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Automated HPLC-HRGC : a powerful method for essential oils analysis. V: Identification of terpene hydrocarbons of bergamot, lemon, mandarin, sweet orange, bitter orange, grapefruit, clementine and Mexican lime oils by coupled HPLC-HRGC-MS(ITD)

Identifieur interne : 003928 ( Main/Merge ); précédent : 003927; suivant : 003929

Automated HPLC-HRGC : a powerful method for essential oils analysis. V: Identification of terpene hydrocarbons of bergamot, lemon, mandarin, sweet orange, bitter orange, grapefruit, clementine and Mexican lime oils by coupled HPLC-HRGC-MS(ITD)

Auteurs : L. Mondello [Royaume-Uni] ; P. Dugo [Royaume-Uni] ; K. D. Bartle [Royaume-Uni] ; G. Dugo ; A. Cotroneo

Source :

RBID : Pascal:95-0138395

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Abstract

A fully automated HPLC-HRGC-MS(ITD) system was used for the analysis of the terpene hydrocarbon fraction of eight essential oils: bergamot, lemon, mandarin, sweet orange, bitter orange, grapefruit, clementine and Mexican lime. The system allows the isolation by LC of the hydrocarbon fraction followed by transfer into the GC and identification of the single components by MS(ITD). LC-GC-MS coupling gives more accurate results than those obtained from GC-MS analysis of the whole essential oil. The results obtained were compared with those reported in the literature, and represent a reference for the characterization of the citrus essential oils

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Pascal:95-0138395

Le document en format XML

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<term>Automation</term>
<term>Bergamot</term>
<term>Bitter orange</term>
<term>Chemical analysis</term>
<term>Chemical composition</term>
<term>Citrus aurantifolia</term>
<term>Citrus aurantium</term>
<term>Citrus fruit</term>
<term>Citrus limonum</term>
<term>Citrus paradisi</term>
<term>Citrus reticulata</term>
<term>Citrus sinensis</term>
<term>Clementine</term>
<term>Coupled method</term>
<term>Essential oil</term>
<term>Gas chromatography</term>
<term>Grapefruit</term>
<term>HPLC chromatography</term>
<term>High resolution</term>
<term>Hydrocarbon</term>
<term>Lemon</term>
<term>Mandarin</term>
<term>Mass spectrometry</term>
<term>Monoterpene</term>
<term>On line</term>
<term>Orange</term>
<term>Sesquiterpenes</term>
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<term>Analyse chimique</term>
<term>Composition chimique</term>
<term>Huile essentielle</term>
<term>Agrume</term>
<term>Bergamote</term>
<term>Citron</term>
<term>Mandarine</term>
<term>Orange</term>
<term>Bigarade</term>
<term>Pomélo</term>
<term>Clémentine</term>
<term>Citrus aurantifolia</term>
<term>Citrus paradisi</term>
<term>Citrus aurantium</term>
<term>Citrus sinensis</term>
<term>Citrus reticulata</term>
<term>Citrus limon</term>
<term>Méthode couplée</term>
<term>Chromatographie HPLC</term>
<term>Chromatographie phase gazeuse</term>
<term>Haute résolution</term>
<term>Automatisation</term>
<term>En ligne</term>
<term>Spectrométrie masse</term>
<term>Monoterpène</term>
<term>Sesquiterpène</term>
<term>Hydrocarbure</term>
<term>Citrus bergamia</term>
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<term>Huile essentielle</term>
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<div type="abstract" xml:lang="en">A fully automated HPLC-HRGC-MS(ITD) system was used for the analysis of the terpene hydrocarbon fraction of eight essential oils: bergamot, lemon, mandarin, sweet orange, bitter orange, grapefruit, clementine and Mexican lime. The system allows the isolation by LC of the hydrocarbon fraction followed by transfer into the GC and identification of the single components by MS(ITD). LC-GC-MS coupling gives more accurate results than those obtained from GC-MS analysis of the whole essential oil. The results obtained were compared with those reported in the literature, and represent a reference for the characterization of the citrus essential oils</div>
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