One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
Identifieur interne : 000129 ( Main/Merge ); précédent : 000128; suivant : 000130One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
Auteurs : Assem Barakat ; Mousa Al-Noaimi ; Mohammed Suleiman ; Abdullah S. Aldwayyan ; Belkheir Hammouti ; Taibi Ben Hadda ; Salim F. Haddad ; Ahmed Boshaala ; Ismail WaradSource :
- International Journal of Molecular Sciences [ 1422-0067 ] ; 2013.
Abstract
[NiCl2(C14H12N2)(H2O)] complex has been synthesized from nickel chloride hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as
Url:
DOI: 10.3390/ijms141223941
PubMed: 24351867
PubMed Central: 3876087
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PMC:3876087Le document en format XML
<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel <italic>Aqua</italic>
(2,9-dimethyl-1,10-phenanthroline)NiCl<sub>2</sub>
Complex</title>
<author><name sortKey="Barakat, Assem" sort="Barakat, Assem" uniqKey="Barakat A" first="Assem" last="Barakat">Assem Barakat</name>
<affiliation><nlm:aff id="af1-ijms-14-23941">Department of Chemistry, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>ambarakat@ksu.edu.sa</email>
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<author><name sortKey="Al Noaimi, Mousa" sort="Al Noaimi, Mousa" uniqKey="Al Noaimi M" first="Mousa" last="Al-Noaimi">Mousa Al-Noaimi</name>
<affiliation><nlm:aff id="af2-ijms-14-23941">Department of Chemistry, Hashemite University, Zarqa 13115, Jordan; E-Mail:<email>manoaimi@hu.edu.jo</email>
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<author><name sortKey="Suleiman, Mohammed" sort="Suleiman, Mohammed" uniqKey="Suleiman M" first="Mohammed" last="Suleiman">Mohammed Suleiman</name>
<affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email>
</nlm:aff>
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<author><name sortKey="Aldwayyan, Abdullah S" sort="Aldwayyan, Abdullah S" uniqKey="Aldwayyan A" first="Abdullah S." last="Aldwayyan">Abdullah S. Aldwayyan</name>
<affiliation><nlm:aff id="af4-ijms-14-23941">Department of Physics and Astronomy, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>dwayyan@ksu.edu.sa</email>
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<author><name sortKey="Hammouti, Belkheir" sort="Hammouti, Belkheir" uniqKey="Hammouti B" first="Belkheir" last="Hammouti">Belkheir Hammouti</name>
<affiliation><nlm:aff id="af5-ijms-14-23941">Laboratoire de Chimie Appliquée et Environnement, LCAE-URAC18, Faculity of Science, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>hammoutib@gmail.com</email>
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<affiliation><nlm:aff id="af7-ijms-14-23941">Department of Chemistry, the University of Jordan, Amman 11942, Jordan; E-Mail:<email>hadsal2003@yahoo.com</email>
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<author><name sortKey="Boshaala, Ahmed" sort="Boshaala, Ahmed" uniqKey="Boshaala A" first="Ahmed" last="Boshaala">Ahmed Boshaala</name>
<affiliation><nlm:aff id="af8-ijms-14-23941">Department of Chemistry, Faculty of Science, Benghazi University, P.O. Box 1308, Benghazi 5341, Libya; E-Mail:<email>ahmedboshaala@yahoo.co.uk</email>
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<author><name sortKey="Warad, Ismail" sort="Warad, Ismail" uniqKey="Warad I" first="Ismail" last="Warad">Ismail Warad</name>
<affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel <italic>Aqua</italic>
(2,9-dimethyl-1,10-phenanthroline)NiCl<sub>2</sub>
Complex</title>
<author><name sortKey="Barakat, Assem" sort="Barakat, Assem" uniqKey="Barakat A" first="Assem" last="Barakat">Assem Barakat</name>
<affiliation><nlm:aff id="af1-ijms-14-23941">Department of Chemistry, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>ambarakat@ksu.edu.sa</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Al Noaimi, Mousa" sort="Al Noaimi, Mousa" uniqKey="Al Noaimi M" first="Mousa" last="Al-Noaimi">Mousa Al-Noaimi</name>
<affiliation><nlm:aff id="af2-ijms-14-23941">Department of Chemistry, Hashemite University, Zarqa 13115, Jordan; E-Mail:<email>manoaimi@hu.edu.jo</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Suleiman, Mohammed" sort="Suleiman, Mohammed" uniqKey="Suleiman M" first="Mohammed" last="Suleiman">Mohammed Suleiman</name>
<affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Aldwayyan, Abdullah S" sort="Aldwayyan, Abdullah S" uniqKey="Aldwayyan A" first="Abdullah S." last="Aldwayyan">Abdullah S. Aldwayyan</name>
<affiliation><nlm:aff id="af4-ijms-14-23941">Department of Physics and Astronomy, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>dwayyan@ksu.edu.sa</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Hammouti, Belkheir" sort="Hammouti, Belkheir" uniqKey="Hammouti B" first="Belkheir" last="Hammouti">Belkheir Hammouti</name>
<affiliation><nlm:aff id="af5-ijms-14-23941">Laboratoire de Chimie Appliquée et Environnement, LCAE-URAC18, Faculity of Science, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>hammoutib@gmail.com</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Ben Hadda, Taibi" sort="Ben Hadda, Taibi" uniqKey="Ben Hadda T" first="Taibi" last="Ben Hadda">Taibi Ben Hadda</name>
<affiliation><nlm:aff id="af6-ijms-14-23941">Lab of Chemical Material, FSO, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>taibi.ben.hadda@gmail.com</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Haddad, Salim F" sort="Haddad, Salim F" uniqKey="Haddad S" first="Salim F." last="Haddad">Salim F. Haddad</name>
<affiliation><nlm:aff id="af7-ijms-14-23941">Department of Chemistry, the University of Jordan, Amman 11942, Jordan; E-Mail:<email>hadsal2003@yahoo.com</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Boshaala, Ahmed" sort="Boshaala, Ahmed" uniqKey="Boshaala A" first="Ahmed" last="Boshaala">Ahmed Boshaala</name>
<affiliation><nlm:aff id="af8-ijms-14-23941">Department of Chemistry, Faculty of Science, Benghazi University, P.O. Box 1308, Benghazi 5341, Libya; E-Mail:<email>ahmedboshaala@yahoo.co.uk</email>
</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Warad, Ismail" sort="Warad, Ismail" uniqKey="Warad I" first="Ismail" last="Warad">Ismail Warad</name>
<affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email>
</nlm:aff>
</affiliation>
</author>
</analytic>
<series><title level="j">International Journal of Molecular Sciences</title>
<idno type="eISSN">1422-0067</idno>
<imprint><date when="2013">2013</date>
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<front><div type="abstract" xml:lang="en"><p>[NiCl<sub>2</sub>
(C<sub>14</sub>
H<sub>12</sub>
N<sub>2</sub>
)(H<sub>2</sub>
O)] complex has been synthesized from nickel chloride hexahydrate (NiCl<sub>2</sub>
·6H<sub>2</sub>
O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as <italic>N</italic>
,<italic>N</italic>
-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 ºC in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).</p>
</div>
</front>
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