The effect of absorbed hydrogen on the dissolution of steel
Identifieur interne : 001587 ( Main/Curation ); précédent : 001586; suivant : 001588The effect of absorbed hydrogen on the dissolution of steel
Auteurs : Sebastian Thomas [Australie] ; Noemie Ott [Australie, France] ; Rebecca F. Schaller [Australie, États-Unis] ; Jodie A. Yuwono [Australie] ; Polina Volovitch [France] ; Guruprasad Sundararajan [Inde] ; Nikhil V. Medhekar [Australie] ; Kevin Ogle [France] ; John R. Scully [États-Unis] ; Nick Birbilis [Australie]Source :
- Heliyon [ 2405-8440 ] ; 2016.
Abstract
Atomic hydrogen (H) was introduced into steel (AISI 1018 mild steel) by controlled cathodic pre-charging. The resultant steel sample, comprising about 1 ppmw diffusible H, and a reference uncharged sample, were studied using atomic emission spectroelectrochemistry (AESEC). AESEC involved potentiodynamic polarisation in a flowing non-passivating electrolyte (0.6 M NaCl, pH 1.95) with real time reconciliation of metal dissolution using on-line inductively coupled plasma-atomic emission spectroscopy (ICP-OES). The presence of absorbed H was shown to significantly increase anodic Fe dissolution, as evidenced by the enhanced detection of Fe2+ ions by ICP-OES. We discuss this important finding in the context of previously proposed mechanisms for H-effects on the corrosion of steels.
Url:
DOI: 10.1016/j.heliyon.2016.e00209
PubMed: 27981250
PubMed Central: 5148784
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Schaller</name><affiliation wicri:level="1"><nlm:aff id="aff0005">Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800, Australia</nlm:aff><country xml:lang="fr">Australie</country><wicri:regionArea>Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800</wicri:regionArea><wicri:noRegion>Victoria 3800</wicri:noRegion></affiliation><affiliation wicri:level="2"><nlm:aff id="aff0015">Department of Materials Science and Engineering, University of Virginia, Charlottesville, VA 22904, USA</nlm:aff><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Materials Science and Engineering, University of Virginia, Charlottesville, VA 22904</wicri:regionArea><placeName><region type="state">Virginie</region></placeName></affiliation></author><author><name sortKey="Yuwono, Jodie A" sort="Yuwono, Jodie A" uniqKey="Yuwono J" first="Jodie A." last="Yuwono">Jodie A. Yuwono</name><affiliation wicri:level="1"><nlm:aff id="aff0005">Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800, Australia</nlm:aff><country xml:lang="fr">Australie</country><wicri:regionArea>Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800</wicri:regionArea><wicri:noRegion>Victoria 3800</wicri:noRegion></affiliation></author><author><name sortKey="Volovitch, Polina" sort="Volovitch, Polina" uniqKey="Volovitch P" first="Polina" last="Volovitch">Polina Volovitch</name><affiliation wicri:level="1"><nlm:aff id="aff0010">Chimie ParisTech, Ecole Nationale Supurieure de Chimie de Paris, Paris 75005, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Chimie ParisTech, Ecole Nationale Supurieure de Chimie de Paris, Paris 75005</wicri:regionArea><wicri:noRegion>75005</wicri:noRegion><placeName><settlement type="city">Paris</settlement><region type="région" nuts="2">Île-de-France</region></placeName></affiliation></author><author><name sortKey="Sundararajan, Guruprasad" sort="Sundararajan, Guruprasad" uniqKey="Sundararajan G" first="Guruprasad" last="Sundararajan">Guruprasad Sundararajan</name><affiliation wicri:level="1"><nlm:aff id="aff0020">GE Global Research, Bangalore 560066, India</nlm:aff><country xml:lang="fr">Inde</country><wicri:regionArea>GE Global Research, Bangalore 560066</wicri:regionArea><wicri:noRegion>Bangalore 560066</wicri:noRegion></affiliation></author><author><name sortKey="Medhekar, Nikhil V" sort="Medhekar, Nikhil V" uniqKey="Medhekar N" first="Nikhil V." last="Medhekar">Nikhil V. Medhekar</name><affiliation wicri:level="1"><nlm:aff id="aff0005">Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800, Australia</nlm:aff><country xml:lang="fr">Australie</country><wicri:regionArea>Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800</wicri:regionArea><wicri:noRegion>Victoria 3800</wicri:noRegion></affiliation></author><author><name sortKey="Ogle, Kevin" sort="Ogle, Kevin" uniqKey="Ogle K" first="Kevin" last="Ogle">Kevin Ogle</name><affiliation wicri:level="1"><nlm:aff id="aff0010">Chimie ParisTech, Ecole Nationale Supurieure de Chimie de Paris, Paris 75005, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Chimie ParisTech, Ecole Nationale Supurieure de Chimie de Paris, Paris 75005</wicri:regionArea><wicri:noRegion>75005</wicri:noRegion><placeName><settlement type="city">Paris</settlement><region type="région" nuts="2">Île-de-France</region></placeName></affiliation></author><author><name sortKey="Scully, John R" sort="Scully, John R" uniqKey="Scully J" first="John R." last="Scully">John R. Scully</name><affiliation wicri:level="2"><nlm:aff id="aff0015">Department of Materials Science and Engineering, University of Virginia, Charlottesville, VA 22904, USA</nlm:aff><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Materials Science and Engineering, University of Virginia, Charlottesville, VA 22904</wicri:regionArea><placeName><region type="state">Virginie</region></placeName></affiliation></author><author><name sortKey="Birbilis, Nick" sort="Birbilis, Nick" uniqKey="Birbilis N" first="Nick" last="Birbilis">Nick Birbilis</name><affiliation wicri:level="1"><nlm:aff id="aff0005">Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800, Australia</nlm:aff><country xml:lang="fr">Australie</country><wicri:regionArea>Department of Materials Science and Engineering, Monash University, Clayton, Victoria 3800</wicri:regionArea><wicri:noRegion>Victoria 3800</wicri:noRegion></affiliation></author></analytic><series><title level="j">Heliyon</title><idno type="eISSN">2405-8440</idno><imprint><date when="2016">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>Atomic hydrogen (H) was introduced into steel (AISI 1018 mild steel) by controlled cathodic pre-charging. The resultant steel sample, comprising about 1 ppmw diffusible H, and a reference uncharged sample, were studied using atomic emission spectroelectrochemistry (AESEC). AESEC involved potentiodynamic polarisation in a flowing non-passivating electrolyte (0.6 M NaCl, pH 1.95) with real time reconciliation of metal dissolution using on-line inductively coupled plasma-atomic emission spectroscopy (ICP-OES). The presence of absorbed H was shown to significantly increase anodic Fe dissolution, as evidenced by the enhanced detection of Fe<sup>2+</sup> ions by ICP-OES. We discuss this important finding in the context of previously proposed mechanisms for H-effects on the corrosion of steels.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Rawls, G B" uniqKey="Rawls G">G.B. Rawls</name></author><author><name sortKey="Adams, T" uniqKey="Adams T">T. Adams</name></author><author><name sortKey="Newhouse, N L" uniqKey="Newhouse N">N.L. 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