleId IdType="doi">10.1016/j.foodchem.2015.09.010</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>Brésil</li></country><region><li>Rio Grande do Sul</li></region></list><tree><country name="Brésil"><region name="Rio Grande do Sul"><name sortKey="Rizzetti, Tiele M" sort="Rizzetti, Tiele M" uniqKey="Rizzetti T" first="Tiele M" last="Rizzetti">Tiele M. Rizzetti</name></region><name sortKey="Adaime, Martha B" sort="Adaime, Martha B" uniqKey="Adaime M" first="Martha B" last="Adaime">Martha B. Adaime</name><name sortKey="Kemmerich, Magali" sort="Kemmerich, Magali" uniqKey="Kemmerich M" first="Magali" last="Kemmerich">Magali Kemmerich</name><name sortKey="Martins, Manoel L" sort="Martins, Manoel L" uniqKey="Martins M" first="Manoel L" last="Martins">Manoel L. Martins</name><name sortKey="Prestes, Osmar D" sort="Prestes, Osmar D" uniqKey="Prestes O" first="Osmar D" last="Prestes">Osmar D. Prestes</name><name sortKey="Zanella, Renato" sort="Zanella, Renato" uniqKey="Zanella R" first="Renato" last="Zanella">Renato Zanella</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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