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Synthetic Route Effect on Macromolecular Architecture: From Block to Gradient Copolymers Based on Acryloyl Galactose Monomer Using RAFT Polymerization

Identifieur interne : 001632 ( PascalFrancis/Checkpoint ); précédent : 001631; suivant : 001633

Synthetic Route Effect on Macromolecular Architecture: From Block to Gradient Copolymers Based on Acryloyl Galactose Monomer Using RAFT Polymerization

Auteurs : Pierre Escale [France, Australie] ; S. R. Simon Ting [Australie] ; Abdel Khoukh [France] ; Laurent Rubatat [France] ; Maud Save [France] ; Martina H. Stenzel [Australie] ; Laurent Billon [France]

Source :

RBID : Pascal:11-0366829

Descripteurs français

English descriptors

Abstract

Statistical, gradient, and block copolymer containing 2-(2',3',4',6'-tetra-O-acetyl-β-D-galactosyloxy)ethyl acrylate (AcGalEA) glycomonomer and styrene (S) were synthesized by RAFT polymerization using S-methoxycarbonylphenylmethyl dodecyltrithiocarbonate (MCPDT) as control agent. The block copolymer was synthesized by a two-stage experiment, whereas the statistical and gradient copolymers were obtained in one-pot synthesis. Results obtained from the size exclusion chromatography (SEC) and the nuclear magnetic resonance (NMR) reveal that the polymers synthesized by RAFT were controlled. The kinetic of each synthetic route was investigated, and the reactivity ratio of both monomers was estimated by in situ NMR experiments: AcGalEA = 0.07 ± 0.01 and rs = 0.7 ± 0.1. Moreover the AcGalEA moieties were deacetylated to achieve potential amphiphilic bioactive copolymer. The preparation of three different macromolecular architectures to form honeycomb porous films by breath figure process was investigated using atomic force microscopy (AFM).


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<s0>Copolymère biséquencé</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG">
<s0>Diblock copolymer</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA">
<s0>Copolímero bisecuencia</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE">
<s0>Copolymère statistique</s0>
<s2>NK</s2>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG">
<s0>Random copolymer</s0>
<s2>NK</s2>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA">
<s0>Copolímero estadístico</s0>
<s2>NK</s2>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE">
<s0>Acrylate copolymère</s0>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG">
<s0>Acrylate copolymer</s0>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA">
<s0>Acrilato copolímero</s0>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE">
<s0>Copolymère vivant</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG">
<s0>Living copolymer</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA">
<s0>Copolímero viviente</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE">
<s0>Groupe latéral</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG">
<s0>Lateral group</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA">
<s0>Grupo lateral</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE">
<s0>Aldose</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG">
<s0>Aldose</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA">
<s0>Aldosa</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE">
<s0>Glycoside</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG">
<s0>Glycoside</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA">
<s0>Glicósido</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE">
<s0>Préparation</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG">
<s0>Preparation</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA">
<s0>Preparación</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE">
<s0>Copolymérisation radicalaire</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG">
<s0>Radical copolymerization</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA">
<s0>Copolimerización radical</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE">
<s0>Transfert chaîne</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG">
<s0>Chain transfer</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA">
<s0>Transferencia en cadena</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE">
<s0>Trithiocarbonate organique</s0>
<s1>ACT</s1>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG">
<s0>Organic trithiocarbonate</s0>
<s1>ACT</s1>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA">
<s0>Tritiocarbonato orgánico</s0>
<s1>ACT</s1>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE">
<s0>Rapport réactivité</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG">
<s0>Reactivity ratio</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA">
<s0>Relación reactividad</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE">
<s0>Modification chimique</s0>
<s5>15</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG">
<s0>Chemical modification</s0>
<s5>15</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA">
<s0>Modificación química</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE">
<s0>Désacétylation</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG">
<s0>Deacetylation</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA">
<s0>Desacetilación</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE">
<s0>Film</s0>
<s5>18</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG">
<s0>Film</s0>
<s5>18</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA">
<s0>Película</s0>
<s5>18</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE">
<s0>Matériau poreux</s0>
<s5>19</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG">
<s0>Porous material</s0>
<s5>19</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA">
<s0>Material poroso</s0>
<s5>19</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE">
<s0>Morphologie</s0>
<s5>20</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG">
<s0>Morphology</s0>
<s5>20</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA">
<s0>Morfología</s0>
<s5>20</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE">
<s0>Structure nid abeille</s0>
<s5>21</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG">
<s0>Honeycomb structure</s0>
<s5>21</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA">
<s0>Estructura alveolar</s0>
<s5>21</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE">
<s0>Etude expérimentale</s0>
<s5>22</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG">
<s0>Experimental study</s0>
<s5>22</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA">
<s0>Estudio experimental</s0>
<s5>22</s5>
</fC03>
<fC03 i1="21" i2="X" l="FRE">
<s0>Addition fragmentation réversible</s0>
<s4>INC</s4>
<s5>32</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE">
<s0>Coulée solution</s0>
<s4>INC</s4>
<s5>33</s5>
</fC03>
<fC03 i1="23" i2="X" l="FRE">
<s0>Méthode figures souffle</s0>
<s4>INC</s4>
<s5>34</s5>
</fC03>
<fC03 i1="24" i2="X" l="FRE">
<s0>Glycopolymère</s0>
<s4>CD</s4>
<s5>96</s5>
</fC03>
<fC03 i1="24" i2="X" l="ENG">
<s0>Glycopolymer</s0>
<s4>CD</s4>
<s5>96</s5>
</fC03>
<fC03 i1="25" i2="X" l="FRE">
<s0>Copolymère gradient</s0>
<s4>CD</s4>
<s5>97</s5>
</fC03>
<fC03 i1="25" i2="X" l="ENG">
<s0>Gradient copolymer</s0>
<s4>CD</s4>
<s5>97</s5>
</fC03>
<fN21>
<s1>249</s1>
</fN21>
<fN44 i1="01">
<s1>PSI</s1>
</fN44>
<fN82>
<s1>PSI</s1>
</fN82>
</pA>
</standard>
</inist>
<affiliations>
<list>
<country>
<li>Australie</li>
<li>France</li>
</country>
</list>
<tree>
<country name="France">
<noRegion>
<name sortKey="Escale, Pierre" sort="Escale, Pierre" uniqKey="Escale P" first="Pierre" last="Escale">Pierre Escale</name>
</noRegion>
<name sortKey="Billon, Laurent" sort="Billon, Laurent" uniqKey="Billon L" first="Laurent" last="Billon">Laurent Billon</name>
<name sortKey="Khoukh, Abdel" sort="Khoukh, Abdel" uniqKey="Khoukh A" first="Abdel" last="Khoukh">Abdel Khoukh</name>
<name sortKey="Rubatat, Laurent" sort="Rubatat, Laurent" uniqKey="Rubatat L" first="Laurent" last="Rubatat">Laurent Rubatat</name>
<name sortKey="Save, Maud" sort="Save, Maud" uniqKey="Save M" first="Maud" last="Save">Maud Save</name>
</country>
<country name="Australie">
<noRegion>
<name sortKey="Escale, Pierre" sort="Escale, Pierre" uniqKey="Escale P" first="Pierre" last="Escale">Pierre Escale</name>
</noRegion>
<name sortKey="Simon Ting, S R" sort="Simon Ting, S R" uniqKey="Simon Ting S" first="S. R." last="Simon Ting">S. R. Simon Ting</name>
<name sortKey="Stenzel, Martina H" sort="Stenzel, Martina H" uniqKey="Stenzel M" first="Martina H." last="Stenzel">Martina H. Stenzel</name>
</country>
</tree>
</affiliations>
</record>

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