Serveur d'exploration sur le nickel au Maghreb

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X-ray diffraction, microstructure, Mössbauer and magnetization studies of nanostructured Fe50Ni50 alloy prepared by mechanical alloying

Identifieur interne : 000213 ( PascalFrancis/Curation ); précédent : 000212; suivant : 000214

X-ray diffraction, microstructure, Mössbauer and magnetization studies of nanostructured Fe50Ni50 alloy prepared by mechanical alloying

Auteurs : A. Guittoum [Algérie] ; A. Layadi [Algérie] ; A. Bourzami [Algérie] ; H. Tafat [Algérie] ; N. Souami [Algérie] ; S. Boutarfaia [Algérie] ; D. Lacour [France]

Source :

RBID : Pascal:08-0253702

Descripteurs français

English descriptors

Abstract

Nanocrystalline Fe50Ni50 alloy samples were prepared by the mechanical alloying process using planetary high-energy ball mill. The alloy formation and different physical properties were investigated as a function of milling time, t, (in the 0-50 h range) by means of the X-ray diffraction (XRD) technique, scanning electron microscopy (SEM), energy dispersive X-ray (EDAX), Mössbauer spectroscopy and the vibrating sample magnetometer (VSM). The complete formation of γ-FeNi is observed after 24 h milling. When milling time increases from 0 to 50 h, the lattice parameter increases towards the Fe50Ni50 bulk value, the grain size decreases from 67 to 13 nm, while the strain increases from 0.09% to 0.41%. Grain morphologies at different formation stages were observed by SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.
pA  
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A08 01  1  ENG  @1 X-ray diffraction, microstructure, Mössbauer and magnetization studies of nanostructured Fe50Ni50 alloy prepared by mechanical alloying
A11 01  1    @1 GUITTOUM (A.)
A11 02  1    @1 LAYADI (A.)
A11 03  1    @1 BOURZAMI (A.)
A11 04  1    @1 TAFAT (H.)
A11 05  1    @1 SOUAMI (N.)
A11 06  1    @1 BOUTARFAIA (S.)
A11 07  1    @1 LACOUR (D.)
A14 01      @1 Nuclear Research Center of Algiers, 2 Bd Frantz Fanon, BP 399, Alger-Gare @2 Alger @3 DZA @Z 1 aut. @Z 5 aut.
A14 02      @1 Département de Physique, Faculté des Sciences, Université de Sétif @2 19000 @3 DZA @Z 2 aut. @Z 3 aut.
A14 03      @1 Laboratory S.G.M., UST.H.B., BP 32 @2 Bab-Ezzouar @3 DZA @Z 4 aut.
A14 04      @1 Centre de Recherche Nucléaire de Draria, BP 43 @2 Alger @3 DZA @Z 6 aut.
A14 05      @1 LPM, Nancy-University, CNRS @2 54506 Vandoeuvre les Nancy @3 FRA @Z 7 aut.
A20       @1 1385-1392
A21       @1 2008
A23 01      @0 ENG
A43 01      @1 INIST @2 17230 @5 354000173641010220
A44       @0 0000 @1 © 2008 INIST-CNRS. All rights reserved.
A45       @0 37 ref.
A47 01  1    @0 08-0253702
A60       @1 P
A61       @0 A
A64 01  1    @0 Journal of magnetism and magnetic materials
A66 01      @0 NLD
C01 01    ENG  @0 Nanocrystalline Fe50Ni50 alloy samples were prepared by the mechanical alloying process using planetary high-energy ball mill. The alloy formation and different physical properties were investigated as a function of milling time, t, (in the 0-50 h range) by means of the X-ray diffraction (XRD) technique, scanning electron microscopy (SEM), energy dispersive X-ray (EDAX), Mössbauer spectroscopy and the vibrating sample magnetometer (VSM). The complete formation of γ-FeNi is observed after 24 h milling. When milling time increases from 0 to 50 h, the lattice parameter increases towards the Fe50Ni50 bulk value, the grain size decreases from 67 to 13 nm, while the strain increases from 0.09% to 0.41%. Grain morphologies at different formation stages were observed by SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.
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C02 02  3    @0 001B70F80
C02 03  3    @0 001B70E75
C03 01  3  FRE  @0 Diffraction RX @5 02
C03 01  3  ENG  @0 XRD @5 02
C03 02  3  FRE  @0 Microstructure @5 03
C03 02  3  ENG  @0 Microstructure @5 03
C03 03  3  FRE  @0 Effet Mössbauer @5 04
C03 03  3  ENG  @0 Moessbauer effect @5 04
C03 04  X  FRE  @0 Aimantation saturation @5 05
C03 04  X  ENG  @0 Saturation magnetization @5 05
C03 04  X  SPA  @0 Imanación saturación @5 05
C03 05  3  FRE  @0 Alliage mécanique @5 06
C03 05  3  ENG  @0 Mechanical alloying @5 06
C03 06  X  FRE  @0 Broyeur boulet @5 07
C03 06  X  ENG  @0 Ball mill @5 07
C03 06  X  SPA  @0 Molino bolas @5 07
C03 07  X  FRE  @0 Broyeur satellite @5 08
C03 07  X  ENG  @0 Planetary mill @5 08
C03 07  X  SPA  @0 Molino rodillos satelite @5 08
C03 08  3  FRE  @0 Microscopie électronique balayage @5 09
C03 08  3  ENG  @0 Scanning electron microscopy @5 09
C03 09  3  FRE  @0 Force coercitive @5 10
C03 09  3  ENG  @0 Coercive force @5 10
C03 10  3  FRE  @0 Hystérésis magnétique @5 11
C03 10  3  ENG  @0 Magnetic hysteresis @5 11
C03 11  3  FRE  @0 Paramètre cristallin @5 12
C03 11  3  ENG  @0 Lattice parameters @5 12
C03 12  3  FRE  @0 Fer alliage @5 15
C03 12  3  ENG  @0 Iron alloys @5 15
C03 13  X  FRE  @0 Nanocristal @5 16
C03 13  X  ENG  @0 Nanocrystal @5 16
C03 13  X  SPA  @0 Nanocristal @5 16
C03 14  3  FRE  @0 Nickel alliage @5 17
C03 14  3  ENG  @0 Nickel alloys @5 17
C03 15  3  FRE  @0 Métal transition alliage @5 48
C03 15  3  ENG  @0 Transition element alloys @5 48
N21       @1 162

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<term>Microstructure</term>
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<div type="abstract" xml:lang="en">Nanocrystalline Fe
<sub>50</sub>
Ni
<sub>50</sub>
alloy samples were prepared by the mechanical alloying process using planetary high-energy ball mill. The alloy formation and different physical properties were investigated as a function of milling time, t, (in the 0-50 h range) by means of the X-ray diffraction (XRD) technique, scanning electron microscopy (SEM), energy dispersive X-ray (EDAX), Mössbauer spectroscopy and the vibrating sample magnetometer (VSM). The complete formation of γ-FeNi is observed after 24 h milling. When milling time increases from 0 to 50 h, the lattice parameter increases towards the Fe
<sub>50</sub>
Ni
<sub>50</sub>
bulk value, the grain size decreases from 67 to 13 nm, while the strain increases from 0.09% to 0.41%. Grain morphologies at different formation stages were observed by SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.</div>
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<sub>50</sub>
Ni
<sub>50</sub>
alloy samples were prepared by the mechanical alloying process using planetary high-energy ball mill. The alloy formation and different physical properties were investigated as a function of milling time, t, (in the 0-50 h range) by means of the X-ray diffraction (XRD) technique, scanning electron microscopy (SEM), energy dispersive X-ray (EDAX), Mössbauer spectroscopy and the vibrating sample magnetometer (VSM). The complete formation of γ-FeNi is observed after 24 h milling. When milling time increases from 0 to 50 h, the lattice parameter increases towards the Fe
<sub>50</sub>
Ni
<sub>50</sub>
bulk value, the grain size decreases from 67 to 13 nm, while the strain increases from 0.09% to 0.41%. Grain morphologies at different formation stages were observed by SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.</s0>
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<s5>05</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG">
<s0>Saturation magnetization</s0>
<s5>05</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA">
<s0>Imanación saturación</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE">
<s0>Alliage mécanique</s0>
<s5>06</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG">
<s0>Mechanical alloying</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE">
<s0>Broyeur boulet</s0>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG">
<s0>Ball mill</s0>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA">
<s0>Molino bolas</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE">
<s0>Broyeur satellite</s0>
<s5>08</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG">
<s0>Planetary mill</s0>
<s5>08</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA">
<s0>Molino rodillos satelite</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE">
<s0>Microscopie électronique balayage</s0>
<s5>09</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG">
<s0>Scanning electron microscopy</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE">
<s0>Force coercitive</s0>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG">
<s0>Coercive force</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE">
<s0>Hystérésis magnétique</s0>
<s5>11</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG">
<s0>Magnetic hysteresis</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE">
<s0>Paramètre cristallin</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG">
<s0>Lattice parameters</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE">
<s0>Fer alliage</s0>
<s5>15</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG">
<s0>Iron alloys</s0>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE">
<s0>Nanocristal</s0>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG">
<s0>Nanocrystal</s0>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA">
<s0>Nanocristal</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE">
<s0>Nickel alliage</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG">
<s0>Nickel alloys</s0>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE">
<s0>Métal transition alliage</s0>
<s5>48</s5>
</fC03>
<fC03 i1="15" i2="3" l="ENG">
<s0>Transition element alloys</s0>
<s5>48</s5>
</fC03>
<fN21>
<s1>162</s1>
</fN21>
</pA>
</standard>
</inist>
</record>

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   |texte=   X-ray diffraction, microstructure, Mössbauer and magnetization studies of nanostructured Fe50Ni50 alloy prepared by mechanical alloying
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