High di-electric constant nano-structure ceramics synthesis using novel electric discharge assisted mechanical milling and magneto ball milling and its properties
Identifieur interne :
005D34 ( PascalFrancis/Curation );
précédent :
005D33;
suivant :
005D35
High di-electric constant nano-structure ceramics synthesis using novel electric discharge assisted mechanical milling and magneto ball milling and its properties
Auteurs : A. A. Chowdhury [
Australie] ;
A. Calka [
Australie] ;
D. Wexler [
Australie] ;
K. Konstantinov [
Australie]
Source :
-
International journal of nanotechnology [ 1475-7435 ] ; 2014.
RBID : Pascal:15-0016262
Descripteurs français
- Pascal (Inist)
- Décharge électrique,
Alliage mécanique,
Céramique oxyde,
Réaction état solide,
Frittage,
Traitement thermique,
Précurseur,
Nanopoudre,
Diffraction RX,
Microscopie électronique transmission,
Microscopie électronique balayage,
CaCu3Ti4O12,
8107W.
English descriptors
- KwdEn :
- Electric discharges,
Heat treatments,
Mechanical alloying,
Nanopowder,
Oxide ceramics,
Precursor,
Scanning electron microscopy,
Sintering,
Solid state reaction,
Transmission electron microscopy,
XRD.
Abstract
The conventional method to prepare functional oxides is ceramic-powder-based processing typically via solid-state reaction of microcrystalline starting powders at high temperatures. Disadvantages of this approach include the high temperatures of reaction, limited degree of product chemical homogeneity and difficulties in achieving rapid sintering. Various chemical-based processing routes have been developed to prepare powders of more homogeneous composition, improved reactivity and sintering ability at low temperatures. Regardless of the route chosen to synthesise complex oxides, almost all of them require lengthy heat treatment schedules that usually exceed 10 h, as well as multi-stage processing steps. We describe two approaches to address these problems, applied to successful synthesis of both MgAl2O4 and CaCu3Ti4O12 (CCT) oxides exhibiting excellent di-electric properties. One approach employed the novel direct synthesis technique of electric discharge assisted mechanical milling (EDAMM) and the second used the more conventional method of controlled ball milling using the magneto-mechanical method followed by heat treatment of nano-structural products. By using EDAMM, nano-crystalline precursors for transformation into high di-electric constant ceramics could be formed in as little as 0.1% of the processing time required for conventional solid-state techniques while ball milling using the magneto method also resulted in nano-structural precursors powders suitable for reaction by heat treatment to form oxide supercapacitor. Sample characterisation was carried out using XRD, TEM and SEM. Di-electric property measurements were performed using AC-LCR and by DC meters.
| pA |
| A01 | 01 | 1 | | @0 1475-7435 |
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| A03 | | 1 | | @0 Int. j. nanotechnol. |
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| A05 | | | | @2 11 |
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| A06 | | | | @2 9-11 |
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| A08 | 01 | 1 | ENG | @1 High di-electric constant nano-structure ceramics synthesis using novel electric discharge assisted mechanical milling and magneto ball milling and its properties |
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| A09 | 01 | 1 | ENG | @1 Symposium 'Nanomaterials for Energy Conversion and Storage' |
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| A11 | 01 | 1 | | @1 CHOWDHURY (A. A.) |
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| A11 | 02 | 1 | | @1 CALKA (A.) |
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| A11 | 03 | 1 | | @1 WEXLER (D.) |
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| A11 | 04 | 1 | | @1 KONSTANTINOV (K.) |
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| A12 | 01 | 1 | | @1 CABOT (Andreu) @9 ed. |
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| A12 | 02 | 1 | | @1 LIU (Hong) @9 ed. |
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| A12 | 03 | 1 | | @1 ROBINSON (Richard D.) @9 ed. |
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| A14 | 01 | | | @1 School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong @2 NSW 2522 @3 AUS @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut. |
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| A15 | 01 | | | @1 Catalonia Institute for Energy Research - IREC, Sant Adrià del Besos @2 08930 Barcelona @3 ESP @Z 1 aut. |
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| A15 | 02 | | | @1 Institució Catalana de Recerca i Estudis Avançats - ICREA @2 Barcelona 08010 @3 ESP @Z 1 aut. |
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| A15 | 03 | | | @1 State Key Laboratory of Crystal Materials, Center of Bio & Micro/nano Functional Materials, Shandong University, 27 Shandanan Road @2 Jinan 250100 @3 CHN @Z 2 aut. |
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| A15 | 04 | | | @1 Department of Materials Science and Engineering, Cornell University @2 Ithaca, New York 14853 @3 USA @Z 3 aut. |
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| A18 | 01 | 1 | | @1 European Materials Research Society (E-MRS) @2 Strasbourg @3 FRA @9 org-cong. |
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| A23 | 01 | | | @0 ENG |
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| A43 | 01 | | | @1 INIST @2 27530 @5 354000502541020010 |
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| A44 | | | | @0 0000 @1 © 2015 INIST-CNRS. All rights reserved. |
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| A47 | 01 | 1 | | @0 15-0016262 |
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| A60 | | | | @1 P @2 C |
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| A64 | 01 | 1 | | @0 International journal of nanotechnology |
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| A66 | 01 | | | @0 CHE |
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| C01 | 01 | | ENG | @0 The conventional method to prepare functional oxides is ceramic-powder-based processing typically via solid-state reaction of microcrystalline starting powders at high temperatures. Disadvantages of this approach include the high temperatures of reaction, limited degree of product chemical homogeneity and difficulties in achieving rapid sintering. Various chemical-based processing routes have been developed to prepare powders of more homogeneous composition, improved reactivity and sintering ability at low temperatures. Regardless of the route chosen to synthesise complex oxides, almost all of them require lengthy heat treatment schedules that usually exceed 10 h, as well as multi-stage processing steps. We describe two approaches to address these problems, applied to successful synthesis of both MgAl2O4 and CaCu3Ti4O12 (CCT) oxides exhibiting excellent di-electric properties. One approach employed the novel direct synthesis technique of electric discharge assisted mechanical milling (EDAMM) and the second used the more conventional method of controlled ball milling using the magneto-mechanical method followed by heat treatment of nano-structural products. By using EDAMM, nano-crystalline precursors for transformation into high di-electric constant ceramics could be formed in as little as 0.1% of the processing time required for conventional solid-state techniques while ball milling using the magneto method also resulted in nano-structural precursors powders suitable for reaction by heat treatment to form oxide supercapacitor. Sample characterisation was carried out using XRD, TEM and SEM. Di-electric property measurements were performed using AC-LCR and by DC meters. |
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| C02 | 01 | 3 | | @0 001B80A07W |
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| C03 | 01 | 3 | FRE | @0 Décharge électrique @5 01 |
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| C03 | 01 | 3 | ENG | @0 Electric discharges @5 01 |
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| C03 | 02 | 3 | FRE | @0 Alliage mécanique @5 02 |
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| C03 | 02 | 3 | ENG | @0 Mechanical alloying @5 02 |
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| C03 | 03 | X | FRE | @0 Céramique oxyde @5 03 |
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| C03 | 03 | X | ENG | @0 Oxide ceramics @5 03 |
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| C03 | 03 | X | SPA | @0 Cerámica óxido @5 03 |
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| C03 | 04 | X | FRE | @0 Réaction état solide @5 04 |
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| C03 | 04 | X | ENG | @0 Solid state reaction @5 04 |
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| C03 | 04 | X | SPA | @0 Reacción estado sólido @5 04 |
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| C03 | 05 | 3 | FRE | @0 Frittage @5 05 |
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| C03 | 05 | 3 | ENG | @0 Sintering @5 05 |
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| C03 | 06 | 3 | FRE | @0 Traitement thermique @5 06 |
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| C03 | 06 | 3 | ENG | @0 Heat treatments @5 06 |
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| C03 | 07 | 3 | FRE | @0 Précurseur @5 07 |
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| C03 | 07 | 3 | ENG | @0 Precursor @5 07 |
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| C03 | 08 | X | FRE | @0 Nanopoudre @5 08 |
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| C03 | 08 | X | ENG | @0 Nanopowder @5 08 |
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| C03 | 08 | X | SPA | @0 Nanopolvo @5 08 |
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| C03 | 09 | 3 | FRE | @0 Diffraction RX @5 09 |
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| C03 | 09 | 3 | ENG | @0 XRD @5 09 |
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| C03 | 10 | 3 | FRE | @0 Microscopie électronique transmission @5 10 |
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| C03 | 10 | 3 | ENG | @0 Transmission electron microscopy @5 10 |
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| C03 | 11 | 3 | FRE | @0 Microscopie électronique balayage @5 11 |
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| C03 | 11 | 3 | ENG | @0 Scanning electron microscopy @5 11 |
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| C03 | 12 | 3 | FRE | @0 CaCu3Ti4O12 @4 INC @5 46 |
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| C03 | 13 | 3 | FRE | @0 8107W @4 INC @5 71 |
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| N21 | | | | @1 019 |
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| N44 | 01 | | | @1 OTO |
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| N82 | | | | @1 OTO |
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| pR |
| A30 | 01 | 1 | ENG | @1 European Materials Research Society Spring Meeting. Symposium 'Nanomaterials for Energy Conversion and Storage' @3 Strasbourg FRA @4 2013-05-27 |
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Le document en format XML
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</affiliation><series><title level="j" type="main">International journal of nanotechnology</title>
<title level="j" type="abbreviated">Int. j. nanotechnol.</title>
<idno type="ISSN">1475-7435</idno>
<imprint><date when="2014">2014</date>
</imprint><seriesStmt><title level="j" type="main">International journal of nanotechnology</title>
<title level="j" type="abbreviated">Int. j. nanotechnol.</title>
<idno type="ISSN">1475-7435</idno>
</seriesStmt><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Electric discharges</term>
<term>Heat treatments</term>
<term>Mechanical alloying</term>
<term>Nanopowder</term>
<term>Oxide ceramics</term>
<term>Precursor</term>
<term>Scanning electron microscopy</term>
<term>Sintering</term>
<term>Solid state reaction</term>
<term>Transmission electron microscopy</term>
<term>XRD</term>
</keywords><keywords scheme="Pascal" xml:lang="fr"><term>Décharge électrique</term>
<term>Alliage mécanique</term>
<term>Céramique oxyde</term>
<term>Réaction état solide</term>
<term>Frittage</term>
<term>Traitement thermique</term>
<term>Précurseur</term>
<term>Nanopoudre</term>
<term>Diffraction RX</term>
<term>Microscopie électronique transmission</term>
<term>Microscopie électronique balayage</term>
<term>CaCu3Ti4O12</term>
<term>8107W</term>
</keywords><front><div type="abstract" xml:lang="en">The conventional method to prepare functional oxides is ceramic-powder-based processing typically via solid-state reaction of microcrystalline starting powders at high temperatures. Disadvantages of this approach include the high temperatures of reaction, limited degree of product chemical homogeneity and difficulties in achieving rapid sintering. Various chemical-based processing routes have been developed to prepare powders of more homogeneous composition, improved reactivity and sintering ability at low temperatures. Regardless of the route chosen to synthesise complex oxides, almost all of them require lengthy heat treatment schedules that usually exceed 10 h, as well as multi-stage processing steps. We describe two approaches to address these problems, applied to successful synthesis of both MgAl<sub>2</sub>
O<sub>4</sub>
and CaCu<sub>3</sub>
Ti<sub>4</sub>
O<sub>12</sub>
(CCT) oxides exhibiting excellent di-electric properties. One approach employed the novel direct synthesis technique of electric discharge assisted mechanical milling (EDAMM) and the second used the more conventional method of controlled ball milling using the magneto-mechanical method followed by heat treatment of nano-structural products. By using EDAMM, nano-crystalline precursors for transformation into high di-electric constant ceramics could be formed in as little as 0.1% of the processing time required for conventional solid-state techniques while ball milling using the magneto method also resulted in nano-structural precursors powders suitable for reaction by heat treatment to form oxide supercapacitor. Sample characterisation was carried out using XRD, TEM and SEM. Di-electric property measurements were performed using AC-LCR and by DC meters.</div><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>1475-7435</s0>
</fA01><fA03 i2="1"><s0>Int. j. nanotechnol.</s0>
</fA03><fA06><s2>9-11</s2>
</fA06><fA08 i1="01" i2="1" l="ENG"><s1>High di-electric constant nano-structure ceramics synthesis using novel electric discharge assisted mechanical milling and magneto ball milling and its properties</s1>
</fA08><fA09 i1="01" i2="1" l="ENG"><s1>Symposium 'Nanomaterials for Energy Conversion and Storage'</s1>
</fA09><fA11 i1="01" i2="1"><s1>CHOWDHURY (A. A.)</s1>
</fA11><fA11 i1="02" i2="1"><s1>CALKA (A.)</s1>
</fA11><fA11 i1="03" i2="1"><s1>WEXLER (D.)</s1>
</fA11><fA11 i1="04" i2="1"><s1>KONSTANTINOV (K.)</s1>
</fA11><fA12 i1="01" i2="1"><s1>CABOT (Andreu)</s1>
<s9>ed.</s9>
</fA12><fA12 i1="02" i2="1"><s1>LIU (Hong)</s1>
<s9>ed.</s9>
</fA12><fA12 i1="03" i2="1"><s1>ROBINSON (Richard D.)</s1>
<s9>ed.</s9>
</fA12><fA14 i1="01"><s1>School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong</s1>
<s2>NSW 2522</s2>
<s3>AUS</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</fA14><fA15 i1="01"><s1>Catalonia Institute for Energy Research - IREC, Sant Adrià del Besos</s1>
<s2>08930 Barcelona</s2>
<s3>ESP</s3>
<sZ>1 aut.</sZ>
</fA15><fA15 i1="02"><s1>Institució Catalana de Recerca i Estudis Avançats - ICREA</s1>
<s2>Barcelona 08010</s2>
<s3>ESP</s3>
<sZ>1 aut.</sZ>
</fA15><fA15 i1="03"><s1>State Key Laboratory of Crystal Materials, Center of Bio & Micro/nano Functional Materials, Shandong University, 27 Shandanan Road</s1>
<s2>Jinan 250100</s2>
<s3>CHN</s3>
<sZ>2 aut.</sZ>
</fA15><fA15 i1="04"><s1>Department of Materials Science and Engineering, Cornell University</s1>
<s2>Ithaca, New York 14853</s2>
<s3>USA</s3>
<sZ>3 aut.</sZ>
</fA15><fA18 i1="01" i2="1"><s1>European Materials Research Society (E-MRS)</s1>
<s2>Strasbourg</s2>
<s3>FRA</s3>
<s9>org-cong.</s9>
</fA18><fA20><s1>728-736</s1>
</fA20><fA21><s1>2014</s1>
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<s2>27530</s2>
<s5>354000502541020010</s5>
</fA43><fA44><s0>0000</s0>
<s1>© 2015 INIST-CNRS. All rights reserved.</s1>
</fA44><fA45><s0>19 ref.</s0>
</fA45><fA47 i1="01" i2="1"><s0>15-0016262</s0>
</fA47><fA60><s1>P</s1>
<s2>C</s2>
</fA60><fA64 i1="01" i2="1"><s0>International journal of nanotechnology</s0>
</fA64><fA66 i1="01"><s0>CHE</s0>
</fA66><fC01 i1="01" l="ENG"><s0>The conventional method to prepare functional oxides is ceramic-powder-based processing typically via solid-state reaction of microcrystalline starting powders at high temperatures. Disadvantages of this approach include the high temperatures of reaction, limited degree of product chemical homogeneity and difficulties in achieving rapid sintering. Various chemical-based processing routes have been developed to prepare powders of more homogeneous composition, improved reactivity and sintering ability at low temperatures. Regardless of the route chosen to synthesise complex oxides, almost all of them require lengthy heat treatment schedules that usually exceed 10 h, as well as multi-stage processing steps. We describe two approaches to address these problems, applied to successful synthesis of both MgAl<sub>2</sub>
O<sub>4</sub>
and CaCu<sub>3</sub>
Ti<sub>4</sub>
O<sub>12</sub>
(CCT) oxides exhibiting excellent di-electric properties. One approach employed the novel direct synthesis technique of electric discharge assisted mechanical milling (EDAMM) and the second used the more conventional method of controlled ball milling using the magneto-mechanical method followed by heat treatment of nano-structural products. By using EDAMM, nano-crystalline precursors for transformation into high di-electric constant ceramics could be formed in as little as 0.1% of the processing time required for conventional solid-state techniques while ball milling using the magneto method also resulted in nano-structural precursors powders suitable for reaction by heat treatment to form oxide supercapacitor. Sample characterisation was carried out using XRD, TEM and SEM. Di-electric property measurements were performed using AC-LCR and by DC meters.</s0><fC02 i1="01" i2="3"><s0>001B80A07W</s0>
</fC02><fC03 i1="01" i2="3" l="FRE"><s0>Décharge électrique</s0>
<s5>01</s5>
</fC03><fC03 i1="01" i2="3" l="ENG"><s0>Electric discharges</s0>
<s5>01</s5>
</fC03><fC03 i1="02" i2="3" l="FRE"><s0>Alliage mécanique</s0>
<s5>02</s5>
</fC03><fC03 i1="02" i2="3" l="ENG"><s0>Mechanical alloying</s0>
<s5>02</s5>
</fC03><fC03 i1="03" i2="X" l="FRE"><s0>Céramique oxyde</s0>
<s5>03</s5>
</fC03><fC03 i1="03" i2="X" l="ENG"><s0>Oxide ceramics</s0>
<s5>03</s5>
</fC03><fC03 i1="03" i2="X" l="SPA"><s0>Cerámica óxido</s0>
<s5>03</s5>
</fC03><fC03 i1="04" i2="X" l="FRE"><s0>Réaction état solide</s0>
<s5>04</s5>
</fC03><fC03 i1="04" i2="X" l="ENG"><s0>Solid state reaction</s0>
<s5>04</s5>
</fC03><fC03 i1="04" i2="X" l="SPA"><s0>Reacción estado sólido</s0>
<s5>04</s5>
</fC03><fC03 i1="05" i2="3" l="FRE"><s0>Frittage</s0>
<s5>05</s5>
</fC03><fC03 i1="05" i2="3" l="ENG"><s0>Sintering</s0>
<s5>05</s5>
</fC03><fC03 i1="06" i2="3" l="FRE"><s0>Traitement thermique</s0>
<s5>06</s5>
</fC03><fC03 i1="06" i2="3" l="ENG"><s0>Heat treatments</s0>
<s5>06</s5>
</fC03><fC03 i1="07" i2="3" l="FRE"><s0>Précurseur</s0>
<s5>07</s5>
</fC03><fC03 i1="07" i2="3" l="ENG"><s0>Precursor</s0>
<s5>07</s5>
</fC03><fC03 i1="08" i2="X" l="FRE"><s0>Nanopoudre</s0>
<s5>08</s5>
</fC03><fC03 i1="08" i2="X" l="ENG"><s0>Nanopowder</s0>
<s5>08</s5>
</fC03><fC03 i1="08" i2="X" l="SPA"><s0>Nanopolvo</s0>
<s5>08</s5>
</fC03><fC03 i1="09" i2="3" l="FRE"><s0>Diffraction RX</s0>
<s5>09</s5>
</fC03><fC03 i1="09" i2="3" l="ENG"><s0>XRD</s0>
<s5>09</s5>
</fC03><fC03 i1="10" i2="3" l="FRE"><s0>Microscopie électronique transmission</s0>
<s5>10</s5>
</fC03><fC03 i1="10" i2="3" l="ENG"><s0>Transmission electron microscopy</s0>
<s5>10</s5>
</fC03><fC03 i1="11" i2="3" l="FRE"><s0>Microscopie électronique balayage</s0>
<s5>11</s5>
</fC03><fC03 i1="11" i2="3" l="ENG"><s0>Scanning electron microscopy</s0>
<s5>11</s5>
</fC03><fC03 i1="12" i2="3" l="FRE"><s0>CaCu3Ti4O12</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03><fC03 i1="13" i2="3" l="FRE"><s0>8107W</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03><fN21><s1>019</s1>
</fN21><fN44 i1="01"><s1>OTO</s1>
</fN44><fN82><s1>OTO</s1>
</fN82><pR><fA30 i1="01" i2="1" l="ENG"><s1>European Materials Research Society Spring Meeting. Symposium 'Nanomaterials for Energy Conversion and Storage'</s1>
<s3>Strasbourg FRA</s3>
<s4>2013-05-27</s4>
</fA30>
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