Differentiation of Aurantii Fructus Immaturus from Poniciri Trifoliatae Fructus Immaturus using Flow- injection Mass spectrometric (FIMS) Metabolic Fingerprinting Method Combined with Chemometrics
Identifieur interne : 000B32 ( Main/Merge ); précédent : 000B31; suivant : 000B33Differentiation of Aurantii Fructus Immaturus from Poniciri Trifoliatae Fructus Immaturus using Flow- injection Mass spectrometric (FIMS) Metabolic Fingerprinting Method Combined with Chemometrics
Auteurs : Yang Zhao [États-Unis] ; Yuan-Shiun Chang [Taïwan] ; Pei Chen [États-Unis]Source :
- Journal of pharmaceutical and biomedical analysis [ 0731-7085 ] ; 2014.
Abstract
A flow-injection mass spectrometric metabolic fingerprinting method in combination with chemometrics was used to differentiate Aurantii Fructus Immaturus from its counterfeit Poniciri Trifoliatae Fructus Immaturus. Flow-injection mass spectrometric (FIMS) fingerprints of 9 Aurantii Fructus Immaturus samples and 12 Poniciri Trifoliatae Fructus Immaturus samples were acquired and analyzed using principal component analysis (PCA) and soft independent modeling of class analogy (SIMCA). The authentic herbs were differentiated from their counterfeits easily. Eight characteristic components which were responsible for the difference between the samples were tentatively identified. Furthermore, three out of the eight components, naringin, hesperidin, and neohesperidin, were quantified. The results are useful to help identify the authenticity of Aurantii Fructus Immaturus.
Url:
DOI: 10.1016/j.jpba.2014.12.035
PubMed: 25622204
PubMed Central: 4351127
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Differentiation of Aurantii Fructus Immaturus from Poniciri Trifoliatae Fructus Immaturus using Flow- injection Mass spectrometric (FIMS) Metabolic Fingerprinting Method Combined with Chemometrics</title><author><name sortKey="Zhao, Yang" sort="Zhao, Yang" uniqKey="Zhao Y" first="Yang" last="Zhao">Yang Zhao</name><affiliation wicri:level="1"><nlm:aff id="A1"> Food Composition and Methods Development Laboratory, Beltsville Human Nutrition Research Center, Agricultural Research Service, U.S. Department of Agriculture, Building-161, BARC-East, 10300 Baltimore Avenue, Beltsville, Maryland 20705, United States</nlm:aff><country xml:lang="fr">États-Unis</country><wicri:regionArea> Food Composition and Methods Development Laboratory, Beltsville Human Nutrition Research Center, Agricultural Research Service, U.S. Department of Agriculture, Building-161, BARC-East, 10300 Baltimore Avenue, Beltsville, Maryland 20705</wicri:regionArea><wicri:noRegion>Maryland 20705</wicri:noRegion></affiliation></author><author><name sortKey="Chang, Yuan Shiun" sort="Chang, Yuan Shiun" uniqKey="Chang Y" first="Yuan-Shiun" last="Chang">Yuan-Shiun Chang</name><affiliation wicri:level="1"><nlm:aff id="A2"> Department of Chinese Pharmaceutical Sciences and Chinese Medicine Resources, College of Pharmacy, China Medical University, Taichung 40402, Taiwan</nlm:aff><country xml:lang="fr">Taïwan</country><wicri:regionArea> Department of Chinese Pharmaceutical Sciences and Chinese Medicine Resources, College of Pharmacy, China Medical University, Taichung 40402</wicri:regionArea><wicri:noRegion>Taichung 40402</wicri:noRegion></affiliation></author><author><name sortKey="Chen, Pei" sort="Chen, Pei" uniqKey="Chen P" first="Pei" last="Chen">Pei Chen</name><affiliation wicri:level="1"><nlm:aff id="A1"> Food Composition and Methods Development Laboratory, Beltsville Human Nutrition Research Center, Agricultural Research 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40402</wicri:regionArea><wicri:noRegion>Taichung 40402</wicri:noRegion></affiliation></author><author><name sortKey="Chen, Pei" sort="Chen, Pei" uniqKey="Chen P" first="Pei" last="Chen">Pei Chen</name><affiliation wicri:level="1"><nlm:aff id="A1"> Food Composition and Methods Development Laboratory, Beltsville Human Nutrition Research Center, Agricultural Research Service, U.S. Department of Agriculture, Building-161, BARC-East, 10300 Baltimore Avenue, Beltsville, Maryland 20705, United States</nlm:aff><country xml:lang="fr">États-Unis</country><wicri:regionArea> Food Composition and Methods Development Laboratory, Beltsville Human Nutrition Research Center, Agricultural Research Service, U.S. Department of Agriculture, Building-161, BARC-East, 10300 Baltimore Avenue, Beltsville, Maryland 20705</wicri:regionArea><wicri:noRegion>Maryland 20705</wicri:noRegion></affiliation></author></analytic><series><title level="j">Journal of pharmaceutical and biomedical analysis</title><idno type="ISSN">0731-7085</idno><idno type="eISSN">1873-264X</idno><imprint><date when="2014">2014</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p id="P1">A flow-injection mass spectrometric metabolic fingerprinting method in combination with chemometrics was used to differentiate Aurantii Fructus Immaturus from its counterfeit Poniciri Trifoliatae Fructus Immaturus. Flow-injection mass spectrometric (FIMS) fingerprints of 9 Aurantii Fructus Immaturus samples and 12 Poniciri Trifoliatae Fructus Immaturus samples were acquired and analyzed using principal component analysis (PCA) and soft independent modeling of class analogy (SIMCA). The authentic herbs were differentiated from their counterfeits easily. Eight characteristic components which were responsible for the difference between the samples were tentatively identified. Furthermore, three out of the eight components, naringin, hesperidin, and neohesperidin, were quantified. The results are useful to help identify the authenticity of Aurantii Fructus Immaturus.</p></div></front></TEI></record>Pour manipuler ce document sous Unix (Dilib)
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