Heterogeneous grain-scale response in ferroic polycrystals under electric field
Identifieur interne : 001D68 ( Main/Exploration ); précédent : 001D67; suivant : 001D69Heterogeneous grain-scale response in ferroic polycrystals under electric field
Auteurs : John E. Daniels [Australie] ; Marta Majkut [Danemark] ; Qingua Cao [Australie] ; S Ren Schmidt [Danemark] ; Jon Wright [France] ; Wook Jo [Corée du Sud] ; Jette Oddershede [Danemark]Source :
- Scientific Reports [ 2045-2322 ] ; 2016.
Abstract
Understanding coupling of ferroic properties over grain boundaries and within clusters of grains in polycrystalline materials is hindered due to a lack of direct experimental methods to probe the behaviour of individual grains in the bulk of a material. Here, a variant of three-dimensional X-ray diffraction (3D-XRD) is used to resolve the non-180° ferroelectric domain switching strain components of 191 grains from the bulk of a polycrystalline electro-ceramic that has undergone an electric-field-induced phase transformation. It is found that while the orientation of a given grain relative to the field direction has a significant influence on the phase and resultant domain texture, there are large deviations from the average behaviour at the grain scale. It is suggested that these deviations arise from local strain and electric field neighbourhoods being highly heterogeneous within the bulk polycrystal. Additionally, the minimisation of electrostatic potentials at the grain boundaries due to interacting ferroelectric domains must also be considered. It is found that the local grain-scale deviations average out over approximately 10–20 grains. These results provide unique insight into the grain-scale interactions of ferroic materials and will be of value for future efforts to comprehensively model these and related materials at that length-scale.
Url:
DOI: 10.1038/srep22820
PubMed: 26955960
PubMed Central: 4783773
Affiliations:
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Daniels</name><affiliation wicri:level="1"><nlm:aff id="a1"><institution>School of Materials Science and Engineering, UNSW Australia</institution>, Sydney NSW 2052,<country>Australia</country></nlm:aff><country xml:lang="fr">Australie</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Majkut, Marta" sort="Majkut, Marta" uniqKey="Majkut M" first="Marta" last="Majkut">Marta Majkut</name><affiliation wicri:level="1"><nlm:aff id="a2"><institution>NEXMAP, DTU Physics, 2800 Kgs. 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Lyngby</institution>,<country>Denmark</country></nlm:aff><country xml:lang="fr">Danemark</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author></analytic><series><title level="j">Scientific Reports</title><idno type="eISSN">2045-2322</idno><imprint><date when="2016">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>Understanding coupling of ferroic properties over grain boundaries and within clusters of grains in polycrystalline materials is hindered due to a lack of direct experimental methods to probe the behaviour of individual grains in the bulk of a material. Here, a variant of three-dimensional X-ray diffraction (3D-XRD) is used to resolve the non-180° ferroelectric domain switching strain components of 191 grains from the bulk of a polycrystalline electro-ceramic that has undergone an electric-field-induced phase transformation. It is found that while the orientation of a given grain relative to the field direction has a significant influence on the phase and resultant domain texture, there are large deviations from the average behaviour at the grain scale. It is suggested that these deviations arise from local strain and electric field neighbourhoods being highly heterogeneous within the bulk polycrystal. Additionally, the minimisation of electrostatic potentials at the grain boundaries due to interacting ferroelectric domains must also be considered. It is found that the local grain-scale deviations average out over approximately 10–20 grains. These results provide unique insight into the grain-scale interactions of ferroic materials and will be of value for future efforts to comprehensively model these and related materials at that length-scale.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Rodel, J" uniqKey="Rodel J">J. Rödel</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Park, S E" uniqKey="Park S">S.-E. Park</name></author><author><name sortKey="Shrout, T R" uniqKey="Shrout T">T. R. Shrout</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Schneider, D" uniqKey="Schneider D">D. Schneider</name></author><author><name sortKey="Jo, W" uniqKey="Jo W">W. Jo</name></author><author><name sortKey="Rodel, J" uniqKey="Rodel J">J. Rödel</name></author><author><name sortKey="Rytz, D" uniqKey="Rytz D">D. Rytz</name></author><author><name sortKey="Granzow, T" uniqKey="Granzow T">T. 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