Enhanced Characterization of the Smell of Death by Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)
Identifieur interne : 000293 ( Main/Merge ); précédent : 000292; suivant : 000294Enhanced Characterization of the Smell of Death by Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)
Auteurs : Jessica Dekeirsschieter [Belgique] ; Pierre-Hugues Stefanuto [Belgique] ; Catherine Brasseur [Belgique] ; Eric Haubruge [Belgique] ; Jean-François Focant [Belgique]Source :
- PLoS ONE [ 1932-6203 ] ; 2012.
Abstract
Soon after death, the decay process of mammalian soft tissues begins and leads to the release of cadaveric volatile compounds in the surrounding environment. The study of postmortem decomposition products is an emerging field of study in forensic science. However, a better knowledge of the smell of death and its volatile constituents may have many applications in forensic sciences. Domestic pigs are the most widely used human body analogues in forensic experiments, mainly due to ethical restrictions. Indeed, decomposition trials on human corpses are restricted in many countries worldwide. This article reports on the use of comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry (GCxGC-TOFMS) for thanatochemistry applications. A total of 832 VOCs released by a decaying pig carcass in terrestrial ecosystem,
Url:
DOI: 10.1371/journal.pone.0039005
PubMed: 22723918
PubMed Central: 3377612
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Enhanced Characterization of the Smell of Death by Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)</title><author><name sortKey="Dekeirsschieter, Jessica" sort="Dekeirsschieter, Jessica" uniqKey="Dekeirsschieter J" first="Jessica" last="Dekeirsschieter">Jessica Dekeirsschieter</name><affiliation wicri:level="4"><nlm:aff id="aff1"><addr-line>Department of Functional and Evolutionary Entomology, Gembloux Agro-Bio Tech, University of Liege, Gembloux, Belgium</addr-line></nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Functional and Evolutionary Entomology, Gembloux Agro-Bio Tech, University of Liege, Gembloux</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de 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Gembloux</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author><author><name sortKey="Stefanuto, Pierre Hugues" sort="Stefanuto, Pierre Hugues" uniqKey="Stefanuto P" first="Pierre-Hugues" last="Stefanuto">Pierre-Hugues Stefanuto</name><affiliation wicri:level="4"><nlm:aff id="aff2"><addr-line>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege, Belgium</addr-line></nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author><author><name sortKey="Brasseur, Catherine" sort="Brasseur, Catherine" uniqKey="Brasseur C" first="Catherine" last="Brasseur">Catherine Brasseur</name><affiliation wicri:level="4"><nlm:aff id="aff2"><addr-line>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege, Belgium</addr-line></nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author><author><name sortKey="Haubruge, Eric" sort="Haubruge, Eric" uniqKey="Haubruge E" first="Eric" last="Haubruge">Eric Haubruge</name><affiliation wicri:level="4"><nlm:aff id="aff1"><addr-line>Department of Functional and Evolutionary Entomology, Gembloux Agro-Bio Tech, University of Liege, Gembloux, Belgium</addr-line></nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Functional and Evolutionary Entomology, Gembloux Agro-Bio Tech, University of Liege, Gembloux</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author><author><name sortKey="Focant, Jean Francois" sort="Focant, Jean Francois" uniqKey="Focant J" first="Jean-François" last="Focant">Jean-François Focant</name><affiliation wicri:level="4"><nlm:aff id="aff2"><addr-line>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege, Belgium</addr-line></nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Chemistry, Organic and Biological Analytical Chemistry, CART, University of Liege, Liege</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author></analytic><series><title level="j">PLoS ONE</title><idno type="eISSN">1932-6203</idno><imprint><date when="2012">2012</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>Soon after death, the decay process of mammalian soft tissues begins and leads to the release of cadaveric volatile compounds in the surrounding environment. The study of postmortem decomposition products is an emerging field of study in forensic science. However, a better knowledge of the smell of death and its volatile constituents may have many applications in forensic sciences. Domestic pigs are the most widely used human body analogues in forensic experiments, mainly due to ethical restrictions. Indeed, decomposition trials on human corpses are restricted in many countries worldwide. This article reports on the use of comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry (GCxGC-TOFMS) for thanatochemistry applications. A total of 832 VOCs released by a decaying pig carcass in terrestrial ecosystem, <italic>i.e</italic>. a forest biotope, were identified by GCxGC-TOFMS. These postmortem compounds belong to many kinds of chemical class, mainly oxygen compounds (alcohols, acids, ketones, aldehydes, esters), sulfur and nitrogen compounds, aromatic compounds such as phenolic molecules and hydrocarbons. The use of GCxGC-TOFMS in study of postmortem volatile compounds instead of conventional GC-MS was successful.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Vass, Aa" uniqKey="Vass A">AA Vass</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Vass, Aa" uniqKey="Vass A">AA Vass</name></author><author><name sortKey="Barshick, Sa" uniqKey="Barshick S">SA Barshick</name></author><author><name sortKey="Sega, G" uniqKey="Sega G">G Sega</name></author><author><name sortKey="Caton, J" uniqKey="Caton J">J Caton</name></author><author><name sortKey="Skeen, Jt" uniqKey="Skeen J">JT Skeen</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Statheropoulos, M" uniqKey="Statheropoulos M">M Statheropoulos</name></author><author><name sortKey="Spiliopoulou, C" uniqKey="Spiliopoulou C">C Spiliopoulou</name></author><author><name sortKey="Agapiou, A" uniqKey="Agapiou A">A 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Rees</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Keller, T" uniqKey="Keller T">T Keller</name></author><author><name sortKey="Schneider, A" uniqKey="Schneider A">A Schneider</name></author><author><name sortKey="Tutsch Bauer, E" uniqKey="Tutsch Bauer E">E Tutsch-Bauer</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Kaliste, E" uniqKey="Kaliste E">E Kaliste</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Paterson, S" uniqKey="Paterson S">S Paterson</name></author><author><name sortKey="Cordero, R" uniqKey="Cordero R">R Cordero</name></author><author><name sortKey="Burlinson, S" uniqKey="Burlinson S">S Burlinson</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Kusano, M" uniqKey="Kusano M">M Kusano</name></author><author><name sortKey="Medez, E" uniqKey="Medez E">E Medez</name></author><author><name sortKey="Furton, Kg" uniqKey="Furton K">KG Furton</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Kovatsi, L" uniqKey="Kovatsi L">L Kovatsi</name></author><author><name sortKey="Giannakis, D" uniqKey="Giannakis D">D Giannakis</name></author><author><name sortKey="Arzoglou, V" uniqKey="Arzoglou V">V Arzoglou</name></author><author><name sortKey="Samanidou, V" uniqKey="Samanidou V">V Samanidou</name></author></analytic></biblStruct></listBibl></div1></back></TEI></record>Pour manipuler ce document sous Unix (Dilib)
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