Electron Backscatter Diffraction and Transmission Kikuchi Diffraction Analysis of an Austenitic Stainless Steel Subjected to Surface Mechanical Attrition Treatment and Plasma Nitriding.
Identifieur interne : 002E60 ( Main/Exploration ); précédent : 002E59; suivant : 002E61Electron Backscatter Diffraction and Transmission Kikuchi Diffraction Analysis of an Austenitic Stainless Steel Subjected to Surface Mechanical Attrition Treatment and Plasma Nitriding.
Auteurs : Gwénaëlle Proust [Australie] ; Delphine Retraint [France] ; Mahdi Chemkhi [France] ; Arjen Roos [France] ; Clemence Demangel [France]Source :
- Microscopy and microanalysis : the official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada [ 1435-8115 ] ; 2015.
Descripteurs français
- KwdFr :
- MESH :
English descriptors
- KwdEn :
- MESH :
- chemical , analysis : Nitrogen.
- chemical , chemistry : Biocompatible Materials, Stainless Steel.
- analysis : Metal Nanoparticles.
- Materials Testing, Microscopy, Electron, Transmission, Plasma Gases, Surface Properties, X-Ray Diffraction.
Abstract
Austenitic 316L stainless steel can be used for orthopedic implants due to its biocompatibility and high corrosion resistance. Its range of applications in this field could be broadened by improving its wear and friction properties. Surface properties can be modified through surface hardening treatments. The effects of such treatments on the microstructure of the alloy were investigated here. Surface Mechanical Attrition Treatment (SMAT) is a surface treatment that enhances mechanical properties of the material surface by creating a thin nanocrystalline layer. After SMAT, some specimens underwent a plasma nitriding process to further enhance their surface properties. Using electron backscatter diffraction, transmission Kikuchi diffraction, energy dispersive spectroscopy, and transmission electron microscopy, the microstructural evolution of the stainless steel after these different surface treatments was characterized. Microstructural features investigated include thickness of the nanocrystalline layer, size of the grains within the nanocrystalline layer, and depth of diffusion of nitrogen atoms within the material.
DOI: 10.1017/S1431927615000793
PubMed: 26139391
Affiliations:
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Delautre,08000 Charleville-Mézières,France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>3CRITT-MDTS,3 bd J. Delautre,08000 Charleville-Mézières</wicri:regionArea><wicri:noRegion>08000 Charleville-Mézières</wicri:noRegion><wicri:noRegion>08000 Charleville-Mézières</wicri:noRegion></affiliation></author></analytic><series><title level="j">Microscopy and microanalysis : the official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada</title><idno type="eISSN">1435-8115</idno><imprint><date when="2015" type="published">2015</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Biocompatible Materials (chemistry)</term><term>Materials Testing</term><term>Metal Nanoparticles (analysis)</term><term>Microscopy, Electron, Transmission</term><term>Nitrogen (analysis)</term><term>Plasma Gases</term><term>Stainless Steel (chemistry)</term><term>Surface Properties</term><term>X-Ray Diffraction</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Acier inoxydable ()</term><term>Azote (analyse)</term><term>Diffraction des rayons X</term><term>Gaz plasmas</term><term>Matériaux biocompatibles ()</term><term>Microscopie électronique à transmission</term><term>Nanoparticules métalliques (analyse)</term><term>Propriétés de surface</term><term>Test de matériaux</term></keywords><keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Nitrogen</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Biocompatible Materials</term><term>Stainless Steel</term></keywords><keywords scheme="MESH" qualifier="analyse" xml:lang="fr"><term>Azote</term><term>Nanoparticules métalliques</term></keywords><keywords scheme="MESH" qualifier="analysis" xml:lang="en"><term>Metal Nanoparticles</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Materials Testing</term><term>Microscopy, Electron, Transmission</term><term>Plasma Gases</term><term>Surface Properties</term><term>X-Ray Diffraction</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Acier inoxydable</term><term>Diffraction des rayons X</term><term>Gaz plasmas</term><term>Matériaux biocompatibles</term><term>Microscopie électronique à transmission</term><term>Propriétés de surface</term><term>Test de matériaux</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Austenitic 316L stainless steel can be used for orthopedic implants due to its biocompatibility and high corrosion resistance. Its range of applications in this field could be broadened by improving its wear and friction properties. Surface properties can be modified through surface hardening treatments. The effects of such treatments on the microstructure of the alloy were investigated here. Surface Mechanical Attrition Treatment (SMAT) is a surface treatment that enhances mechanical properties of the material surface by creating a thin nanocrystalline layer. After SMAT, some specimens underwent a plasma nitriding process to further enhance their surface properties. Using electron backscatter diffraction, transmission Kikuchi diffraction, energy dispersive spectroscopy, and transmission electron microscopy, the microstructural evolution of the stainless steel after these different surface treatments was characterized. Microstructural features investigated include thickness of the nanocrystalline layer, size of the grains within the nanocrystalline layer, and depth of diffusion of nitrogen atoms within the material.</div></front></TEI><affiliations><list><country><li>Australie</li><li>France</li></country><region><li>Nouvelle-Galles du Sud</li></region><settlement><li>Sydney</li></settlement><orgName><li>Université de Sydney</li></orgName></list><tree><country name="Australie"><region name="Nouvelle-Galles du Sud"><name sortKey="Proust, Gwenaelle" sort="Proust, Gwenaelle" uniqKey="Proust G" first="Gwénaëlle" last="Proust">Gwénaëlle Proust</name></region></country><country name="France"><noRegion><name sortKey="Retraint, Delphine" sort="Retraint, Delphine" uniqKey="Retraint D" first="Delphine" last="Retraint">Delphine Retraint</name></noRegion><name sortKey="Chemkhi, Mahdi" sort="Chemkhi, Mahdi" uniqKey="Chemkhi M" first="Mahdi" last="Chemkhi">Mahdi Chemkhi</name><name sortKey="Demangel, Clemence" sort="Demangel, Clemence" uniqKey="Demangel C" first="Clemence" last="Demangel">Clemence Demangel</name><name sortKey="Roos, Arjen" sort="Roos, Arjen" uniqKey="Roos A" first="Arjen" last="Roos">Arjen Roos</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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