Four-step iron(ii) spin state cascade driven by antagonistic solid state interactions.
Identifieur interne : 000C14 ( PubMed/Checkpoint ); précédent : 000C13; suivant : 000C15Four-step iron(ii) spin state cascade driven by antagonistic solid state interactions.
Auteurs : Natasha F. Sciortino ; Katrina A. Zenere ; Maggie E. Corrigan ; Gregory J. Halder [États-Unis] ; Guillaume Chastanet [France] ; Jean-François Létard [France] ; Cameron J. Kepert ; Suzanne M. NevilleSource :
- Chemical science [ 2041-6520 ] ; 2017.
Abstract
A four-stepped cascade of Fe(ii) high spin (HS) to low spin (LS) states is demonstrated in a family of 2-D Hofmann materials, [Fe3(II)(saltrz)6(M(II)(CN)4)3]·8(H2O) (M(II) = Pd (1(Pd) ), Pt (1(Pt) ); saltrz = (E)-2-(((4H-1,2,4-triazol-4-yl)imino)methyl)phenol). Alongside the fully HS and LS Fe(ii) states, fractional spin state stabilization occurs at HS/LS values of 5/6, 2/3, and 1/6. This unconventional spin state periodicity is driven by the presence of multiple spin crossover (SCO) active Fe(ii) sites which are in subtly distinct environments driven by a network of antagonistic host-host and host-guest interactions. Alternating long- and short-range magnetostructural ordering is achieved over the five distinct spin state ratios HS(1.0)LS(0.0), HS(0.833)LS(0.167), HS(0.667)LS(0.333), HS(0.167)LS(0.833), and HS(0.0)LS(1.0) owing to the flexibility of this 2-D interdigitated lattice topology interconnected by intermolecular interactions. A distinct wave-like spin state patterning is structurally evidenced for each intermediate phase.
DOI: 10.1039/c6sc03114e
PubMed: 28451220
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Sciortino</name><affiliation><nlm:affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</nlm:affiliation><wicri:noCountry code="subField">Australia </wicri:noCountry></affiliation></author><author><name sortKey="Zenere, Katrina A" sort="Zenere, Katrina A" uniqKey="Zenere K" first="Katrina A" last="Zenere">Katrina A. Zenere</name><affiliation><nlm:affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</nlm:affiliation><wicri:noCountry code="subField">Australia </wicri:noCountry></affiliation></author><author><name sortKey="Corrigan, Maggie E" sort="Corrigan, Maggie E" uniqKey="Corrigan M" first="Maggie E" last="Corrigan">Maggie E. Corrigan</name><affiliation><nlm:affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</nlm:affiliation><wicri:noCountry code="subField">Australia </wicri:noCountry></affiliation></author><author><name sortKey="Halder, Gregory J" sort="Halder, Gregory J" uniqKey="Halder G" first="Gregory J" last="Halder">Gregory J. Halder</name><affiliation wicri:level="2"><nlm:affiliation>X-ray Science Division , Advanced Photon Source , Argonne National Laboratory , IL 60439 , USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>X-ray Science Division , Advanced Photon Source , Argonne National Laboratory , IL 60439 </wicri:regionArea><placeName><region type="state">Illinois</region></placeName></affiliation></author><author><name sortKey="Chastanet, Guillaume" sort="Chastanet, Guillaume" uniqKey="Chastanet G" first="Guillaume" last="Chastanet">Guillaume Chastanet</name><affiliation wicri:level="3"><nlm:affiliation>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac , France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac </wicri:regionArea><placeName><region type="region" nuts="2">Nouvelle-Aquitaine</region><region type="old region" nuts="2">Aquitaine</region><settlement type="city">, Pessac </settlement></placeName></affiliation></author><author><name sortKey="Letard, Jean Francois" sort="Letard, Jean Francois" uniqKey="Letard J" first="Jean-François" last="Létard">Jean-François Létard</name><affiliation wicri:level="3"><nlm:affiliation>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac , France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac </wicri:regionArea><placeName><region type="region" nuts="2">Nouvelle-Aquitaine</region><region type="old region" nuts="2">Aquitaine</region><settlement type="city">, Pessac </settlement></placeName></affiliation></author><author><name sortKey="Kepert, Cameron J" sort="Kepert, Cameron J" uniqKey="Kepert C" first="Cameron J" last="Kepert">Cameron J. Kepert</name><affiliation><nlm:affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</nlm:affiliation><wicri:noCountry code="subField">Australia </wicri:noCountry></affiliation></author><author><name sortKey="Neville, Suzanne M" sort="Neville, Suzanne M" uniqKey="Neville S" first="Suzanne M" last="Neville">Suzanne M. Neville</name><affiliation><nlm:affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</nlm:affiliation><wicri:noCountry code="subField">Australia </wicri:noCountry></affiliation></author></analytic><series><title level="j">Chemical science</title><idno type="ISSN">2041-6520</idno><imprint><date when="2017" type="published">2017</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A four-stepped cascade of Fe(ii) high spin (HS) to low spin (LS) states is demonstrated in a family of 2-D Hofmann materials, [Fe3(II)(saltrz)6(M(II)(CN)4)3]·8(H2O) (M(II) = Pd (1(Pd) ), Pt (1(Pt) ); saltrz = (E)-2-(((4H-1,2,4-triazol-4-yl)imino)methyl)phenol). Alongside the fully HS and LS Fe(ii) states, fractional spin state stabilization occurs at HS/LS values of 5/6, 2/3, and 1/6. This unconventional spin state periodicity is driven by the presence of multiple spin crossover (SCO) active Fe(ii) sites which are in subtly distinct environments driven by a network of antagonistic host-host and host-guest interactions. Alternating long- and short-range magnetostructural ordering is achieved over the five distinct spin state ratios HS(1.0)LS(0.0), HS(0.833)LS(0.167), HS(0.667)LS(0.333), HS(0.167)LS(0.833), and HS(0.0)LS(1.0) owing to the flexibility of this 2-D interdigitated lattice topology interconnected by intermolecular interactions. A distinct wave-like spin state patterning is structurally evidenced for each intermediate phase.</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">28451220</PMID><DateCreated><Year>2017</Year><Month>04</Month><Day>28</Day></DateCreated><DateRevised><Year>2017</Year><Month>08</Month><Day>16</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Print">2041-6520</ISSN><JournalIssue CitedMedium="Print"><Volume>8</Volume><Issue>1</Issue><PubDate><Year>2017</Year><Month>Jan</Month><Day>01</Day></PubDate></JournalIssue><Title>Chemical science</Title><ISOAbbreviation>Chem Sci</ISOAbbreviation></Journal><ArticleTitle>Four-step iron(ii) spin state cascade driven by antagonistic solid state interactions.</ArticleTitle><Pagination><MedlinePgn>701-707</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1039/c6sc03114e</ELocationID><Abstract><AbstractText>A four-stepped cascade of Fe(ii) high spin (HS) to low spin (LS) states is demonstrated in a family of 2-D Hofmann materials, [Fe3(II)(saltrz)6(M(II)(CN)4)3]·8(H2O) (M(II) = Pd (1(Pd) ), Pt (1(Pt) ); saltrz = (E)-2-(((4H-1,2,4-triazol-4-yl)imino)methyl)phenol). Alongside the fully HS and LS Fe(ii) states, fractional spin state stabilization occurs at HS/LS values of 5/6, 2/3, and 1/6. This unconventional spin state periodicity is driven by the presence of multiple spin crossover (SCO) active Fe(ii) sites which are in subtly distinct environments driven by a network of antagonistic host-host and host-guest interactions. Alternating long- and short-range magnetostructural ordering is achieved over the five distinct spin state ratios HS(1.0)LS(0.0), HS(0.833)LS(0.167), HS(0.667)LS(0.333), HS(0.167)LS(0.833), and HS(0.0)LS(1.0) owing to the flexibility of this 2-D interdigitated lattice topology interconnected by intermolecular interactions. A distinct wave-like spin state patterning is structurally evidenced for each intermediate phase.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Sciortino</LastName><ForeName>Natasha F</ForeName><Initials>NF</Initials><AffiliationInfo><Affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zenere</LastName><ForeName>Katrina A</ForeName><Initials>KA</Initials><AffiliationInfo><Affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Corrigan</LastName><ForeName>Maggie E</ForeName><Initials>ME</Initials><AffiliationInfo><Affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Halder</LastName><ForeName>Gregory J</ForeName><Initials>GJ</Initials><AffiliationInfo><Affiliation>X-ray Science Division , Advanced Photon Source , Argonne National Laboratory , IL 60439 , USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Chastanet</LastName><ForeName>Guillaume</ForeName><Initials>G</Initials><AffiliationInfo><Affiliation>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac , France.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Létard</LastName><ForeName>Jean-François</ForeName><Initials>JF</Initials><AffiliationInfo><Affiliation>CNRS , Univ. Bordeaux , ICMCB , UPR 9048 , F-33600 , Pessac , France.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Kepert</LastName><ForeName>Cameron J</ForeName><Initials>CJ</Initials><AffiliationInfo><Affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Neville</LastName><ForeName>Suzanne M</ForeName><Initials>SM</Initials><AffiliationInfo><Affiliation>School of Chemistry , The University of Sydney , NSW 2006 , Australia . Email: suzanne.neville@sydney.edu.au ; Tel: +61-2-9351-7791.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2016</Year><Month>09</Month><Day>12</Day></ArticleDate></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Chem Sci</MedlineTA><NlmUniqueID>101545951</NlmUniqueID><ISSNLinking>2041-6520</ISSNLinking></MedlineJournalInfo><CommentsCorrectionsList><CommentsCorrections RefType="Cites"><RefSource>Inorg Chem. 2014 Aug 4;53(15):7886-93</RefSource><PMID Version="1">25046355</PMID></CommentsCorrections><CommentsCorrections RefType="Cites"><RefSource>J Am Chem Soc. 2010 Mar 17;132(10):3553-60</RefSource><PMID Version="1">20158241</PMID></CommentsCorrections><CommentsCorrections RefType="Cites"><RefSource>Chem Soc Rev. 2011 Jul;40(7):4119-42</RefSource><PMID 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Version="1">23504535</PMID></CommentsCorrections><CommentsCorrections RefType="Cites"><RefSource>Angew Chem Int Ed Engl. 2003 Aug 18;42(32):3825-30</RefSource><PMID Version="1">12923856</PMID></CommentsCorrections></CommentsCorrectionsList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2016</Year><Month>07</Month><Day>14</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2016</Year><Month>09</Month><Day>11</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2017</Year><Month>4</Month><Day>29</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2017</Year><Month>4</Month><Day>30</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2017</Year><Month>4</Month><Day>30</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">28451220</ArticleId><ArticleId 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Corrigan</name><name sortKey="Kepert, Cameron J" sort="Kepert, Cameron J" uniqKey="Kepert C" first="Cameron J" last="Kepert">Cameron J. Kepert</name><name sortKey="Neville, Suzanne M" sort="Neville, Suzanne M" uniqKey="Neville S" first="Suzanne M" last="Neville">Suzanne M. Neville</name><name sortKey="Sciortino, Natasha F" sort="Sciortino, Natasha F" uniqKey="Sciortino N" first="Natasha F" last="Sciortino">Natasha F. Sciortino</name><name sortKey="Zenere, Katrina A" sort="Zenere, Katrina A" uniqKey="Zenere K" first="Katrina A" last="Zenere">Katrina A. Zenere</name></noCountry><country name="États-Unis"><region name="Illinois"><name sortKey="Halder, Gregory J" sort="Halder, Gregory J" uniqKey="Halder G" first="Gregory J" last="Halder">Gregory J. Halder</name></region></country><country name="France"><region name="Nouvelle-Aquitaine"><name sortKey="Chastanet, Guillaume" sort="Chastanet, Guillaume" uniqKey="Chastanet G" first="Guillaume" last="Chastanet">Guillaume Chastanet</name></region><name sortKey="Letard, Jean Francois" sort="Letard, Jean Francois" uniqKey="Letard J" first="Jean-François" last="Létard">Jean-François Létard</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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